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Information card for entry 7157923
Preview
| Coordinates | 7157923.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C16 H17 N O4 |
|---|---|
| Calculated formula | C16 H17 N O4 |
| Title of publication | The effect of carbonyl on the isomerization of a galanthan ring system and total synthesis of (±)-β-lycorane. |
| Authors of publication | Liang, Leilei; Li, Ji; Shen, Baochun; Zhang, Yili; Liu, Jianping; Chen, Jingbo; Liu, Dandan |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2021 |
| Journal volume | 19 |
| Journal issue | 12 |
| Pages of publication | 2767 - 2772 |
| a | 5.2488 ± 0.0002 Å |
| b | 7.5956 ± 0.0003 Å |
| c | 33.4224 ± 0.0012 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 1332.48 ± 0.09 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0282 |
| Residual factor for significantly intense reflections | 0.0278 |
| Weighted residual factors for significantly intense reflections | 0.0734 |
| Weighted residual factors for all reflections included in the refinement | 0.0737 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.057 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 263853 (current) | 2021-04-05 | cif/ Updating files of 7157923 Original log message: Adding full bibliography for 7157923.cif. |
7157923.cif |
| 262454 | 2021-03-04 | cif/ Adding structures of 7157923 via cif-deposit CGI script. |
7157923.cif |
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Users of the data should acknowledge the original authors of the
structural data.