#------------------------------------------------------------------------------ #$Date: 2023-01-29 03:29:46 +0200 (Sun, 29 Jan 2023) $ #$Revision: 280658 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/15/91/7159122.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7159122 loop_ _publ_author_name 'Larin, Astrid' 'Pfrunder, Michael' 'Mullen, Kathleen' 'Wiedbrauk, Sandra' 'Boase, Nathan' 'Fairfull-Smith, Kathryn' _publ_section_title ; Synergistic or Antagonistic Antioxidant Combinations - A Case Study Exploring Flavonoid-Nitroxide Hybrids ; _journal_name_full 'Organic & Biomolecular Chemistry' _journal_paper_doi 10.1039/D2OB02101C _journal_year 2023 _chemical_formula_moiety 'C21 H20 N O4' _chemical_formula_sum 'C21 H20 N O4' _chemical_formula_weight 350.38 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _audit_creation_date 2022-07-29 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408) ; _audit_update_record ; 2022-12-12 deposited with the CCDC. 2023-01-27 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 104.29(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 6.8730(14) _cell_length_b 20.799(4) _cell_length_c 12.761(3) _cell_measurement_reflns_used 561 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 32.208 _cell_measurement_theta_min 25.244 _cell_volume 1767.8(7) _computing_cell_refinement 'XDS (Kabsch, 1993)' _computing_data_collection 'AS QEGUI' _computing_data_reduction 'XDS (Kabsch, 1993)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2019/2 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.991 _diffrn_measured_fraction_theta_max 0.837 _diffrn_measurement_device_type 'Dectris Eiger 16M' _diffrn_measurement_method 'Phi Scan' _diffrn_radiation_monochromator 'Silicon Double Crystal' _diffrn_radiation_type Synchrotron _diffrn_radiation_wavelength 0.7108 _diffrn_reflns_av_R_equivalents 0.0312 _diffrn_reflns_av_unetI/netI 0.0173 _diffrn_reflns_Laue_measured_fraction_full 0.991 _diffrn_reflns_Laue_measured_fraction_max 0.837 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_k_min -29 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 31161 _diffrn_reflns_point_group_measured_fraction_full 0.991 _diffrn_reflns_point_group_measured_fraction_max 0.837 _diffrn_reflns_theta_full 25.244 _diffrn_reflns_theta_max 32.208 _diffrn_reflns_theta_min 3.059 _diffrn_source 'MX2 Beamline Australian Synchrotron' _exptl_absorpt_coefficient_mu 0.091 _exptl_absorpt_correction_T_max 'Value not reported by XDS' _exptl_absorpt_correction_T_min 'Value not reported by XDS' _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'XDS (Kabsch, 1993)' _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.316 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 740 _exptl_crystal_size_max 0.1 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.748 _refine_diff_density_min -0.260 _refine_diff_density_rms 0.054 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.138 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 240 _refine_ls_number_reflns 5232 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.138 _refine_ls_R_factor_all 0.0688 _refine_ls_R_factor_gt 0.0649 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1216P)^2^+0.2334P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1968 _refine_ls_wR_factor_ref 0.2021 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4565 _reflns_number_total 5232 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d2ob02101c2.cif _cod_data_source_block 7 _cod_database_code 7159122 _shelx_shelxl_version_number 2019/2 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.991 _shelx_estimated_absorpt_t_min 0.991 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2.a Aromatic/amide H refined with riding coordinates: C14(H14), C2(H2), C17(H17), C16(H16), C8(H8), C7(H7), C6(H6) 2.b Idealised Me refined as rotating group: C21(H21A,H21B,H21C), C19(H19A,H19B,H19C), C18(H18A,H18B,H18C), C20(H20A,H20B, H20C) 2.c Idealised tetrahedral OH refined as rotating group: O3(H3) ; _shelx_res_file ; TITL p21_c_a.res in P2(1)/c p21_c.res created by SHELXL-2019/2 at 10:12:19 on 29-Jul-2022 REM Old TITL P21_c in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.215, Rweak 0.003, Alpha 0.026 REM 0.799 for 118 systematic absences, Orientation as input REM Formula found by SHELXT: C22 O4 CELL 0.7108 6.873 20.799 12.761 90 104.286 90 ZERR 4 0.0014 0.0042 0.0026 0 0.03 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N O UNIT 84 80 4 16 L.S. 4 PLAN 5 SIZE 0.1 0.1 0.1 TEMP -173(2) CONF BOND list 4 MORE -1 BOND $H fmap 2 acta REM REM REM WGHT 0.121600 0.233400 FVAR 1.03758 O1 4 0.249530 0.475960 0.414622 11.00000 0.06928 0.03106 = 0.02736 0.00247 0.01740 0.00036 O3 4 0.225916 0.483562 0.787345 11.00000 0.07811 0.04488 = 0.02891 0.00250 0.02011 0.00007 AFIX 147 H3 2 0.238743 0.522936 0.776018 11.00000 -1.50000 AFIX 0 O2 4 0.273004 0.586170 0.681807 11.00000 0.08856 0.03988 = 0.02733 -0.00149 0.02062 -0.00285 O4 4 0.272603 0.751579 -0.043867 11.00000 0.12593 0.03717 = 0.03281 0.00889 0.03040 0.00328 N1 3 0.275023 0.705606 0.022668 11.00000 0.09821 0.03293 = 0.02679 0.00295 0.02416 0.00237 C15 1 0.272175 0.563215 0.301495 11.00000 0.06175 0.03364 = 0.02556 0.00226 0.01520 0.00128 C1 1 0.266555 0.541048 0.410247 11.00000 0.05994 0.03182 = 0.02729 0.00210 0.01422 0.00049 C14 1 0.278722 0.629088 0.280594 11.00000 0.06809 0.03267 = 0.02489 0.00019 0.01688 0.00151 AFIX 43 H14 2 0.283444 0.659624 0.336529 11.00000 -1.20000 AFIX 0 C3 1 0.264094 0.552305 0.599722 11.00000 0.06468 0.03645 = 0.02681 0.00183 0.01542 -0.00003 C2 1 0.275445 0.579048 0.497523 11.00000 0.06680 0.03347 = 0.02678 0.00135 0.01598 -0.00151 AFIX 43 H2 2 0.289443 0.624215 0.491068 11.00000 -1.20000 AFIX 0 C9 1 0.236605 0.446801 0.509245 11.00000 0.06177 0.03474 = 0.02942 0.00412 0.01597 0.00072 C17 1 0.265121 0.539377 0.114451 11.00000 0.07413 0.03367 = 0.02739 -0.00113 0.01820 0.00133 AFIX 43 H17 2 0.260661 0.509155 0.058089 11.00000 -1.20000 AFIX 0 C10 1 0.279455 0.717257 0.138088 11.00000 0.08144 0.03188 = 0.02553 0.00319 0.01997 0.00367 C16 1 0.266108 0.518725 0.218343 11.00000 0.06836 0.03211 = 0.02921 0.00057 0.01732 0.00079 AFIX 43 H16 2 0.262633 0.474014 0.232996 11.00000 -1.20000 AFIX 0 C11 1 0.278204 0.649083 0.176831 11.00000 0.06878 0.03251 = 0.02602 0.00158 0.01788 0.00276 C13 1 0.269411 0.637272 -0.010880 11.00000 0.08349 0.03446 = 0.02519 0.00094 0.02082 0.00273 C5 1 0.223513 0.450266 0.696647 11.00000 0.06233 0.04196 = 0.02959 0.00565 0.01654 0.00168 C4 1 0.240628 0.483052 0.602043 11.00000 0.06066 0.03551 = 0.02756 0.00350 0.01494 0.00095 C8 1 0.219167 0.380577 0.507214 11.00000 0.06943 0.03340 = 0.03470 0.00247 0.01678 0.00082 AFIX 43 H8 2 0.220392 0.356730 0.443887 11.00000 -1.20000 AFIX 0 C21 1 0.456203 0.621209 -0.050983 11.00000 0.08635 0.04564 = 0.03373 0.00067 0.02736 0.00076 AFIX 137 H21A 2 0.454279 0.646107 -0.116431 11.00000 -1.50000 H21B 2 0.456906 0.575197 -0.067422 11.00000 -1.50000 H21C 2 0.576941 0.632047 0.005244 11.00000 -1.50000 AFIX 0 C19 1 0.467300 0.754764 0.192770 11.00000 0.08643 0.03378 = 0.03885 0.00362 0.01707 -0.00154 AFIX 137 H19A 2 0.586046 0.732610 0.181117 11.00000 -1.50000 H19B 2 0.476790 0.757730 0.270515 11.00000 -1.50000 H19C 2 0.459985 0.798095 0.161877 11.00000 -1.50000 AFIX 0 C12 1 0.270750 0.604728 0.094660 11.00000 0.07086 0.03366 = 0.02557 0.00137 0.01760 0.00288 C7 1 0.199747 0.350036 0.601179 11.00000 0.07040 0.03600 = 0.04044 0.00699 0.01769 0.00029 AFIX 43 H7 2 0.185097 0.304617 0.601156 11.00000 -1.20000 AFIX 0 C6 1 0.201199 0.384184 0.695116 11.00000 0.06584 0.04046 = 0.03515 0.00982 0.01658 0.00184 AFIX 43 H6 2 0.186903 0.362163 0.758010 11.00000 -1.20000 AFIX 0 C18 1 0.091016 0.753840 0.146423 11.00000 0.08650 0.03879 = 0.04040 0.00515 0.02361 0.01066 AFIX 137 H18A 2 0.093306 0.797074 0.116220 11.00000 -1.50000 H18B 2 0.087241 0.757087 0.222509 11.00000 -1.50000 H18C 2 -0.028336 0.730817 0.105882 11.00000 -1.50000 AFIX 0 C20 1 0.076601 0.623895 -0.097772 11.00000 0.08640 0.04602 = 0.02947 0.00229 0.01567 0.00366 AFIX 137 H20A 2 -0.039516 0.637612 -0.071675 11.00000 -1.50000 H20B 2 0.066439 0.577749 -0.113707 11.00000 -1.50000 H20C 2 0.079299 0.647748 -0.163627 11.00000 -1.50000 AFIX 0 HKLF 4 REM p21_c_a.res in P2(1)/c REM wR2 = 0.2021, GooF = S = 1.138, Restrained GooF = 1.138 for all data REM R1 = 0.0649 for 4565 Fo > 4sig(Fo) and 0.0688 for all 5232 data REM 240 parameters refined using 0 restraints END WGHT 0.1218 0.2307 REM Highest difference peak 0.748, deepest hole -0.260, 1-sigma level 0.054 Q1 1 0.2661 0.3482 0.4035 11.00000 0.05 0.75 Q2 1 0.2682 0.5596 0.4576 11.00000 0.05 0.36 Q3 1 0.2352 0.4648 0.5564 11.00000 0.05 0.35 Q4 1 0.2726 0.6249 0.1372 11.00000 0.05 0.35 Q5 1 0.2737 0.6399 0.2214 11.00000 0.05 0.33 ; _shelx_res_checksum 9610 _shelx_hkl_file ; 0 -1 0 1.31 0.08 0 -1 0 1.31 0.08 0 -3 0 0.00 0.15 0 -3 0 -0.08 0.15 0 3 0 0.00 0.15 0 3 0 0.00 0.15 0 -4 0 422.87 12.42 0 -4 0 406.52 11.96 0 4 0 418.71 12.27 0 4 0 418.55 12.27 0 -5 0 0.62 0.23 0 -5 0 -0.08 0.23 0 5 0 0.08 0.23 0 5 0 0.54 0.23 0 -6 0 2782.13 81.09 0 6 0 2875.48 83.79 0 7 0 0.46 0.23 0 7 0 0.77 0.23 0 -9 0 0.08 0.23 0 -9 0 0.46 0.23 0 9 0 0.54 0.23 0 9 0 0.23 0.31 0 -10 0 4227.20 123.21 0 -10 0 4356.05 126.92 0 10 0 4331.36 126.22 0 10 0 4193.25 122.29 0 -11 0 0.15 0.23 0 -11 0 0.46 0.31 0 11 0 -0.23 0.31 0 11 0 -0.15 0.23 0 -12 0 1658.01 48.53 0 -12 0 1685.02 49.38 0 12 0 1847.81 54.16 0 12 0 1687.33 49.30 0 -13 0 0.39 0.31 0 -13 0 0.15 0.23 0 13 0 0.00 0.23 0 13 0 0.15 0.39 0 -14 0 86.10 2.78 0 -14 0 84.64 2.85 0 14 0 91.43 3.09 0 14 0 89.42 2.93 0 -15 0 0.08 0.31 0 -15 0 0.15 0.31 0 15 0 -0.31 0.23 0 15 0 -0.39 0.39 0 -16 0 222.28 6.79 0 16 0 227.21 6.94 0 -17 0 0.23 0.31 0 -17 0 0.00 0.39 0 17 0 0.15 0.31 0 17 0 0.08 0.46 0 -18 0 691.52 20.68 0 -18 0 669.69 19.91 0 18 0 668.30 19.83 0 18 0 637.67 19.13 0 -19 0 0.08 0.46 0 19 0 -0.54 0.46 0 -20 0 19.52 1.08 0 -20 0 20.14 1.23 0 -21 0 0.00 0.46 0 -21 0 -0.77 0.46 0 21 0 -0.39 0.54 0 21 0 -0.31 0.46 0 -22 0 318.64 9.95 0 -22 0 347.50 10.65 0 22 0 348.34 10.65 0 22 0 327.90 10.34 0 -23 0 -0.15 0.39 0 -23 0 0.15 0.46 0 23 0 -0.39 0.54 0 23 0 0.08 0.46 0 -24 0 83.56 3.01 0 -24 0 76.92 2.93 0 -25 0 -0.15 0.46 0 -25 0 0.39 0.39 0 25 0 -0.54 0.46 0 25 0 0.85 0.62 0 -26 0 120.74 4.32 0 -26 0 133.47 4.55 0 -27 0 -0.08 0.46 0 -27 0 0.69 0.54 0 27 0 -0.08 0.62 0 27 0 0.54 0.46 0 -28 0 15.28 1.23 0 -28 -1 32.25 1.77 0 -28 -1 27.08 1.62 0 27 1 23.69 1.47 0 -27 -1 20.68 1.31 0 -27 -1 15.89 1.47 0 26 1 38.04 1.85 0 26 1 33.87 2.01 0 25 1 17.44 1.39 0 25 1 20.52 1.31 0 24 1 31.94 1.62 0 24 1 26.39 1.62 0 -24 -1 28.24 1.54 0 -24 -1 28.39 1.47 0 23 1 39.27 1.93 0 23 1 40.27 1.85 0 -23 -1 42.36 1.85 0 -23 -1 38.11 1.77 0 22 1 45.60 1.93 0 22 1 44.67 2.08 0 -22 -1 50.38 2.16 0 -22 -1 51.00 2.08 0 21 1 7.33 0.77 0 21 1 7.33 0.85 0 -21 -1 8.49 0.85 0 -21 -1 9.10 0.85 0 20 1 350.58 10.96 0 20 1 360.69 10.96 0 -20 -1 378.28 11.50 0 -20 -1 352.28 10.88 0 19 1 52.16 2.01 0 19 1 48.30 2.08 0 -19 -1 46.60 1.93 0 -19 -1 53.24 2.01 0 18 1 6.02 0.62 0 18 1 7.10 0.77 0 -18 -1 6.25 0.69 0 -18 -1 6.48 0.62 0 17 1 63.65 2.47 0 -17 -1 62.11 2.31 0 16 1 29.16 1.39 0 16 1 27.70 1.23 0 -16 -1 25.92 1.23 0 -16 -1 28.47 1.23 0 15 1 182.08 5.79 0 15 1 181.31 5.63 0 -15 -1 180.69 5.63 0 -15 -1 183.08 5.79 0 14 1 48.84 1.77 0 -14 -1 50.46 1.77 0 13 1 56.40 1.93 0 13 1 52.62 2.01 0 -13 -1 57.09 2.01 0 12 1 3.24 0.39 0 12 1 3.63 0.46 0 -12 -1 3.63 0.46 0 -12 -1 2.78 0.39 0 11 1 1.23 0.39 0 11 1 2.08 0.31 0 -11 -1 1.23 0.31 0 -11 -1 1.54 0.39 0 10 1 2666.40 77.85 0 10 1 2623.97 76.61 0 -10 -1 2620.88 76.54 0 -10 -1 2638.62 77.00 0 9 1 3542.08 103.31 0 9 1 3425.58 99.84 0 -9 -1 3400.89 99.22 0 -9 -1 3392.41 98.91 0 8 1 3538.23 103.15 0 8 1 3809.03 111.10 0 -8 -1 3409.38 99.37 0 -8 -1 3599.18 104.93 0 7 1 875.68 25.69 0 7 1 865.65 25.38 0 -7 -1 839.42 24.61 0 -7 -1 892.66 26.15 0 6 1 896.52 26.31 0 6 1 901.92 26.39 0 -6 -1 884.17 25.92 0 -6 -1 947.44 27.77 0 5 1 67.20 2.16 0 5 1 66.35 2.16 0 -5 -1 66.20 2.08 0 -5 -1 69.67 2.24 0 4 1 368.48 10.88 0 4 1 355.98 10.49 0 -4 -1 352.28 10.42 0 -4 -1 380.36 11.19 0 0 1 0.15 0.08 0 0 -1 0.15 0.08 0 -4 1 320.72 9.41 0 4 -1 320.26 9.41 0 -5 1 71.91 2.16 0 -5 1 64.81 2.01 0 5 -1 59.79 1.85 0 5 -1 65.89 2.01 0 -6 1 891.11 26.00 0 -6 1 809.33 23.69 0 -7 1 774.61 22.68 0 -7 1 837.88 24.53 0 -8 1 3526.65 102.77 0 -8 1 3456.44 100.76 0 8 -1 3668.61 106.93 0 8 -1 3400.12 99.14 0 -9 1 3446.41 100.45 0 -9 1 3268.96 95.28 0 9 -1 3278.99 95.67 0 9 -1 3431.76 99.99 0 -10 1 2492.81 72.76 0 -10 1 2729.67 79.62 0 10 -1 2630.91 76.69 0 10 -1 2523.67 73.68 0 -11 1 1.39 0.31 0 -11 1 1.85 0.31 0 11 -1 1.00 0.23 0 11 -1 0.77 0.31 0 -12 1 3.32 0.31 0 -12 1 3.39 0.39 0 12 -1 3.16 0.46 0 12 -1 3.63 0.31 0 -13 1 55.70 1.85 0 -13 1 55.63 1.93 0 13 -1 55.09 2.01 0 13 -1 55.47 1.85 0 -14 1 47.45 1.62 0 -14 1 52.00 1.85 0 14 -1 48.76 1.70 0 14 -1 50.54 1.85 0 -15 1 180.07 5.56 0 -15 1 179.77 5.63 0 15 -1 176.68 5.56 0 15 -1 173.21 5.32 0 -16 1 30.01 1.31 0 -16 1 29.09 1.16 0 16 -1 29.09 1.16 0 16 -1 30.40 1.39 0 -17 1 59.41 2.08 0 -17 1 65.73 2.39 0 17 -1 57.79 2.01 0 17 -1 57.25 2.24 0 -18 1 6.40 0.54 0 18 -1 6.79 0.54 0 -19 1 49.76 1.85 0 19 -1 47.99 1.77 0 -20 1 343.02 10.57 0 -20 1 374.96 11.34 0 20 -1 350.43 10.57 0 20 -1 350.12 10.88 0 -21 1 7.41 0.69 0 -21 1 7.72 0.77 0 21 -1 7.10 0.85 0 21 -1 6.94 0.62 0 -22 1 47.45 2.01 0 22 -1 46.91 2.08 0 -23 1 41.05 1.85 0 -23 1 39.73 1.70 0 23 -1 40.20 1.93 0 -24 1 30.86 1.47 0 -24 1 27.77 1.47 0 -25 1 17.82 1.08 0 -25 1 16.43 1.16 0 26 -1 30.55 1.77 0 28 2 9.88 1.08 0 28 2 7.10 1.08 0 26 2 9.34 1.08 0 -26 -2 8.18 0.93 0 25 2 0.08 0.54 0 25 2 0.85 0.62 0 -25 -2 0.00 0.46 0 -25 -2 0.23 0.46 0 24 2 100.45 3.63 0 -24 -2 97.52 3.55 0 23 2 2.31 0.69 0 23 2 2.47 0.62 0 -23 -2 2.31 0.62 0 -23 -2 1.62 0.54 0 22 2 2.08 0.62 0 22 2 1.23 0.62 0 -22 -2 1.00 0.54 0 -22 -2 1.54 0.54 0 21 2 10.18 1.00 0 21 2 9.49 0.85 0 -21 -2 10.26 0.85 0 -21 -2 10.65 0.93 0 20 2 10.34 1.00 0 20 2 8.72 0.77 0 -20 -2 9.72 0.85 0 -20 -2 10.49 0.85 0 19 2 122.13 4.24 0 19 2 127.30 4.24 0 -19 -2 122.60 4.17 0 -19 -2 130.16 4.32 0 18 2 0.93 0.54 0 18 2 1.62 0.39 0 -18 -2 1.00 0.46 0 -18 -2 0.62 0.39 0 17 2 61.88 2.39 0 17 2 62.96 2.31 0 -17 -2 64.89 2.31 0 -17 -2 64.11 2.39 0 16 2 53.47 2.01 0 16 2 51.15 2.08 0 -16 -2 54.86 2.08 0 -16 -2 52.62 2.01 0 15 2 703.94 20.99 0 -15 -2 737.50 21.91 0 -14 -2 3.16 0.46 0 13 2 1026.90 30.32 0 13 2 1021.50 30.09 0 -13 -2 1005.30 29.63 0 -13 -2 1047.73 30.86 0 12 2 986.78 29.01 0 -12 -2 1027.67 30.32 0 -12 -2 939.72 27.70 0 11 2 180.07 5.56 0 -11 -2 177.68 5.48 0 10 2 7.18 0.54 0 10 2 8.18 0.62 0 -10 -2 8.49 0.54 0 -10 -2 7.95 0.54 0 9 2 171.12 5.32 0 9 2 169.04 5.17 0 -9 -2 172.51 5.32 0 -9 -2 163.26 5.01 0 8 2 41.20 1.47 0 8 2 42.82 1.54 0 -8 -2 43.59 1.54 0 -8 -2 42.36 1.54 0 7 2 96.60 3.09 0 7 2 101.22 3.16 0 -7 -2 95.90 3.01 0 -7 -2 96.83 3.09 0 6 2 294.80 8.80 0 6 2 280.22 8.41 0 -6 -2 287.78 8.64 0 -6 -2 290.40 8.72 0 4 2 1905.67 55.63 0 4 2 1972.80 57.56 0 -4 -2 1916.47 55.94 0 -4 -2 1947.34 56.78 0 3 2 2618.57 76.30 0 2 2 960.55 28.08 0 2 2 934.32 27.31 0 -2 -2 988.33 28.86 0 -2 -2 1004.53 29.40 0 1 2 818.59 23.92 0 1 2 888.03 25.92 0 -1 -2 820.13 23.99 0 -1 -2 837.11 24.46 0 0 2 1491.36 43.51 0 0 2 1408.04 41.05 0 0 -2 1467.45 42.74 0 0 -2 1487.51 43.36 0 -1 2 840.19 24.53 0 -1 2 821.68 23.99 0 1 -2 817.05 23.84 0 1 -2 824.76 24.07 0 -2 2 1028.45 30.01 0 -2 2 952.07 27.77 0 2 -2 999.90 29.16 0 2 -2 968.27 28.24 0 3 -2 2816.08 82.09 0 -4 2 1833.15 53.47 0 4 -2 1897.96 55.40 0 -6 2 249.43 7.33 0 6 -2 249.05 7.33 0 7 -2 98.22 2.93 0 7 -2 96.75 2.93 0 -8 2 40.04 1.31 0 -8 2 40.66 1.31 0 8 -2 39.97 1.31 0 8 -2 42.67 1.31 0 -9 2 167.11 5.01 0 -9 2 152.45 4.63 0 -10 2 8.18 0.39 0 -10 2 8.56 0.46 0 10 -2 7.87 0.39 0 10 -2 8.80 0.54 0 -11 2 167.42 5.09 0 -11 2 177.91 5.32 0 11 -2 175.75 5.25 0 11 -2 172.75 5.25 0 -12 2 946.66 27.70 0 -12 2 945.89 27.77 0 12 -2 972.90 28.47 0 12 -2 924.29 27.16 0 -13 2 977.53 28.62 0 -13 2 942.81 27.70 0 13 -2 992.18 29.09 0 13 -2 956.69 28.16 0 -14 2 3.39 0.46 0 -14 2 2.70 0.31 0 14 -2 3.09 0.31 0 14 -2 4.40 0.54 0 -15 2 698.93 20.68 0 -15 2 706.18 20.75 0 15 -2 705.33 20.75 0 15 -2 675.40 20.06 0 -16 2 52.00 1.77 0 -16 2 49.61 1.85 0 16 -2 52.62 2.01 0 16 -2 53.54 1.77 0 -17 2 64.27 2.16 0 -17 2 71.21 2.47 0 17 -2 70.83 2.62 0 17 -2 64.65 2.16 0 -18 2 0.93 0.46 0 -18 2 1.08 0.31 0 18 -2 0.85 0.31 0 18 -2 0.62 0.54 0 -19 2 126.38 4.01 0 -19 2 117.27 3.93 0 19 -2 125.45 3.93 0 19 -2 117.04 4.01 0 -20 2 8.41 0.62 0 -20 2 9.34 0.85 0 20 -2 9.64 0.93 0 20 -2 10.57 0.69 0 -21 2 8.72 0.62 0 -21 2 8.56 0.77 0 21 -2 9.80 0.93 0 21 -2 9.95 0.69 0 -22 2 1.23 0.39 0 22 -2 1.39 0.39 0 22 -2 0.85 0.62 0 -23 2 2.85 0.46 0 23 -2 2.55 0.46 0 -24 2 101.38 3.39 0 -25 2 -0.54 0.39 0 29 3 38.88 2.08 0 29 3 35.64 2.31 0 28 3 19.52 1.62 0 28 3 22.76 1.54 0 -28 -3 22.61 1.54 0 -28 -3 19.98 1.39 0 -27 -3 80.78 3.24 0 -27 -3 92.51 3.55 0 26 3 10.42 1.16 0 26 3 11.42 1.08 0 -26 -3 9.80 1.00 0 -26 -3 10.96 0.93 0 25 3 9.95 1.00 0 25 3 7.95 1.00 0 -25 -3 9.26 0.93 0 -25 -3 8.56 0.93 0 24 3 15.66 1.31 0 -24 -3 15.89 1.16 0 23 3 1.70 0.62 0 23 3 1.23 0.62 0 -23 -3 0.77 0.54 0 -23 -3 2.31 0.62 0 21 3 59.72 2.55 0 21 3 57.94 2.31 0 -21 -3 65.19 2.55 0 -21 -3 64.89 2.55 0 20 3 94.82 3.32 0 20 3 92.58 3.47 0 -20 -3 88.88 3.24 0 -20 -3 98.68 3.47 0 19 3 4.55 0.62 0 19 3 4.94 0.69 0 -19 -3 5.17 0.69 0 -19 -3 4.17 0.62 0 18 3 1085.54 32.25 0 18 3 1087.85 32.17 0 -18 -3 1094.03 32.33 0 -18 -3 1087.85 32.25 0 17 3 3.93 0.62 0 17 3 4.78 0.54 0 -17 -3 5.56 0.62 0 -17 -3 4.09 0.62 0 16 3 190.26 6.02 0 16 3 181.85 5.86 0 -16 -3 198.36 6.33 0 -16 -3 189.80 6.02 0 15 3 195.97 6.25 0 15 3 201.91 6.33 0 -15 -3 204.38 6.48 0 -15 -3 198.82 6.25 0 14 3 218.11 6.87 0 14 3 211.86 6.56 0 -14 -3 220.43 6.87 0 -14 -3 224.13 7.02 0 13 3 71.21 2.55 0 13 3 64.96 2.31 0 -13 -3 62.73 2.24 0 -13 -3 69.13 2.47 0 12 3 24.92 1.16 0 -12 -3 24.15 1.08 0 11 3 0.85 0.39 0 11 3 0.69 0.31 0 -11 -3 0.46 0.39 0 -11 -3 0.54 0.31 0 10 3 772.30 22.84 0 10 3 764.20 22.61 0 -10 -3 746.38 22.07 0 -10 -3 766.98 22.68 0 9 3 0.39 0.23 0 -9 -3 0.46 0.31 0 8 3 1484.42 43.51 0 8 3 1485.96 43.51 0 -8 -3 1495.22 43.82 0 -8 -3 1467.45 42.97 0 7 3 534.82 15.82 0 7 3 511.37 15.20 0 -7 -3 534.13 15.82 0 -7 -3 528.65 15.66 0 6 3 1048.51 30.78 0 6 3 1079.37 31.63 0 -6 -3 1073.97 31.48 0 -6 -3 1060.85 31.09 0 5 3 772.30 22.76 0 5 3 771.30 22.68 0 -5 -3 766.28 22.53 0 -5 -3 780.79 22.99 0 4 3 1234.44 36.18 0 4 3 1206.67 35.34 0 -4 -3 1215.16 35.57 0 -4 -3 1188.92 34.80 0 3 3 1624.07 47.45 0 3 3 1688.10 49.30 0 -3 -3 1698.90 49.61 0 -3 -3 1664.19 48.61 0 2 3 1810.78 52.85 0 2 3 1840.87 53.70 0 -2 -3 1825.43 53.31 0 -2 -3 1826.21 53.31 0 1 3 60.87 1.93 0 1 3 62.42 2.01 0 -1 -3 64.11 2.08 0 -1 -3 64.04 2.08 0 0 -3 0.54 0.31 0 0 -3 0.46 0.23 0 -1 3 62.19 1.93 0 -1 3 61.34 1.93 0 1 -3 63.11 2.01 0 1 -3 65.12 2.08 0 -2 3 1850.90 53.93 0 -2 3 1861.70 54.32 0 2 -3 1801.52 52.54 0 2 -3 1773.74 51.69 0 -3 3 1662.64 48.45 0 -3 3 1583.17 46.21 0 3 -3 1659.56 48.37 0 3 -3 1659.56 48.37 0 -4 3 1095.57 32.02 0 -4 3 1215.93 35.49 0 4 -3 1205.90 35.18 0 4 -3 1172.72 34.26 0 -6 3 1075.51 31.48 0 -6 3 1080.91 31.63 0 6 -3 1078.60 31.56 0 -7 3 489.92 14.35 0 7 -3 518.70 15.20 0 -8 3 1361.75 39.89 0 -8 3 1425.78 41.74 0 8 -3 1425.01 41.74 0 -9 3 0.39 0.15 0 -9 3 0.15 0.15 0 9 -3 0.39 0.15 0 9 -3 0.39 0.23 0 -10 3 751.70 21.99 0 -10 3 725.31 21.29 0 10 -3 734.96 21.60 0 10 -3 811.65 23.76 0 -11 3 0.39 0.23 0 -11 3 0.31 0.15 0 11 -3 0.23 0.15 0 11 -3 0.54 0.23 0 -12 3 22.61 0.77 0 -12 3 20.83 0.85 0 12 -3 21.45 0.85 0 12 -3 21.91 0.77 0 -13 3 64.81 2.01 0 -13 3 63.42 2.08 0 13 -3 68.05 2.08 0 13 -3 60.87 2.01 0 -14 3 211.78 6.33 0 -14 3 195.43 5.94 0 14 -3 214.48 6.40 0 14 -3 208.39 6.33 0 -15 3 196.20 5.86 0 -15 3 194.27 5.94 0 15 -3 196.35 5.86 0 15 -3 183.78 5.63 0 -16 3 190.10 5.71 0 -16 3 173.90 5.40 0 16 -3 186.40 5.63 0 16 -3 191.80 5.94 0 -17 3 4.86 0.54 0 -17 3 4.86 0.39 0 17 -3 4.47 0.39 0 17 -3 4.32 0.54 0 -18 3 1018.42 30.01 0 -18 3 1037.70 30.48 0 -19 3 4.55 0.39 0 -19 3 4.32 0.54 0 19 -3 4.40 0.54 0 19 -3 4.78 0.39 0 -20 3 83.32 2.85 0 -20 3 84.25 2.70 0 -21 3 58.40 2.01 0 -21 3 57.63 2.08 0 21 -3 53.78 2.01 0 21 -3 58.64 1.93 0 -22 3 0.77 0.31 0 -22 3 0.85 0.39 0 22 -3 1.08 0.31 0 22 -3 1.16 0.46 0 -23 3 1.47 0.31 0 29 4 69.21 3.39 0 -29 -4 72.83 3.01 0 28 4 42.51 2.16 0 27 4 13.81 1.31 0 27 4 16.67 1.31 0 -27 -4 15.43 1.23 0 -27 -4 15.35 1.16 0 26 4 18.05 1.47 0 26 4 22.76 1.47 0 25 4 39.73 2.01 0 25 4 41.74 2.16 0 -25 -4 38.65 1.93 0 -25 -4 39.12 1.85 0 24 4 29.01 1.62 0 24 4 26.85 1.70 0 -24 -4 25.54 1.47 0 -24 -4 27.00 1.54 0 23 4 15.43 1.23 0 23 4 15.28 1.16 0 -23 -4 15.35 1.16 0 -23 -4 15.35 1.16 0 22 4 8.87 0.93 0 -22 -4 7.18 0.77 0 21 4 1.47 0.62 0 21 4 1.54 0.62 0 -21 -4 1.54 0.62 0 -21 -4 1.62 0.54 0 20 4 72.68 2.78 0 -20 -4 79.00 2.93 0 19 4 220.27 7.18 0 19 4 227.83 7.18 0 -19 -4 222.05 7.10 0 -19 -4 225.13 7.10 0 18 4 33.10 1.62 0 18 4 32.56 1.54 0 -18 -4 35.26 1.62 0 -18 -4 36.11 1.70 0 17 4 599.32 18.13 0 17 4 615.76 18.44 0 -17 -4 630.65 18.98 0 -17 -4 635.35 18.98 0 16 4 901.14 26.85 0 16 4 900.37 26.69 0 -16 -4 901.14 26.77 0 -16 -4 930.46 27.54 0 15 4 233.93 7.25 0 15 4 245.19 7.72 0 -15 -4 236.55 7.41 0 -15 -4 246.81 7.64 0 14 4 250.21 7.72 0 14 4 257.30 8.02 0 -14 -4 241.18 7.48 0 -14 -4 251.13 7.79 0 13 4 1334.74 39.35 0 13 4 1298.48 38.19 0 -13 -4 1320.86 38.88 0 -13 -4 1265.31 37.26 0 12 4 0.15 0.31 0 12 4 0.00 0.39 0 -12 -4 0.31 0.31 0 -12 -4 -0.15 0.31 0 11 4 688.90 20.52 0 11 4 648.01 19.21 0 -11 -4 656.49 19.52 0 -11 -4 684.11 20.29 0 10 4 156.00 4.94 0 -10 -4 156.93 4.94 0 9 4 2031.43 59.48 0 9 4 1942.71 56.94 0 -9 -4 1995.94 58.40 0 -9 -4 1914.16 56.09 0 8 4 182.08 5.71 0 8 4 188.56 5.79 0 -8 -4 188.56 5.86 0 -8 -4 193.27 5.94 0 7 4 1880.21 55.01 0 -7 -4 1854.75 54.24 0 6 4 172.82 5.40 0 6 4 178.07 5.48 0 -6 -4 179.61 5.56 0 -6 -4 174.44 5.40 0 5 4 117.81 3.70 0 5 4 115.19 3.70 0 4 4 853.31 25.07 0 4 4 835.56 24.61 0 -4 -4 834.79 24.53 0 -4 -4 831.71 24.46 0 3 4 1516.05 44.36 0 3 4 1552.31 45.44 0 -3 -4 1534.57 44.90 0 -3 -4 1510.65 44.21 0 2 4 0.31 0.23 0 2 4 0.93 0.31 0 -2 -4 0.23 0.23 0 -2 -4 0.39 0.31 0 1 4 4315.93 125.76 0 1 4 4448.63 129.62 0 -1 -4 4430.88 129.08 0 -1 -4 4403.88 128.31 0 0 4 33.10 1.16 0 0 4 31.63 1.16 0 0 -4 32.33 1.16 0 0 -4 32.71 1.16 0 -1 4 4344.47 126.53 0 -1 4 4356.82 126.92 0 1 -4 4363.76 127.07 0 1 -4 4477.18 130.39 0 2 -4 0.23 0.23 0 2 -4 0.46 0.23 0 -3 4 1520.68 44.36 0 -3 4 1499.85 43.82 0 3 -4 1504.48 43.90 0 3 -4 1527.62 44.59 0 -4 4 822.45 24.07 0 -4 4 847.91 24.77 0 4 -4 844.82 24.69 0 4 -4 806.25 23.61 0 -5 4 106.86 3.24 0 -5 4 115.11 3.47 0 5 -4 115.11 3.47 0 5 -4 112.33 3.47 0 -6 4 161.33 4.86 0 -6 4 177.07 5.25 0 6 -4 177.07 5.25 0 6 -4 169.81 5.09 0 7 -4 1941.16 56.71 0 7 -4 1807.69 52.85 0 -8 4 188.56 5.56 0 -8 4 173.59 5.17 0 8 -4 194.89 5.79 0 8 -4 176.68 5.25 0 -9 4 1883.30 55.32 0 9 -4 1230.59 36.26 0 -10 4 144.51 4.32 0 -11 4 670.23 19.98 0 -12 4 0.15 0.08 0 -13 4 1212.07 36.34 0 -14 4 258.77 7.79 0 -15 4 243.73 7.33 0 -16 4 883.40 26.31 0 -17 4 583.35 17.51 0 -18 4 31.71 1.08 0 29 5 0.46 0.62 0 29 5 2.31 0.69 0 -29 -5 2.16 0.54 0 -29 -5 2.70 0.69 0 28 5 13.19 1.31 0 28 5 15.74 1.31 0 -28 -5 13.81 1.16 0 -28 -5 13.96 1.23 0 27 5 4.94 0.93 0 27 5 4.17 1.00 0 -27 -5 4.47 0.77 0 26 5 91.73 3.55 0 -26 -5 82.17 3.24 0 25 5 265.79 8.56 0 25 5 262.17 8.64 0 -25 -5 254.76 8.18 0 -25 -5 240.64 7.79 0 24 5 1.31 0.62 0 24 5 -0.08 0.62 0 -24 -5 0.54 0.54 0 -24 -5 0.00 0.54 0 23 5 216.57 7.48 0 22 5 19.44 1.31 0 22 5 23.84 1.47 0 -22 -5 21.76 1.31 0 -22 -5 22.61 1.39 0 21 5 1.93 0.62 0 21 5 2.01 0.62 0 -21 -5 1.70 0.62 0 -21 -5 2.16 0.54 0 20 5 4.71 0.77 0 -20 -5 5.32 0.69 0 19 5 0.46 0.54 0 19 5 1.00 0.54 0 -19 -5 0.69 0.46 0 -19 -5 0.69 0.54 0 18 5 5.32 0.69 0 -18 -5 4.17 0.62 0 17 5 1500.62 44.21 0 17 5 1563.12 46.14 0 -17 -5 1573.92 46.37 0 -17 -5 1575.46 46.45 0 16 5 8.87 0.77 0 16 5 9.18 0.85 0 -16 -5 8.18 0.77 0 -16 -5 9.18 0.77 0 15 5 7.48 0.77 0 15 5 8.33 0.69 0 -15 -5 8.72 0.77 0 -15 -5 8.95 0.77 0 14 5 10.26 0.85 0 14 5 10.88 0.77 0 -14 -5 12.19 0.85 0 -14 -5 11.50 0.85 0 13 5 142.81 4.71 0 13 5 134.86 4.40 0 -13 -5 129.46 4.24 0 -13 -5 136.41 4.47 0 12 5 125.53 4.09 0 12 5 129.54 4.32 0 -12 -5 126.07 4.09 0 -12 -5 132.39 4.32 0 11 5 0.08 0.39 0 11 5 0.15 0.31 0 -11 -5 0.39 0.39 0 -11 -5 0.31 0.31 0 10 5 151.07 4.78 0 10 5 146.90 4.71 0 -10 -5 152.38 4.86 0 -10 -5 145.66 4.63 0 9 5 78.31 2.70 0 9 5 79.39 2.78 0 -9 -5 78.31 2.70 0 -9 -5 83.94 2.85 0 8 5 266.87 8.18 0 -8 -5 277.52 8.49 0 7 5 5696.96 166.11 0 7 5 5811.15 169.35 0 -7 -5 5719.34 166.73 0 -7 -5 5592.03 163.02 0 6 5 144.28 4.55 0 6 5 148.29 4.71 0 -4 -5 133.71 4.24 0 -4 -5 121.13 3.86 0 3 5 2152.56 62.88 0 3 5 2151.02 62.88 0 -3 -5 2130.96 62.26 0 -3 -5 2123.24 62.03 0 2 5 11.57 0.62 0 2 5 10.72 0.62 0 -2 -5 10.96 0.62 0 -2 -5 11.88 0.62 0 1 5 176.53 5.40 0 1 5 178.45 5.48 0 -1 -5 175.83 5.40 0 -1 -5 186.40 5.71 0 0 5 0.39 0.31 0 0 5 1.08 0.31 0 0 -5 0.15 0.31 0 0 -5 0.00 0.23 0 -1 5 176.06 5.32 0 -1 5 180.00 5.48 0 1 -5 177.22 5.40 0 1 -5 183.01 5.56 0 -2 5 11.88 0.62 0 -2 5 11.50 0.62 0 2 -5 11.50 0.62 0 2 -5 11.42 0.54 0 -3 5 2108.59 61.57 0 -3 5 2084.67 60.87 0 3 -5 2120.93 61.95 0 3 -5 2095.47 61.18 0 -4 5 125.30 3.86 0 -4 5 139.03 4.24 0 4 -5 135.79 4.09 0 4 -5 138.03 4.24 0 -6 5 159.09 4.78 0 -6 5 156.23 4.78 0 6 -5 160.86 4.86 0 6 -5 161.71 4.86 0 -7 5 5470.90 159.47 0 -7 5 5402.24 157.55 0 7 -5 5619.81 163.80 0 7 -5 5625.21 164.03 0 -8 5 245.89 7.25 0 -8 5 243.11 7.25 0 8 -5 256.61 7.56 0 8 -5 251.06 7.48 0 -9 5 70.83 2.24 0 -9 5 75.15 2.24 0 9 -5 76.23 2.31 0 9 -5 76.61 2.31 0 -10 5 146.28 4.40 0 29 6 1.54 0.62 0 -29 -6 1.00 0.69 0 28 6 3.86 0.77 0 28 6 4.71 0.85 0 -28 -6 4.86 0.69 0 -28 -6 3.24 0.69 0 27 6 11.50 1.16 0 27 6 8.33 1.08 0 -27 -6 9.64 1.00 0 -27 -6 10.03 1.08 0 26 6 0.39 0.62 0 26 6 1.00 0.62 0 -26 -6 1.00 0.54 0 -26 -6 0.54 0.62 0 25 6 11.19 1.16 0 25 6 7.41 0.93 0 -25 -6 8.26 0.93 0 -25 -6 9.41 1.00 0 24 6 90.58 3.55 0 24 6 91.66 3.55 0 -24 -6 86.33 3.32 0 -24 -6 83.79 3.24 0 23 6 26.69 1.70 0 23 6 24.53 1.54 0 -23 -6 24.53 1.47 0 -23 -6 26.00 1.47 0 22 6 9.41 1.00 0 22 6 6.48 0.85 0 -22 -6 8.18 0.93 0 -22 -6 9.18 0.93 0 21 6 34.56 1.77 0 21 6 32.40 1.70 0 -21 -6 32.02 1.62 0 -21 -6 36.88 1.85 0 20 6 34.95 1.70 0 20 6 34.10 1.77 0 -20 -6 38.50 1.77 0 -20 -6 36.34 1.77 0 19 6 2.31 0.54 0 19 6 0.77 0.54 0 -19 -6 0.62 0.54 0 -19 -6 1.47 0.54 0 -18 -6 5.25 0.69 0 17 6 189.18 6.25 0 17 6 177.68 5.79 0 -17 -6 186.63 6.02 0 -17 -6 188.87 6.17 0 16 6 195.66 6.25 0 -16 -6 200.67 6.40 0 15 6 2486.63 72.99 0 15 6 2497.44 73.14 0 -15 -6 2416.43 70.83 0 -15 -6 2340.04 68.67 0 14 6 713.20 21.45 0 14 6 649.63 19.44 0 -14 -6 677.17 20.29 0 -14 -6 673.47 20.14 0 13 6 888.03 26.31 0 13 6 913.49 27.16 0 -13 -6 826.31 24.53 0 -13 -6 891.89 26.46 0 12 6 291.56 8.95 0 12 6 305.45 9.49 0 -12 -6 296.34 9.10 0 -12 -6 288.94 8.95 0 11 6 243.11 7.56 0 11 6 240.18 7.56 0 -11 -6 239.64 7.48 0 -11 -6 244.65 7.56 0 10 6 7.87 0.69 0 10 6 8.72 0.69 0 -10 -6 8.64 0.69 0 -10 -6 8.10 0.62 0 9 6 128.85 4.24 0 9 6 134.55 4.32 0 -9 -6 128.54 4.17 0 -9 -6 132.78 4.32 0 8 6 369.95 11.19 0 8 6 365.47 11.11 0 -8 -6 384.38 11.65 0 -8 -6 361.15 10.96 0 -7 -6 1025.36 30.24 0 -7 -6 1029.22 30.32 0 6 6 2451.92 71.75 0 -6 -6 2491.26 72.83 0 5 6 691.83 20.52 0 5 6 653.18 19.37 0 -5 -6 672.23 19.91 0 -5 -6 712.66 21.14 0 4 6 1158.83 34.02 0 4 6 1153.43 33.95 0 -4 -6 1154.21 33.95 0 -4 -6 1149.58 33.79 0 3 6 371.80 11.19 0 3 6 381.83 11.42 0 -3 -6 369.87 11.11 0 -3 -6 363.31 10.88 0 2 6 3307.54 96.52 0 -2 -6 3317.57 96.83 0 1 6 1348.63 39.58 0 1 6 1302.34 38.19 0 -1 -6 1323.17 38.81 0 -1 -6 1330.89 39.04 0 0 6 123.98 3.93 0 0 6 122.44 3.86 0 0 -6 130.00 4.09 0 0 -6 122.36 3.86 0 -1 6 1310.05 38.42 0 -1 6 1335.51 39.12 0 1 -6 1305.42 38.27 0 1 -6 1337.83 39.19 0 -2 6 3253.53 94.90 0 -2 6 3397.04 99.06 0 2 -6 3217.27 93.82 0 2 -6 3181.01 92.81 0 -3 6 378.90 11.26 0 -3 6 382.83 11.42 0 3 -6 369.41 11.03 0 3 -6 372.96 11.11 0 -4 6 1085.54 31.79 0 -4 6 1111.77 32.56 0 -5 6 694.61 20.45 0 -5 6 713.28 20.99 0 5 -6 695.84 20.45 0 5 -6 675.32 19.91 0 -6 6 2471.97 72.21 0 -6 6 2452.69 71.60 0 6 -6 2473.52 72.14 0 6 -6 2549.13 74.45 0 -7 6 1067.02 31.32 0 -7 6 1056.99 30.94 0 7 -6 1062.39 31.09 0 7 -6 999.90 29.40 0 -8 6 364.39 10.80 0 -8 6 352.28 10.49 0 8 -6 363.47 10.72 0 8 -6 349.73 10.42 0 -9 6 122.13 3.78 0 -9 6 131.62 3.93 0 9 -6 125.37 3.86 0 9 -6 128.77 3.86 0 -10 6 8.56 0.39 0 -10 6 8.18 0.46 0 10 -6 8.87 0.39 0 10 -6 9.57 0.46 0 28 7 2.78 0.69 0 -28 -7 2.39 0.77 0 27 7 2.39 0.77 0 27 7 3.01 0.69 0 -27 -7 1.77 0.69 0 -27 -7 2.24 0.62 0 26 7 0.15 0.62 0 26 7 0.85 0.62 0 -26 -7 1.00 0.54 0 -26 -7 0.93 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160.25 5.01 0 5 -7 157.31 4.78 0 -6 7 263.17 7.95 0 -6 7 267.18 8.10 0 6 -7 260.31 7.79 0 6 -7 255.84 7.79 0 -7 7 132.47 4.17 0 -7 7 141.50 4.32 0 7 -7 137.02 4.17 0 7 -7 141.81 4.47 0 -8 7 36.96 1.39 0 -8 7 38.11 1.31 0 8 -7 39.66 1.39 0 8 -7 36.65 1.47 0 -9 7 222.97 6.71 0 -9 7 219.65 6.71 0 9 -7 224.59 6.71 0 9 -7 216.72 6.56 0 -10 7 0.85 0.23 0 -10 7 1.00 0.31 0 10 -7 0.85 0.15 0 10 -7 1.23 0.31 0 11 -7 854.08 25.15 0 11 -7 820.91 24.23 0 26 8 1.54 0.62 0 -26 -8 0.69 0.54 0 25 8 1.31 0.69 0 25 8 2.47 0.69 0 -25 -8 1.70 0.54 0 -25 -8 1.77 0.69 0 -24 -8 8.18 0.85 0 -24 -8 6.79 0.93 0 23 8 31.09 1.77 0 23 8 30.17 1.70 0 -23 -8 31.56 1.62 0 -23 -8 29.94 1.70 0 22 8 51.15 2.39 0 -22 -8 51.31 2.24 0 21 8 37.73 1.93 0 -21 -8 37.96 1.93 0 20 8 19.75 1.39 0 20 8 19.83 1.31 0 -20 -8 22.07 1.39 0 -20 -8 22.07 1.31 0 19 8 22.76 1.39 0 19 8 25.46 1.47 0 -19 -8 26.31 1.47 0 -19 -8 27.16 1.54 0 18 8 7.18 0.85 0 18 8 7.64 0.93 0 -18 -8 7.56 0.93 0 -18 -8 7.87 0.77 0 17 8 22.37 1.39 0 17 8 26.62 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24 -3 29.09 1.62 -1 -25 3 12.81 1.00 1 25 -3 15.97 1.23 -1 -26 3 92.81 3.47 -1 -27 3 82.63 3.24 -1 28 4 2.31 0.77 -1 28 4 3.16 0.69 1 -28 -4 3.01 0.69 1 -28 -4 3.47 0.77 -1 27 4 38.19 2.01 -1 27 4 41.05 2.24 1 -27 -4 38.81 1.93 1 -27 -4 44.67 2.16 -1 26 4 3.47 0.85 -1 26 4 4.63 0.77 1 -26 -4 3.55 0.69 1 -26 -4 4.17 0.77 -1 25 4 6.10 0.77 -1 25 4 5.01 0.85 1 -25 -4 6.25 0.77 1 -25 -4 5.86 0.77 1 -24 -4 129.00 4.55 1 -24 -4 143.12 4.94 -1 23 4 -0.23 0.46 -1 23 4 -0.31 0.46 1 -23 -4 0.23 0.46 -1 22 4 7.41 0.85 -1 22 4 6.33 0.85 1 -22 -4 7.02 0.77 1 -22 -4 5.94 0.77 -1 21 4 -0.31 0.54 -1 21 4 0.54 0.46 1 -21 -4 0.46 0.46 -1 20 4 0.85 0.54 -1 20 4 1.70 0.54 1 -20 -4 1.16 0.46 1 -20 -4 1.85 0.54 -1 19 4 -0.23 0.46 -1 19 4 0.00 0.46 1 -19 -4 0.31 0.46 1 -19 -4 0.23 0.39 -1 18 4 799.30 23.92 -1 18 4 827.85 24.69 1 -18 -4 774.61 23.07 1 -18 -4 792.36 23.61 -1 17 4 1323.94 39.04 -1 17 4 1323.17 39.12 1 -17 -4 1298.48 38.27 1 -17 -4 1279.96 37.80 -1 16 4 2.85 0.54 -1 16 4 2.47 0.54 1 -16 -4 3.86 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2 3937.11 114.88 2 -3 -2 4123.82 120.28 -2 2 2 1709.71 50.07 -2 2 2 1849.35 54.08 2 -2 -2 1721.28 50.38 2 -2 -2 1668.04 48.84 -2 1 2 4.24 0.54 -2 1 2 3.93 0.46 2 -1 -2 3.39 0.54 2 -1 -2 4.09 0.54 -2 0 2 198.98 6.17 -2 0 2 211.48 6.48 2 0 -2 196.89 6.10 2 0 -2 199.98 6.17 -2 -1 2 3.24 0.54 -2 -1 2 3.47 0.62 2 1 -2 4.94 0.54 2 1 -2 4.47 0.54 -2 -2 2 1664.19 48.76 -2 -2 2 1672.67 49.07 2 2 -2 1649.53 48.37 2 2 -2 1712.79 50.23 -2 -3 2 3831.41 111.79 -2 -3 2 3683.27 107.55 2 3 -2 3802.86 110.95 2 3 -2 3802.86 111.02 -2 -4 2 565.84 16.90 -2 -4 2 591.92 17.59 2 4 -2 555.50 16.59 2 4 -2 559.20 16.67 -2 -5 2 88.88 3.01 -2 -5 2 86.87 2.93 2 5 -2 79.78 2.78 2 5 -2 87.65 2.93 -2 -6 2 796.22 23.61 -2 -6 2 814.73 24.15 2 6 -2 820.91 24.30 2 6 -2 846.37 25.07 -2 -7 2 428.28 12.88 -2 -7 2 423.49 12.73 2 7 -2 416.08 12.58 2 7 -2 424.80 12.81 -2 -8 2 101.46 3.39 -2 -8 2 96.21 3.24 2 8 -2 96.90 3.24 2 8 -2 92.66 3.24 -2 -9 2 125.68 4.17 -2 -9 2 124.06 4.09 -2 -10 2 30.40 1.39 -2 -10 2 31.86 1.47 2 10 -2 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48.84 2.39 -2 -25 2 6.71 0.85 -2 -25 2 8.72 1.00 2 25 -2 8.02 0.85 2 25 -2 9.95 1.23 -2 -26 2 1.00 0.54 2 26 -2 0.54 0.77 2 26 -2 1.23 0.54 -2 -27 2 0.00 0.54 -2 -27 2 -0.23 0.46 2 27 -2 0.23 0.54 -2 27 3 8.72 1.08 2 -27 -3 7.33 0.85 -2 26 3 1.00 0.62 -2 26 3 1.70 0.69 2 -26 -3 0.85 0.54 2 -26 -3 1.54 0.62 -2 25 3 -0.31 0.54 2 -25 -3 -0.15 0.54 2 -25 -3 0.00 0.54 -2 24 3 21.68 1.39 -2 24 3 26.93 1.62 2 -24 -3 23.92 1.47 2 -24 -3 18.90 1.31 -2 23 3 20.83 1.39 -2 23 3 23.45 1.47 2 -23 -3 21.06 1.31 2 -23 -3 20.37 1.23 -2 22 3 37.11 1.85 -2 22 3 31.63 1.62 2 -22 -3 30.78 1.54 2 -22 -3 32.48 1.62 -2 21 3 40.66 1.93 -2 21 3 42.67 1.93 2 -21 -3 41.51 1.85 2 -21 -3 40.20 1.77 2 -20 -3 19.67 1.16 2 -20 -3 19.91 1.16 -2 19 3 14.66 1.00 -2 19 3 12.96 0.93 2 -19 -3 13.81 1.00 2 -19 -3 13.66 0.93 -2 18 3 361.85 11.11 -2 18 3 366.17 11.26 2 -18 -3 375.58 11.42 2 -18 -3 364.55 11.26 -2 17 3 75.76 2.70 -2 17 3 78.23 2.85 2 -17 -3 77.92 2.85 2 -17 -3 78.39 2.78 -2 16 3 114.57 3.86 -2 16 3 106.78 3.70 2 -16 -3 112.72 3.86 2 -16 -3 108.71 3.63 -2 15 3 78.08 2.78 -2 15 3 84.41 2.93 2 -15 -3 80.47 2.78 2 -15 -3 77.62 2.78 -2 14 3 11.65 0.77 2 -14 -3 11.88 0.77 -2 13 3 3.01 0.46 2 -13 -3 3.09 0.39 -2 12 3 0.54 0.31 -2 12 3 0.46 0.39 2 -12 -3 0.39 0.31 2 -12 -3 0.85 0.39 -2 11 3 8.26 0.62 -2 11 3 7.48 0.62 2 -11 -3 7.56 0.54 2 -11 -3 7.25 0.62 -2 10 3 10.03 0.69 2 -10 -3 10.88 0.69 -2 9 3 90.04 3.09 2 -9 -3 87.34 2.93 -2 8 3 688.67 20.37 -2 8 3 682.18 20.29 2 -8 -3 672.85 19.98 2 -8 -3 671.00 19.83 -2 7 3 493.62 14.81 -2 7 3 516.38 15.35 2 -7 -3 519.70 15.43 2 -7 -3 482.13 14.43 -2 6 3 55.24 2.01 -2 6 3 56.78 1.93 2 -6 -3 55.63 2.01 2 -6 -3 59.64 2.08 -2 5 3 230.53 7.10 -2 5 3 256.92 7.79 2 -5 -3 238.63 7.25 2 -5 -3 242.95 7.48 -2 4 3 424.96 12.65 -2 4 3 401.43 12.04 2 -4 -3 403.89 12.11 2 -4 -3 411.53 12.27 -2 3 3 1015.33 29.94 -2 3 3 1046.96 30.78 2 -3 -3 1113.31 32.71 2 -3 -3 1050.82 30.94 -2 2 3 48.22 1.77 -2 2 3 47.37 1.77 2 -2 -3 45.52 1.70 2 -2 -3 51.77 1.85 -2 1 3 30.40 1.23 -2 1 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3 2.39 0.62 2 13 -3 2.85 0.46 -2 -14 3 9.64 0.77 -2 -14 3 9.95 0.85 2 14 -3 9.95 0.93 2 14 -3 9.03 0.69 -2 -15 3 75.61 2.70 -2 -15 3 76.84 2.85 2 15 -3 71.44 2.78 2 15 -3 78.23 2.78 -2 -16 3 105.24 3.70 2 16 -3 94.90 3.55 -2 -17 3 70.67 2.78 2 17 -3 61.18 2.55 -2 -18 3 333.69 10.42 -2 -18 3 362.08 11.11 2 18 -3 334.84 10.26 2 18 -3 330.83 10.49 -2 -19 3 9.57 0.85 -2 -19 3 10.96 1.00 -2 -20 3 18.52 1.23 -2 -20 3 17.90 1.16 2 20 -3 19.44 1.39 2 20 -3 16.74 1.08 -2 -21 3 38.11 1.85 -2 -21 3 36.18 1.70 2 21 -3 37.19 1.93 2 21 -3 40.35 1.77 -2 -22 3 28.47 1.62 -2 -22 3 23.69 1.39 2 22 -3 25.07 1.39 2 22 -3 29.78 1.77 -2 -23 3 16.43 1.23 -2 -23 3 16.97 1.23 2 23 -3 16.05 1.08 2 23 -3 16.20 1.31 -2 -24 3 17.82 1.23 -2 -24 3 17.28 1.23 2 24 -3 19.52 1.47 2 24 -3 16.28 1.16 -2 -25 3 0.54 0.46 -2 -25 3 -0.23 0.54 2 25 -3 -0.31 0.62 2 25 -3 0.23 0.46 -2 -26 3 1.70 0.62 -2 -26 3 1.62 0.54 2 26 -3 1.47 0.54 2 26 -3 1.62 0.69 -2 -27 3 7.18 0.85 -2 28 4 28.32 1.93 -2 28 4 33.02 2.01 2 -28 -4 29.55 1.70 2 -28 -4 32.71 1.93 -2 27 4 16.20 1.47 -2 27 4 15.51 1.39 2 -27 -4 14.35 1.16 2 -27 -4 15.51 1.31 -2 26 4 37.65 2.08 -2 26 4 37.42 2.08 2 -26 -4 39.89 2.08 2 -26 -4 37.57 1.93 2 -25 -4 23.38 1.47 2 -25 -4 24.38 1.47 -2 24 4 69.21 2.85 2 -24 -4 73.60 2.93 -2 23 4 1.00 0.54 -2 23 4 0.62 0.54 2 -23 -4 0.54 0.46 2 -23 -4 0.15 0.46 -2 22 4 19.06 1.31 2 -22 -4 19.21 1.23 -2 21 4 3.63 0.69 -2 21 4 2.31 0.62 2 -21 -4 3.93 0.62 2 -21 -4 2.93 0.54 -2 20 4 55.55 2.31 -2 20 4 58.94 2.39 2 -20 -4 55.09 2.16 2 -20 -4 60.26 2.47 -2 19 4 74.92 2.85 -2 19 4 71.83 2.78 2 -19 -4 70.21 2.70 2 -19 -4 72.37 2.70 -2 18 4 1.31 0.46 -2 18 4 0.93 0.54 2 -18 -4 1.70 0.46 2 -18 -4 1.85 0.54 -2 17 4 384.07 11.73 -2 17 4 383.37 11.80 2 -17 -4 402.43 12.19 2 -17 -4 412.46 12.65 -2 16 4 1456.64 42.90 -2 16 4 1428.87 42.13 2 -16 -4 1522.22 44.83 2 -16 -4 1521.45 44.90 -2 15 4 635.43 18.98 -2 15 4 607.27 18.21 2 -15 -4 639.60 19.21 2 -15 -4 619.38 18.52 -2 14 4 101.38 3.47 -2 14 4 101.15 3.39 2 -14 -4 102.07 3.39 2 -14 -4 108.25 3.70 -2 13 4 623.55 18.59 -2 13 4 633.66 18.98 2 -13 -4 648.85 19.37 2 -13 -4 640.14 19.06 -2 12 4 107.24 3.55 -2 12 4 103.31 3.47 2 -12 -4 108.17 3.63 2 -12 -4 111.02 3.63 -2 11 4 202.14 6.33 2 -11 -4 198.13 6.17 -2 10 4 56.09 2.01 2 -10 -4 54.70 1.93 -2 9 4 196.51 6.10 -2 9 4 194.35 6.10 2 -9 -4 198.21 6.10 2 -9 -4 191.03 6.02 -2 8 4 191.49 6.02 -2 8 4 187.71 5.79 2 -8 -4 190.88 6.02 2 -8 -4 185.01 5.71 -2 7 4 126.07 4.09 2 -7 -4 120.67 3.93 -2 6 4 726.62 21.60 2 -6 -4 714.28 21.22 -2 5 4 4.55 0.46 -2 5 4 5.09 0.54 2 -5 -4 3.24 0.46 2 -5 -4 4.71 0.54 -2 4 4 891.11 26.39 -2 4 4 874.91 25.77 2 -4 -4 874.14 25.77 2 -4 -4 830.16 24.53 -2 3 4 446.33 13.35 -2 3 4 401.89 12.11 2 -3 -4 419.09 12.58 2 -3 -4 408.22 12.19 -2 1 4 75.84 2.55 -2 1 4 73.37 2.62 2 -1 -4 81.40 2.78 2 -1 -4 72.52 2.55 -2 0 4 628.80 18.67 -2 0 4 648.70 19.29 -2 -1 4 74.22 2.62 -2 -1 4 78.54 2.70 2 1 -4 74.99 2.62 2 1 -4 75.69 2.62 -2 -2 4 234.16 7.18 -2 -2 4 215.95 6.71 2 2 -4 212.56 6.64 2 2 -4 212.71 6.56 -2 -3 4 422.87 12.65 -2 -3 4 389.78 11.80 2 3 -4 387.31 11.65 2 3 -4 421.02 12.65 -2 -4 4 805.47 23.92 -2 -4 4 790.04 23.38 2 4 -4 788.50 23.38 2 4 -4 818.59 24.23 -2 -5 4 4.47 0.54 -2 -5 4 4.24 0.62 2 5 -4 4.94 0.62 2 5 -4 3.63 0.54 -2 -6 4 685.35 20.45 -2 -6 4 683.65 20.29 2 6 -4 675.47 20.14 2 6 -4 686.12 20.37 -2 -7 4 120.05 4.01 -2 -7 4 122.60 4.01 2 7 -4 117.12 3.86 2 7 -4 121.90 4.01 -2 -8 4 183.16 5.86 -2 -8 4 177.99 5.63 2 8 -4 175.91 5.56 2 8 -4 172.98 5.56 -2 -9 4 179.69 5.71 -2 -9 4 185.09 5.86 2 9 -4 185.40 5.86 2 9 -4 185.01 5.94 -2 -10 4 53.00 2.01 -2 -10 4 54.24 2.08 2 10 -4 56.40 2.08 2 10 -4 52.93 2.08 -2 -11 4 184.24 5.86 -2 -11 4 172.82 5.56 2 11 -4 191.65 6.17 2 11 -4 185.32 5.86 -2 -12 4 97.06 3.32 -2 -12 4 93.28 3.32 2 12 -4 102.69 3.47 2 12 -4 96.60 3.39 -2 -13 4 613.29 18.36 2 13 -4 639.21 19.06 -2 -14 4 90.58 3.16 2 14 -4 90.73 3.09 -2 -15 4 567.07 17.05 -2 -15 4 574.17 17.28 2 15 -4 593.54 17.98 2 15 -4 588.75 17.59 -2 -16 4 1286.14 37.96 -2 -16 4 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1.31 4 -9 -4 19.37 1.08 -4 8 4 35.49 1.62 -4 8 4 33.48 1.77 4 -8 -4 33.56 1.54 4 -8 -4 31.25 1.62 -4 7 4 63.73 2.62 -4 7 4 59.95 2.31 4 -7 -4 65.43 2.62 4 -7 -4 59.25 2.31 -4 6 4 335.00 10.57 -4 6 4 327.36 10.11 4 -6 -4 336.85 10.42 4 -6 -4 337.47 10.57 -4 5 4 6.87 0.85 -4 5 4 7.79 0.77 4 -5 -4 5.63 0.69 4 -5 -4 7.41 0.85 -4 4 4 461.30 14.04 -4 4 4 472.56 14.50 4 -4 -4 475.65 14.50 4 -4 -4 462.69 14.12 -4 3 4 2.08 0.54 -4 3 4 2.62 0.69 4 -3 -4 2.39 0.62 4 -3 -4 2.78 0.54 -4 2 4 89.19 3.24 -4 2 4 100.30 3.70 4 -2 -4 92.27 3.39 4 -2 -4 87.03 3.16 -4 1 4 17.98 1.16 -4 1 4 18.29 1.31 4 -1 -4 17.67 1.16 4 -1 -4 15.20 1.08 -4 0 4 133.71 4.55 -4 0 4 150.06 5.17 4 0 -4 138.18 4.71 4 0 -4 143.35 4.86 -4 -1 4 15.28 1.31 -4 -1 4 14.20 1.08 4 1 -4 17.44 1.16 4 1 -4 20.14 1.31 -4 -2 4 99.30 3.55 -4 -2 4 90.35 3.39 4 2 -4 88.73 3.32 4 2 -4 92.89 3.47 -4 -3 4 3.39 0.69 -4 -3 4 4.32 0.77 4 3 -4 2.16 0.62 4 3 -4 3.39 0.69 -4 -4 4 485.75 14.81 -4 -4 4 471.71 14.50 4 4 -4 469.09 14.35 4 4 -4 447.18 13.81 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796.99 23.76 4 -4 -5 891.89 26.62 4 -4 -5 834.79 25.00 -4 3 5 405.36 12.58 -4 3 5 408.60 12.50 4 -3 -5 413.15 12.73 4 -3 -5 422.72 12.96 -4 2 5 283.77 9.10 -4 2 5 276.90 8.72 4 -2 -5 268.11 8.49 4 -2 -5 270.81 8.56 -4 1 5 230.15 7.48 -4 1 5 232.38 7.41 4 -1 -5 221.35 7.18 4 -1 -5 219.58 7.02 -4 0 5 -0.62 0.62 -4 0 5 0.39 0.46 4 0 -5 -0.23 0.54 4 0 -5 -0.39 0.46 -4 -1 5 224.28 7.33 -4 -1 5 231.46 7.41 4 1 -5 230.07 7.41 4 1 -5 228.14 7.41 -4 -2 5 253.83 8.02 -4 -2 5 272.04 8.72 4 2 -5 266.49 8.49 4 2 -5 279.52 8.87 -4 -3 5 396.72 12.19 -4 -3 5 410.38 12.73 4 3 -5 417.55 12.88 4 3 -5 410.07 12.73 -4 -4 5 827.85 24.92 -4 -4 5 757.64 22.68 4 4 -5 852.54 25.54 4 4 -5 825.53 24.77 -4 -5 5 1452.79 42.97 -4 -5 5 1331.66 39.58 4 5 -5 1433.50 42.43 4 5 -5 1387.98 41.12 -4 -6 5 134.63 4.78 -4 -6 5 141.19 4.86 4 6 -5 133.47 4.71 4 6 -5 131.08 4.63 -4 -7 5 1360.97 40.35 -4 -7 5 1377.18 40.89 4 7 -5 1299.25 38.65 4 7 -5 1326.26 39.35 -4 -8 5 714.59 21.68 -4 -8 5 709.19 21.37 4 8 -5 705.87 21.37 4 8 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30.48 2.08 4 23 -5 29.40 1.77 -4 -24 5 0.23 0.62 -4 -24 5 -0.46 0.62 4 24 -5 -0.23 0.69 4 24 -5 0.39 0.54 -4 -25 5 9.03 1.16 -4 -25 5 11.50 1.23 4 25 -5 10.96 1.23 4 25 -5 11.88 1.39 -4 -26 5 7.79 1.39 -4 26 6 14.04 1.54 -4 26 6 14.58 1.31 4 -26 -6 11.65 1.00 4 -26 -6 9.26 1.16 -4 25 6 0.85 0.62 -4 25 6 2.08 0.85 4 -25 -6 1.85 0.69 -4 24 6 2.78 0.85 -4 24 6 2.62 0.69 4 -24 -6 3.09 0.62 4 -24 -6 1.70 0.69 -4 23 6 9.88 1.00 -4 23 6 9.64 1.23 4 -23 -6 11.42 1.00 4 -23 -6 10.26 1.16 -4 22 6 6.71 0.85 -4 22 6 5.79 1.08 4 -22 -6 7.79 1.00 4 -22 -6 7.10 0.77 -4 21 6 32.10 1.77 -4 21 6 31.02 2.01 4 -21 -6 31.71 1.70 4 -21 -6 31.48 1.93 -4 20 6 2.93 0.85 -4 20 6 1.93 0.62 4 -20 -6 2.55 0.77 4 -20 -6 2.31 0.54 -4 19 6 2.08 0.77 -4 19 6 2.01 0.62 4 -19 -6 2.08 0.54 4 -19 -6 2.62 0.77 -4 18 6 7.79 0.85 4 -18 -6 7.87 0.77 -4 17 6 35.26 2.08 -4 17 6 35.95 1.77 4 -17 -6 37.57 2.08 4 -17 -6 39.97 1.77 -4 16 6 2.01 0.77 -4 16 6 1.85 0.54 4 -16 -6 1.93 0.54 4 -16 -6 2.16 0.69 -4 15 6 343.33 11.03 4 -15 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6 140.42 4.71 4 -2 -6 147.82 5.09 4 -2 -6 148.36 5.01 -4 1 6 552.03 16.67 -4 1 6 534.90 16.36 4 -1 -6 546.01 16.59 4 -1 -6 531.74 16.20 -4 0 6 53.85 2.39 -4 0 6 58.48 2.31 4 0 -6 50.77 2.24 4 0 -6 54.08 2.24 -4 -1 6 538.99 16.36 -4 -1 6 546.78 16.74 4 1 -6 525.41 16.05 4 1 -6 504.27 15.35 -4 -2 6 151.61 5.25 -4 -2 6 150.60 5.09 4 2 -6 149.91 5.09 4 2 -6 136.48 4.63 -4 -3 6 420.02 13.04 -4 -3 6 402.04 12.42 -4 -4 6 1094.03 32.48 -4 -4 6 1133.37 33.79 4 4 -6 1063.17 31.71 4 4 -6 1131.83 33.72 -4 -5 6 37.65 1.93 -4 -5 6 41.12 1.93 4 5 -6 43.82 2.08 4 5 -6 37.80 1.85 -4 -6 6 12.04 1.00 -4 -6 6 12.19 1.16 4 6 -6 16.05 1.23 4 6 -6 13.12 1.16 -4 -7 6 223.36 7.25 -4 -7 6 246.58 8.02 4 7 -6 248.05 8.02 4 7 -6 248.66 8.10 4 8 -6 115.34 4.24 4 8 -6 116.50 4.17 -4 -9 6 23.92 1.47 -4 -9 6 29.16 1.70 4 9 -6 24.92 1.54 4 9 -6 28.16 1.70 -4 -10 6 161.48 5.56 -4 -10 6 182.23 6.17 4 10 -6 161.02 5.63 4 10 -6 167.96 5.71 -4 -11 6 137.41 4.86 -4 -11 6 130.23 4.63 4 11 -6 126.45 4.63 4 11 -6 134.17 4.71 -4 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0.62 5 -25 -7 0.39 0.54 -5 24 7 3.55 1.00 -5 24 7 2.93 0.69 5 -24 -7 4.71 0.69 5 -24 -7 4.71 1.00 -5 23 7 47.29 2.47 5 -23 -7 43.75 2.16 -5 22 7 20.29 1.85 -5 22 7 15.82 1.31 5 -22 -7 17.05 1.23 5 -22 -7 18.67 1.62 -5 21 7 1.39 0.93 -5 21 7 0.39 0.62 5 -21 -7 0.39 0.69 -5 20 7 2.62 0.93 -5 20 7 3.09 0.69 5 -20 -7 2.85 0.62 5 -20 -7 2.78 0.77 -5 19 7 4.24 1.00 -5 19 7 4.24 0.69 5 -19 -7 3.63 0.85 5 -19 -7 3.16 0.62 -5 18 7 10.18 1.39 -5 18 7 8.49 1.00 5 -18 -7 11.03 1.16 5 -18 -7 10.49 0.93 -5 17 7 2.39 0.62 -5 17 7 1.31 0.77 5 -17 -7 2.16 0.62 5 -17 -7 2.93 0.77 -5 16 7 15.89 1.47 -5 16 7 13.96 1.16 5 -16 -7 14.66 1.08 5 -16 -7 12.88 1.23 -5 15 7 6.71 1.08 -5 15 7 6.25 0.85 5 -15 -7 5.94 0.93 5 -15 -7 7.72 0.85 -5 14 7 60.56 2.55 -5 14 7 57.25 2.85 5 -14 -7 59.79 2.85 5 -14 -7 57.25 2.39 -5 13 7 74.14 2.93 -5 13 7 78.00 3.47 5 -13 -7 74.84 2.93 5 -13 -7 81.24 3.39 -5 12 7 371.72 11.57 5 -12 -7 370.56 11.50 -5 11 7 90.81 3.39 5 -11 -7 94.74 3.47 -5 10 7 3.47 0.62 -5 10 7 3.16 0.93 5 -10 -7 3.86 0.69 5 -10 -7 3.63 0.85 -5 9 7 11.88 1.23 -5 9 7 11.26 1.00 5 -9 -7 14.66 1.31 5 -9 -7 11.80 1.00 -5 8 7 51.62 2.55 -5 8 7 43.75 2.08 5 -8 -7 43.05 2.01 5 -8 -7 50.38 2.39 -5 7 7 -0.23 0.69 5 -7 -7 0.15 0.62 -5 6 7 16.28 1.39 5 -6 -7 17.51 1.39 -5 5 7 1.31 0.77 -5 5 7 0.69 0.62 5 -5 -7 1.54 0.69 5 -5 -7 0.46 0.54 -5 4 7 204.15 6.71 -5 4 7 191.88 6.64 5 -4 -7 201.52 6.64 5 -4 -7 187.71 6.40 -5 3 7 4.86 0.93 -5 3 7 3.24 0.69 5 -3 -7 4.09 0.85 5 -3 -7 4.47 0.85 -5 2 7 17.44 1.23 -5 2 7 16.97 1.47 5 -2 -7 18.98 1.39 5 -2 -7 18.75 1.39 -5 1 7 227.91 7.41 -5 1 7 244.57 8.18 5 -1 -7 229.99 7.56 5 -1 -7 244.73 8.10 -5 0 7 0.15 0.62 -5 0 7 0.31 0.85 5 0 -7 0.46 0.69 5 0 -7 -0.39 0.62 -5 -1 7 245.96 8.02 -5 -1 7 253.83 8.49 5 1 -7 238.63 7.95 5 1 -7 230.46 7.64 -5 -2 7 17.90 1.39 -5 -2 7 19.67 1.54 5 2 -7 17.75 1.39 5 2 -7 19.21 1.47 -5 -3 7 4.55 0.85 -5 -3 7 4.32 1.00 5 3 -7 6.10 0.93 5 3 -7 6.10 0.93 -5 -4 7 199.29 6.71 -5 -4 7 197.67 6.79 5 4 -7 192.50 6.56 5 4 -7 200.21 6.79 -5 -5 7 2.01 0.77 -5 -5 7 1.39 0.85 5 5 -7 0.23 0.77 5 5 -7 1.08 0.69 -5 -6 7 16.36 1.31 -5 -6 7 16.43 1.47 5 6 -7 16.20 1.31 5 6 -7 15.97 1.39 -5 -7 7 -0.39 0.69 -5 -7 7 -1.16 0.62 5 7 -7 0.31 0.62 5 7 -7 0.23 0.69 -5 -8 7 50.23 2.47 -5 -8 7 47.76 2.31 5 8 -7 44.52 2.24 5 8 -7 51.15 2.55 -5 -9 7 11.80 1.23 5 9 -7 9.10 1.39 5 9 -7 12.34 1.16 -5 -10 7 3.63 0.85 5 10 -7 3.55 0.77 -5 -11 7 91.19 3.70 5 11 -7 94.28 3.70 -5 -12 7 335.15 10.80 -5 -12 7 322.81 10.42 5 12 -7 329.60 10.80 5 12 -7 359.53 11.42 -5 -13 7 74.38 3.16 5 13 -7 76.23 3.16 5 13 -7 78.16 3.39 -5 -14 7 56.24 2.70 -5 -14 7 62.49 2.78 5 14 -7 48.99 2.39 5 14 -7 58.25 2.85 -5 -15 7 7.79 1.00 5 15 -7 7.33 1.08 -5 -16 7 14.43 1.31 -5 -16 7 14.04 1.39 5 16 -7 13.73 1.39 5 16 -7 11.03 1.23 -5 -17 7 1.93 0.77 -5 -17 7 1.39 0.69 5 17 -7 2.24 0.69 5 17 -7 3.32 0.85 -5 -18 7 11.80 1.23 -5 -18 7 9.03 1.16 5 18 -7 10.18 1.08 5 18 -7 10.65 1.31 -5 -19 7 4.63 0.85 -5 -19 7 3.24 0.85 5 19 -7 2.62 0.77 5 19 -7 4.17 1.00 -5 -20 7 2.08 0.77 -5 -20 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0.31 0.54 5 -16 -8 0.00 0.69 -5 15 8 29.40 1.62 -5 15 8 28.08 1.93 5 -15 -8 28.24 1.54 5 -15 -8 26.23 1.77 -5 14 8 16.12 1.47 -5 14 8 15.43 1.16 5 -14 -8 14.66 1.31 5 -14 -8 16.20 1.16 -5 13 8 53.00 2.31 -5 13 8 51.85 2.70 5 -13 -8 50.54 2.47 5 -13 -8 51.38 2.24 -5 12 8 0.62 0.69 -5 12 8 -0.15 0.54 5 -12 -8 0.31 0.54 5 -12 -8 1.16 0.69 -5 11 8 103.92 4.17 -5 11 8 101.15 3.70 5 -11 -8 102.15 3.70 5 -11 -8 98.37 3.86 -5 10 8 10.72 1.23 -5 10 8 7.64 0.85 5 -10 -8 10.49 0.93 -5 9 8 0.85 0.46 5 -9 -8 0.15 0.54 -5 8 8 2.01 0.54 5 -8 -8 2.01 0.62 -5 7 8 65.89 3.01 -5 7 8 63.27 2.55 5 -7 -8 67.59 2.93 5 -7 -8 69.21 2.70 5 -6 -8 14.81 1.08 5 -6 -8 16.12 1.31 -5 5 8 3.47 0.69 -5 5 8 4.47 0.93 5 -5 -8 3.01 0.77 5 -5 -8 2.62 0.62 -5 4 8 8.33 1.08 -5 4 8 8.80 1.00 5 -4 -8 9.88 1.08 5 -4 -8 7.25 0.85 -5 3 8 19.29 1.54 5 -3 -8 17.51 1.39 -5 2 8 -0.08 0.69 5 -2 -8 -0.39 0.62 -5 1 8 0.54 0.69 5 -1 -8 -0.46 0.62 -5 0 8 10.65 1.23 5 0 -8 8.10 1.00 -5 -1 8 0.46 0.77 5 1 -8 0.00 0.69 -5 -2 8 0.62 0.77 5 2 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2.39 5 -13 -9 47.53 2.08 -5 12 9 43.28 2.39 -5 12 9 45.98 2.16 5 -12 -9 46.60 2.08 5 -12 -9 47.83 2.39 -5 11 9 10.34 1.23 -5 11 9 11.42 1.00 5 -11 -9 9.72 1.08 5 -11 -9 9.95 0.93 -5 10 9 59.64 2.85 -5 10 9 66.81 2.70 5 -10 -9 56.24 2.62 5 -10 -9 64.04 2.55 -5 9 9 1.31 0.77 -5 9 9 2.24 0.62 5 -9 -9 1.70 0.62 5 -9 -9 2.24 0.69 -5 8 9 8.18 1.08 -5 8 9 7.33 0.85 5 -8 -9 7.64 0.85 5 -8 -9 7.02 1.08 -5 7 9 71.37 3.16 -5 7 9 63.11 2.55 5 -7 -9 75.15 3.16 5 -7 -9 66.35 2.70 -5 6 9 83.25 3.16 -5 6 9 85.72 3.63 5 -6 -9 88.42 3.32 5 -6 -9 85.33 3.47 -5 5 9 25.92 1.47 5 -5 -9 25.38 1.47 -5 4 9 1.39 0.54 -5 3 9 -0.69 0.85 -5 3 9 0.54 0.54 5 -3 -9 -0.23 0.46 5 -3 -9 0.54 0.77 -5 2 9 41.82 2.01 -5 2 9 41.20 2.24 5 -2 -9 42.43 1.93 5 -2 -9 44.75 2.31 -5 1 9 56.48 2.70 -5 1 9 56.32 2.47 5 -1 -9 52.93 2.31 5 -1 -9 58.02 2.70 -5 0 9 0.15 0.77 -5 0 9 1.23 0.62 5 0 -9 0.31 0.54 5 0 -9 0.31 0.69 -5 -1 9 57.25 2.47 -5 -1 9 57.40 2.70 5 1 -9 58.56 2.55 5 1 -9 59.64 2.70 -5 -2 9 39.66 1.93 -5 -2 9 41.74 2.31 5 2 -9 40.81 2.24 5 2 -9 43.82 2.16 -5 -3 9 -0.31 0.54 -5 -3 9 -0.69 0.85 5 3 -9 0.08 0.69 5 3 -9 -0.46 0.62 -5 -4 9 0.54 0.62 -5 -4 9 2.01 0.85 5 4 -9 0.08 0.69 5 4 -9 1.93 0.77 -5 -5 9 31.48 1.93 -5 -5 9 29.40 1.70 -5 -6 9 81.86 3.47 -5 -6 9 79.31 3.16 5 6 -9 85.33 3.47 5 6 -9 78.00 3.24 -5 -7 9 68.13 3.01 -5 -7 9 61.88 2.70 5 7 -9 62.19 2.78 5 7 -9 65.81 2.93 -5 -8 9 7.33 1.08 -5 -8 9 7.33 0.93 5 8 -9 6.87 0.93 5 8 -9 7.41 1.00 -5 -9 9 2.08 0.85 -5 -9 9 2.47 0.69 5 9 -9 1.77 0.69 5 9 -9 1.47 0.69 -5 -10 9 62.26 2.78 -5 -10 9 63.19 2.93 5 10 -9 60.49 2.70 5 10 -9 57.17 2.70 -5 -11 9 8.56 1.23 -5 -11 9 11.19 1.16 5 11 -9 8.64 1.00 5 11 -9 8.56 1.08 -5 -12 9 40.89 2.24 5 12 -9 39.73 2.16 -5 -13 9 43.67 2.31 5 13 -9 39.04 2.16 5 14 -9 6.71 1.08 -5 -15 9 17.21 1.47 -5 -15 9 19.98 1.54 5 15 -9 16.05 1.31 5 15 -9 15.97 1.39 -5 -16 9 2.16 0.77 -5 -16 9 1.54 0.77 5 16 -9 1.00 0.69 5 16 -9 2.62 0.77 -5 -17 9 0.15 0.69 -5 -17 9 1.08 0.69 5 17 -9 0.62 0.62 5 17 -9 0.62 0.62 -5 -18 9 4.71 0.93 -5 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1.70 -9 0 0 14.43 1.39 9 0 0 13.35 1.23 9 0 0 8.80 1.62 -9 -1 0 2.55 1.00 -9 -1 0 3.01 0.93 9 1 0 1.39 1.08 9 1 0 3.47 0.77 -9 -2 0 -0.69 0.62 9 2 0 0.23 0.62 -9 -3 0 3.16 0.85 9 3 0 2.78 0.69 -9 12 1 0.08 0.93 -9 12 1 -0.39 0.69 9 -12 -1 0.00 0.69 9 -12 -1 0.62 0.62 -9 11 1 1.08 0.93 -9 11 1 0.00 0.77 9 -11 -1 0.23 0.69 9 -11 -1 0.77 0.77 -9 9 1 4.17 1.08 -9 9 1 2.62 0.93 9 -9 -1 0.54 0.77 9 -9 -1 1.93 0.85 -9 8 1 0.77 0.85 -9 8 1 -0.54 0.85 9 -8 -1 0.93 0.77 9 -8 -1 1.16 0.77 -9 7 1 0.85 0.85 -9 7 1 -0.23 0.85 9 -7 -1 0.00 0.62 9 -7 -1 0.54 0.77 -9 6 1 1.47 0.85 -9 6 1 2.08 0.85 9 -6 -1 0.46 0.69 9 -6 -1 0.31 0.85 -9 5 1 0.85 0.85 -9 5 1 1.31 0.93 9 -5 -1 1.62 0.69 9 -5 -1 1.31 0.93 -9 4 1 1.08 0.85 -9 4 1 0.62 0.77 9 -4 -1 -0.93 0.85 9 -4 -1 -0.54 0.62 -9 3 1 0.77 0.85 -9 3 1 3.39 1.00 9 -3 -1 1.39 0.93 9 -3 -1 2.01 0.69 -9 2 1 2.78 0.77 -9 2 1 1.08 0.85 9 -2 -1 1.16 1.00 9 -2 -1 0.69 0.62 -9 1 1 1.54 0.69 -9 1 1 0.77 0.85 9 -1 -1 0.62 0.54 9 -1 -1 0.23 0.93 -9 0 1 0.54 0.85 -9 0 1 -0.39 0.62 9 0 -1 -0.08 0.54 9 0 -1 1.08 0.93 -9 -1 1 -0.46 0.69 -9 -1 1 1.23 0.85 9 1 -1 -0.23 0.54 9 1 -1 0.39 0.93 -9 -2 1 0.46 0.93 -9 -2 1 1.70 0.77 9 2 -1 0.00 1.00 9 2 -1 1.54 0.62 -9 -3 1 1.47 0.77 9 3 -1 1.47 0.62 -9 -4 1 0.31 0.69 9 4 -1 0.08 0.54 -9 -5 1 0.54 0.85 -9 13 2 0.00 0.77 -9 13 2 1.85 0.93 9 -13 -2 0.77 0.69 9 -13 -2 0.85 0.69 -9 12 2 -0.54 0.93 -9 12 2 -0.46 0.77 9 -12 -2 -0.15 0.62 9 -12 -2 0.69 0.77 -9 11 2 0.39 0.93 -9 11 2 0.85 0.77 9 -11 -2 0.69 0.69 9 -11 -2 0.46 0.69 -9 10 2 1.31 0.93 -9 10 2 -0.23 0.77 9 -10 -2 0.31 0.69 9 -10 -2 0.54 0.77 -9 9 2 0.46 0.77 -9 9 2 0.39 0.85 9 -9 -2 -0.39 0.69 9 -9 -2 -0.15 0.69 -9 8 2 -0.23 0.77 -9 8 2 0.00 0.77 9 -8 -2 0.23 0.69 9 -8 -2 0.31 0.77 -9 7 2 0.08 0.77 -9 7 2 0.62 0.85 9 -7 -2 0.23 0.77 9 -7 -2 0.08 0.62 -9 6 2 -0.31 0.77 -9 6 2 -0.23 0.77 9 -6 -2 -0.85 0.77 9 -6 -2 -0.08 0.62 -9 5 2 2.01 0.93 -9 5 2 1.00 0.93 9 -5 -2 2.16 0.77 9 -5 -2 1.70 0.93 -9 4 2 1.47 0.93 -9 4 2 2.70 0.93 9 -4 -2 3.09 0.77 9 -4 -2 1.70 0.93 -9 3 2 1.47 0.77 -9 3 2 -0.23 0.77 9 -3 -2 -0.23 0.93 9 -3 -2 0.23 0.62 -9 2 2 1.31 0.85 -9 2 2 0.15 0.85 9 -2 -2 0.39 0.93 9 -2 -2 1.08 0.62 -9 1 2 1.47 0.85 -9 1 2 2.08 0.93 9 -1 -2 1.62 0.69 9 -1 -2 1.31 1.08 -9 0 2 0.00 0.77 -9 0 2 0.08 0.77 9 0 -2 0.93 0.62 9 0 -2 -0.15 0.85 -9 -1 2 4.24 1.00 -9 -1 2 2.62 0.93 9 1 -2 1.62 1.08 9 1 -2 3.70 0.77 -9 -2 2 1.39 0.77 -9 -2 2 1.62 0.93 9 2 -2 0.54 0.93 9 2 -2 0.46 0.62 -9 -3 2 1.31 0.93 -9 -3 2 0.93 0.69 9 3 -2 0.08 1.08 9 3 -2 0.69 0.62 -9 -4 2 0.69 0.77 9 4 -2 1.31 0.62 -9 -5 2 2.08 0.77 9 5 -2 2.93 0.69 -9 14 3 1.00 0.85 -9 14 3 2.16 0.77 9 -14 -3 1.54 0.77 9 -14 -3 3.32 0.93 -9 13 3 1.00 0.93 -9 13 3 0.85 0.69 9 -13 -3 -0.08 0.69 9 -13 -3 0.62 0.69 -9 12 3 -0.54 0.85 -9 12 3 1.00 0.77 9 -12 -3 0.23 0.69 9 -12 -3 0.31 0.62 -9 11 3 1.08 0.77 -9 11 3 0.77 0.93 9 -11 -3 -0.23 0.69 9 -11 -3 -0.62 0.69 -9 10 3 0.39 0.69 -9 10 3 0.62 0.93 9 -10 -3 0.62 0.69 9 -10 -3 -0.69 0.69 -9 9 3 0.08 0.85 -9 9 3 -0.08 0.69 9 -9 -3 -0.08 0.69 9 -9 -3 -0.08 0.69 -9 8 3 1.70 0.85 -9 8 3 1.77 0.93 9 -8 -3 1.08 0.77 9 -8 -3 1.85 0.93 -9 7 3 -0.15 0.77 -9 7 3 0.39 0.85 9 -7 -3 -1.16 0.62 9 -7 -3 1.16 0.77 -9 6 3 0.08 0.85 -9 6 3 1.47 0.85 9 -6 -3 0.62 0.85 9 -6 -3 0.39 0.69 -9 5 3 2.62 0.93 -9 5 3 1.54 0.93 9 -5 -3 0.93 0.85 9 -5 -3 1.47 0.69 -9 4 3 2.16 0.85 -9 4 3 1.16 0.93 9 -4 -3 0.85 0.69 9 -4 -3 1.77 0.93 -9 3 3 -0.54 0.85 -9 3 3 1.47 0.77 9 -3 -3 0.15 0.85 9 -3 -3 1.00 0.69 -9 2 3 3.86 1.08 -9 2 3 4.47 1.00 9 -2 -3 4.71 1.16 9 -2 -3 4.55 0.85 -9 1 3 0.46 0.77 -9 1 3 0.31 0.77 9 -1 -3 -0.23 0.62 9 -1 -3 -0.69 0.85 -9 0 3 -0.62 0.77 -9 0 3 0.93 0.85 9 0 -3 0.93 0.93 9 0 -3 0.15 0.62 -9 -1 3 -0.46 0.77 -9 -1 3 0.69 0.77 9 1 -3 -0.23 0.62 9 1 -3 -0.69 0.93 -9 -2 3 3.78 1.00 -9 -2 3 4.71 1.00 9 2 -3 5.32 0.85 9 2 -3 5.48 1.31 -9 -3 3 0.00 0.85 -9 -3 3 0.46 0.77 9 3 -3 0.69 1.00 9 3 -3 1.70 0.69 -9 -4 3 2.47 0.85 9 4 -3 0.54 0.62 -9 -5 3 1.54 0.77 9 5 -3 1.39 0.69 -9 -6 3 0.15 0.69 9 6 -3 0.00 0.62 -9 15 4 0.08 0.69 9 -15 -4 -0.15 0.77 -9 14 4 3.47 0.93 9 -14 -4 4.71 1.00 -9 13 4 1.85 0.85 -9 13 4 4.78 1.08 9 -13 -4 1.31 0.85 9 -13 -4 2.47 0.77 -9 12 4 13.04 1.54 -9 12 4 8.64 1.31 9 -12 -4 8.18 1.16 9 -12 -4 10.42 1.23 -9 11 4 6.64 1.16 -9 11 4 4.40 1.08 9 -11 -4 4.94 1.00 9 -11 -4 7.79 1.08 -9 10 4 -0.85 0.77 -9 10 4 -0.31 0.69 9 -10 -4 0.46 0.69 9 -10 -4 0.15 0.69 -9 9 4 0.54 0.77 -9 9 4 0.08 0.77 9 -9 -4 0.54 0.62 9 -9 -4 0.23 0.77 -9 8 4 1.62 0.85 -9 8 4 0.62 0.77 9 -8 -4 2.39 0.93 9 -8 -4 0.69 0.69 -9 7 4 3.86 1.08 -9 7 4 6.56 1.16 9 -7 -4 5.32 1.00 9 -7 -4 5.09 1.16 -9 6 4 3.32 0.93 -9 6 4 2.62 0.93 9 -6 -4 2.31 0.77 9 -6 -4 3.47 1.00 -9 5 4 0.08 0.77 -9 5 4 0.77 0.77 9 -5 -4 -0.54 0.62 9 -5 -4 0.62 0.77 -9 4 4 1.00 0.85 -9 4 4 1.31 0.77 9 -4 -4 0.62 0.77 9 -4 -4 0.77 0.69 -9 3 4 1.16 0.85 -9 3 4 2.08 0.85 9 -3 -4 0.23 0.85 9 -3 -4 0.39 0.62 -9 2 4 2.78 0.85 -9 2 4 2.62 1.00 9 -2 -4 3.01 0.77 9 -2 -4 2.24 1.00 -9 1 4 0.00 0.77 -9 1 4 -0.31 0.85 9 -1 -4 -0.23 0.85 9 -1 -4 0.15 0.62 -9 0 4 2.08 0.85 -9 0 4 1.70 0.85 9 0 -4 1.93 1.00 9 0 -4 1.00 0.69 -9 -1 4 -0.39 0.77 -9 -1 4 0.85 0.77 9 1 -4 -0.15 0.85 9 1 -4 -0.15 0.54 -9 -2 4 1.70 0.85 -9 -2 4 3.16 0.93 9 2 -4 2.62 0.77 9 2 -4 1.31 1.00 -9 -3 4 0.23 0.85 -9 -3 4 -0.31 0.77 9 3 -4 0.46 0.93 9 3 -4 0.39 0.69 -9 -4 4 -0.62 0.69 9 4 -4 0.85 0.62 -9 -5 4 -1.00 0.77 9 5 -4 -0.39 0.62 -9 -6 4 2.62 0.93 9 6 -4 2.08 0.77 -9 13 5 9.03 1.31 9 -13 -5 6.10 1.00 -9 12 5 4.32 1.16 9 -12 -5 2.78 0.85 -9 11 5 20.99 1.85 9 -11 -5 17.13 1.47 -9 10 5 2.16 0.93 -9 10 5 2.39 0.85 9 -10 -5 1.00 0.77 9 -10 -5 1.93 0.77 -9 9 5 3.86 0.93 -9 9 5 5.79 1.08 9 -9 -5 5.63 1.08 9 -9 -5 3.55 0.85 -9 8 5 0.54 0.77 -9 8 5 0.08 0.77 9 -8 -5 -0.69 0.77 9 -8 -5 0.23 0.69 -9 7 5 0.54 0.77 -9 7 5 1.00 0.77 9 -7 -5 0.77 0.62 9 -7 -5 0.08 0.77 -9 6 5 0.93 0.77 -9 6 5 -0.39 0.69 9 -6 -5 0.46 0.85 9 -6 -5 -0.08 0.62 -9 5 5 -0.69 0.69 -9 5 5 -0.54 0.77 9 -5 -5 -0.31 0.69 9 -5 -5 0.46 0.62 -9 4 5 0.31 0.69 -9 4 5 -0.77 0.77 9 -4 -5 0.31 0.62 9 -4 -5 -0.23 0.77 -9 3 5 3.01 0.93 -9 3 5 1.39 0.93 9 -3 -5 0.93 0.85 9 -3 -5 1.39 0.69 -9 2 5 0.31 0.77 -9 2 5 0.77 0.77 9 -2 -5 0.23 0.77 9 -2 -5 0.31 0.62 -9 1 5 0.62 0.77 -9 1 5 0.31 0.77 9 -1 -5 0.69 0.85 9 -1 -5 0.00 0.62 -9 0 5 0.46 0.77 -9 0 5 0.39 0.77 9 0 -5 0.00 0.62 9 0 -5 0.39 0.85 -9 -1 5 -0.93 0.69 -9 -1 5 -0.15 0.69 9 1 -5 -0.31 0.62 9 1 -5 -1.62 0.85 -9 -2 5 1.16 0.85 -9 -2 5 0.00 0.77 9 2 -5 0.69 0.62 9 2 -5 0.62 0.93 -9 -3 5 1.85 0.85 9 3 -5 2.16 0.69 -9 -4 5 -0.46 0.77 9 4 -5 -0.39 0.62 -9 -5 5 -0.54 0.69 9 5 -5 0.31 0.62 -9 -6 5 0.39 0.77 9 6 -5 -0.31 0.62 -9 11 6 6.48 1.31 9 -11 -6 4.40 1.00 -9 10 6 6.02 1.08 9 -10 -6 5.09 0.93 -9 9 6 -0.62 0.77 9 -9 -6 -0.77 0.62 -9 8 6 -0.85 0.69 9 -8 -6 -0.46 0.62 -9 7 6 1.16 0.77 -9 7 6 2.31 0.85 -9 6 6 0.93 0.69 -9 6 6 1.23 0.77 9 -6 -6 0.46 0.69 9 -6 -6 1.08 0.77 -9 5 6 2.47 0.85 -9 5 6 2.01 0.85 9 -5 -6 3.01 0.93 9 -5 -6 2.24 0.69 -9 4 6 3.93 0.93 -9 4 6 3.39 0.93 9 -4 -6 4.71 1.08 9 -4 -6 4.24 0.85 -9 3 6 0.23 0.69 -9 3 6 0.00 0.69 9 -3 -6 -0.31 0.77 9 -3 -6 0.46 0.62 -9 2 6 0.39 0.69 -9 2 6 0.39 0.77 9 -2 -6 -0.39 0.54 9 -2 -6 -0.85 0.69 -9 1 6 1.23 0.69 -9 1 6 -0.15 0.77 9 -1 -6 0.31 0.62 9 -1 -6 0.77 0.85 -9 0 6 1.08 0.85 -9 0 6 -1.08 0.69 9 0 -6 0.39 0.77 9 0 -6 0.69 0.62 -9 -1 6 -0.39 0.69 -9 -1 6 0.31 0.93 9 1 -6 1.54 0.69 9 1 -6 0.69 0.93 -9 -2 6 0.15 0.77 9 2 -6 1.23 0.69 -9 -3 6 0.31 0.77 9 3 -6 -0.23 0.62 -9 -4 6 3.39 0.93 9 4 -6 4.32 0.85 -9 -5 6 1.47 0.93 -9 8 7 0.15 0.85 9 -8 -7 1.23 0.77 -9 7 7 0.77 0.77 9 -7 -7 0.93 0.69 -9 6 7 -0.46 0.69 9 -6 -7 0.39 0.62 -9 5 7 0.23 0.69 9 -5 -7 0.39 0.62 -9 4 7 1.70 0.77 9 -4 -7 2.85 0.77 -9 3 7 5.17 0.93 9 -3 -7 3.32 0.85 -9 2 7 0.77 0.77 9 -2 -7 1.62 0.69 -9 1 7 14.12 1.39 9 -1 -7 12.50 1.23 -9 0 7 -0.46 0.69 9 0 -7 0.39 0.62 -9 -1 7 11.42 1.31 9 1 -7 12.27 1.16 -9 -2 7 0.62 0.77 9 2 -7 1.16 0.69 -9 -3 7 3.24 0.93 9 3 -7 4.71 0.85 -9 3 8 -0.15 0.77 -9 2 8 0.15 0.77 9 -2 -8 -0.08 0.62 -9 1 8 0.69 0.69 9 -1 -8 0.54 0.62 -9 0 8 1.16 0.85 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 96061 _olex2_submission_original_sample_id 5a _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.24953(15) 0.47596(4) 0.41462(7) 0.0416(2) Uani 1 1 d . . . . . O3 O 0.22592(17) 0.48356(5) 0.78735(7) 0.0494(3) Uani 1 1 d . . . . . H3 H 0.238743 0.522936 0.776018 0.074 Uiso 1 1 calc R U . . . O2 O 0.27300(18) 0.58617(5) 0.68181(7) 0.0508(3) Uani 1 1 d . . . . . O4 O 0.2726(2) 0.75158(5) -0.04387(8) 0.0634(3) Uani 1 1 d . . . . . N1 N 0.2750(2) 0.70561(5) 0.02267(8) 0.0511(3) Uani 1 1 d . . . . . C15 C 0.2722(2) 0.56322(6) 0.30150(9) 0.0395(3) Uani 1 1 d . . . . . C1 C 0.26656(19) 0.54105(6) 0.41025(9) 0.0391(3) Uani 1 1 d . . . . . C14 C 0.2787(2) 0.62909(6) 0.28059(9) 0.0409(3) Uani 1 1 d . . . . . H14 H 0.283444 0.659624 0.336529 0.049 Uiso 1 1 calc R U . . . C3 C 0.2641(2) 0.55230(6) 0.59972(9) 0.0419(3) Uani 1 1 d . . . . . C2 C 0.2754(2) 0.57905(6) 0.49752(9) 0.0416(3) Uani 1 1 d . . . . . H2 H 0.289443 0.624215 0.491068 0.050 Uiso 1 1 calc R U . . . C9 C 0.2366(2) 0.44680(6) 0.50924(9) 0.0411(3) Uani 1 1 d . . . . . C17 C 0.2651(2) 0.53938(6) 0.11445(9) 0.0441(3) Uani 1 1 d . . . . . H17 H 0.260661 0.509155 0.058089 0.053 Uiso 1 1 calc R U . . . C10 C 0.2795(2) 0.71726(6) 0.13809(9) 0.0451(3) Uani 1 1 d . . . . . C16 C 0.2661(2) 0.51872(6) 0.21834(9) 0.0423(3) Uani 1 1 d . . . . . H16 H 0.262633 0.474014 0.232996 0.051 Uiso 1 1 calc R U . . . C11 C 0.2782(2) 0.64908(6) 0.17683(9) 0.0414(3) Uani 1 1 d . . . . . C13 C 0.2694(2) 0.63727(6) -0.01088(9) 0.0464(3) Uani 1 1 d . . . . . C5 C 0.2235(2) 0.45027(6) 0.69665(10) 0.0437(3) Uani 1 1 d . . . . . C4 C 0.2406(2) 0.48305(6) 0.60204(9) 0.0405(3) Uani 1 1 d . . . . . C8 C 0.2192(2) 0.38058(6) 0.50721(10) 0.0452(3) Uani 1 1 d . . . . . H8 H 0.220392 0.356730 0.443887 0.054 Uiso 1 1 calc R U . . . C21 C 0.4562(3) 0.62121(7) -0.05098(11) 0.0530(3) Uani 1 1 d . . . . . H21A H 0.454279 0.646107 -0.116431 0.080 Uiso 1 1 calc R U . . . H21B H 0.456906 0.575197 -0.067422 0.080 Uiso 1 1 calc R U . . . H21C H 0.576941 0.632047 0.005244 0.080 Uiso 1 1 calc R U . . . C19 C 0.4673(3) 0.75476(6) 0.19277(11) 0.0527(3) Uani 1 1 d . . . . . H19A H 0.586046 0.732610 0.181117 0.079 Uiso 1 1 calc R U . . . H19B H 0.476790 0.757730 0.270515 0.079 Uiso 1 1 calc R U . . . H19C H 0.459985 0.798095 0.161877 0.079 Uiso 1 1 calc R U . . . C12 C 0.2707(2) 0.60473(6) 0.09466(9) 0.0424(3) Uani 1 1 d . . . . . C7 C 0.1997(2) 0.35004(7) 0.60118(11) 0.0482(3) Uani 1 1 d . . . . . H7 H 0.185097 0.304617 0.601156 0.058 Uiso 1 1 calc R U . . . C6 C 0.2012(2) 0.38418(6) 0.69512(10) 0.0464(3) Uani 1 1 d . . . . . H6 H 0.186903 0.362163 0.758010 0.056 Uiso 1 1 calc R U . . . C18 C 0.0910(3) 0.75384(7) 0.14642(12) 0.0538(4) Uani 1 1 d . . . . . H18A H 0.093306 0.797074 0.116220 0.081 Uiso 1 1 calc R U . . . H18B H 0.087241 0.757087 0.222509 0.081 Uiso 1 1 calc R U . . . H18C H -0.028336 0.730817 0.105882 0.081 Uiso 1 1 calc R U . . . C20 C 0.0766(3) 0.62389(7) -0.09777(10) 0.0537(4) Uani 1 1 d . . . . . H20A H -0.039516 0.637612 -0.071675 0.081 Uiso 1 1 calc R U . . . H20B H 0.066439 0.577749 -0.113707 0.081 Uiso 1 1 calc R U . . . H20C H 0.079299 0.647748 -0.163627 0.081 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0693(6) 0.0311(4) 0.0274(4) 0.0025(3) 0.0174(4) 0.0004(3) O3 0.0781(7) 0.0449(5) 0.0289(4) 0.0025(3) 0.0201(4) 0.0001(4) O2 0.0886(7) 0.0399(5) 0.0273(4) -0.0015(3) 0.0206(4) -0.0029(4) O4 0.1259(10) 0.0372(5) 0.0328(5) 0.0089(4) 0.0304(5) 0.0033(5) N1 0.0982(9) 0.0329(5) 0.0268(4) 0.0030(4) 0.0242(5) 0.0024(5) C15 0.0618(7) 0.0336(5) 0.0256(5) 0.0023(4) 0.0152(4) 0.0013(5) C1 0.0599(7) 0.0318(5) 0.0273(5) 0.0021(4) 0.0142(4) 0.0005(4) C14 0.0681(7) 0.0327(5) 0.0249(5) 0.0002(4) 0.0169(4) 0.0015(5) C3 0.0647(7) 0.0364(5) 0.0268(5) 0.0018(4) 0.0154(4) 0.0000(5) C2 0.0668(7) 0.0335(5) 0.0268(5) 0.0013(4) 0.0160(5) -0.0015(5) C9 0.0618(7) 0.0347(5) 0.0294(5) 0.0041(4) 0.0160(5) 0.0007(5) C17 0.0741(8) 0.0337(6) 0.0274(5) -0.0011(4) 0.0182(5) 0.0013(5) C10 0.0814(9) 0.0319(5) 0.0255(5) 0.0032(4) 0.0200(5) 0.0037(5) C16 0.0684(8) 0.0321(5) 0.0292(5) 0.0006(4) 0.0173(5) 0.0008(5) C11 0.0688(8) 0.0325(5) 0.0260(5) 0.0016(4) 0.0179(5) 0.0028(5) C13 0.0835(9) 0.0345(5) 0.0252(5) 0.0009(4) 0.0208(5) 0.0027(5) C5 0.0623(7) 0.0420(6) 0.0296(5) 0.0057(5) 0.0165(5) 0.0017(5) C4 0.0607(7) 0.0355(6) 0.0276(5) 0.0035(4) 0.0149(5) 0.0009(4) C8 0.0694(8) 0.0334(6) 0.0347(6) 0.0025(4) 0.0168(5) 0.0008(5) C21 0.0863(10) 0.0456(7) 0.0337(6) 0.0007(5) 0.0274(6) 0.0008(6) C19 0.0864(10) 0.0338(6) 0.0388(6) 0.0036(5) 0.0171(6) -0.0015(6) C12 0.0709(8) 0.0337(5) 0.0256(5) 0.0014(4) 0.0176(5) 0.0029(5) C7 0.0704(8) 0.0360(6) 0.0404(6) 0.0070(5) 0.0177(6) 0.0003(5) C6 0.0658(8) 0.0405(6) 0.0351(6) 0.0098(5) 0.0166(5) 0.0018(5) C18 0.0865(10) 0.0388(6) 0.0404(6) 0.0052(5) 0.0236(6) 0.0107(6) C20 0.0864(10) 0.0460(7) 0.0295(5) 0.0023(5) 0.0157(6) 0.0037(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 O1 C9 120.00(9) . . ? C5 O3 H3 109.5 . . ? O4 N1 C10 122.08(10) . . ? O4 N1 C13 122.09(10) . . ? C13 N1 C10 115.82(9) . . ? C14 C15 C1 119.75(10) . . ? C14 C15 C16 119.93(10) . . ? C16 C15 C1 120.30(10) . . ? O1 C1 C15 111.88(9) . . ? C2 C1 O1 122.24(10) . . ? C2 C1 C15 125.88(11) . . ? C15 C14 H14 120.6 . . ? C11 C14 C15 118.89(10) . . ? C11 C14 H14 120.6 . . ? O2 C3 C2 122.64(12) . . ? O2 C3 C4 121.64(11) . . ? C2 C3 C4 115.72(10) . . ? C1 C2 C3 121.24(11) . . ? C1 C2 H2 119.4 . . ? C3 C2 H2 119.4 . . ? O1 C9 C4 120.95(11) . . ? O1 C9 C8 116.59(11) . . ? C8 C9 C4 122.46(11) . . ? C16 C17 H17 120.6 . . ? C12 C17 H17 120.6 . . ? C12 C17 C16 118.87(11) . . ? N1 C10 C11 99.90(9) . . ? N1 C10 C19 110.22(12) . . ? N1 C10 C18 109.87(12) . . ? C11 C10 C19 113.94(11) . . ? C11 C10 C18 111.91(11) . . ? C19 C10 C18 110.51(11) . . ? C15 C16 H16 119.7 . . ? C17 C16 C15 120.65(11) . . ? C17 C16 H16 119.7 . . ? C14 C11 C10 126.74(10) . . ? C14 C11 C12 120.85(11) . . ? C12 C11 C10 112.38(10) . . ? N1 C13 C21 109.97(12) . . ? N1 C13 C12 100.30(9) . . ? N1 C13 C20 109.88(12) . . ? C12 C13 C21 112.35(12) . . ? C12 C13 C20 112.32(12) . . ? C20 C13 C21 111.46(11) . . ? O3 C5 C4 119.96(12) . . ? O3 C5 C6 120.11(11) . . ? C6 C5 C4 119.92(11) . . ? C9 C4 C3 119.82(10) . . ? C9 C4 C5 118.28(12) . . ? C5 C4 C3 121.90(11) . . ? C9 C8 H8 121.2 . . ? C9 C8 C7 117.70(12) . . ? C7 C8 H8 121.2 . . ? C13 C21 H21A 109.5 . . ? C13 C21 H21B 109.5 . . ? C13 C21 H21C 109.5 . . ? H21A C21 H21B 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C10 C19 H19A 109.5 . . ? C10 C19 H19B 109.5 . . ? C10 C19 H19C 109.5 . . ? H19A C19 H19B 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C17 C12 C11 120.80(10) . . ? C17 C12 C13 127.61(10) . . ? C11 C12 C13 111.59(10) . . ? C8 C7 H7 119.1 . . ? C6 C7 C8 121.83(12) . . ? C6 C7 H7 119.1 . . ? C5 C6 C7 119.79(11) . . ? C5 C6 H6 120.1 . . ? C7 C6 H6 120.1 . . ? C10 C18 H18A 109.5 . . ? C10 C18 H18B 109.5 . . ? C10 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C13 C20 H20A 109.5 . . ? C13 C20 H20B 109.5 . . ? C13 C20 H20C 109.5 . . ? H20A C20 H20B 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C1 1.3611(14) . ? O1 C9 1.3736(13) . ? O3 H3 0.8400 . ? O3 C5 1.3454(15) . ? O2 C3 1.2512(14) . ? O4 N1 1.2761(13) . ? N1 C10 1.4856(15) . ? N1 C13 1.4821(16) . ? C15 C1 1.4719(15) . ? C15 C14 1.3986(16) . ? C15 C16 1.4008(15) . ? C1 C2 1.3547(15) . ? C14 H14 0.9500 . ? C14 C11 1.3871(14) . ? C3 C2 1.4375(15) . ? C3 C4 1.4505(18) . ? C2 H2 0.9500 . ? C9 C4 1.3984(16) . ? C9 C8 1.3823(17) . ? C17 H17 0.9500 . ? C17 C16 1.3920(15) . ? C17 C12 1.3848(17) . ? C10 C11 1.5024(16) . ? C10 C19 1.522(2) . ? C10 C18 1.528(2) . ? C16 H16 0.9500 . ? C11 C12 1.3881(15) . ? C13 C21 1.532(2) . ? C13 C12 1.5053(15) . ? C13 C20 1.529(2) . ? C5 C4 1.4165(15) . ? C5 C6 1.3826(19) . ? C8 H8 0.9500 . ? C8 C7 1.3922(16) . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C7 H7 0.9500 . ? C7 C6 1.3912(18) . ? C6 H6 0.9500 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C1 C2 C3 -1.0(2) . . . . ? O1 C9 C4 C3 -1.65(19) . . . . ? O1 C9 C4 C5 179.01(12) . . . . ? O1 C9 C8 C7 -178.11(12) . . . . ? O3 C5 C4 C3 1.0(2) . . . . ? O3 C5 C4 C9 -179.72(12) . . . . ? O3 C5 C6 C7 -179.71(13) . . . . ? O2 C3 C2 C1 179.60(13) . . . . ? O2 C3 C4 C9 -178.33(13) . . . . ? O2 C3 C4 C5 1.0(2) . . . . ? O4 N1 C10 C11 179.34(14) . . . . ? O4 N1 C10 C19 -60.44(18) . . . . ? O4 N1 C10 C18 61.57(19) . . . . ? O4 N1 C13 C21 62.65(19) . . . . ? O4 N1 C13 C12 -178.85(15) . . . . ? O4 N1 C13 C20 -60.40(18) . . . . ? N1 C10 C11 C14 -179.20(14) . . . . ? N1 C10 C11 C12 -0.87(16) . . . . ? N1 C13 C12 C17 179.31(15) . . . . ? N1 C13 C12 C11 -0.54(16) . . . . ? C15 C1 C2 C3 178.56(13) . . . . ? C15 C14 C11 C10 178.38(13) . . . . ? C15 C14 C11 C12 0.2(2) . . . . ? C1 O1 C9 C4 0.00(18) . . . . ? C1 O1 C9 C8 179.85(12) . . . . ? C1 C15 C14 C11 -178.19(12) . . . . ? C1 C15 C16 C17 178.01(12) . . . . ? C14 C15 C1 O1 176.66(12) . . . . ? C14 C15 C1 C2 -2.9(2) . . . . ? C14 C15 C16 C17 -0.4(2) . . . . ? C14 C11 C12 C17 -0.5(2) . . . . ? C14 C11 C12 C13 179.39(13) . . . . ? C2 C3 C4 C9 1.91(19) . . . . ? C2 C3 C4 C5 -178.78(12) . . . . ? C9 O1 C1 C15 -178.26(11) . . . . ? C9 O1 C1 C2 1.35(19) . . . . ? C9 C8 C7 C6 -1.1(2) . . . . ? C10 N1 C13 C21 -118.55(13) . . . . ? C10 N1 C13 C12 -0.04(16) . . . . ? C10 N1 C13 C20 118.40(13) . . . . ? C10 C11 C12 C17 -178.91(13) . . . . ? C10 C11 C12 C13 0.95(17) . . . . ? C16 C15 C1 O1 -1.80(18) . . . . ? C16 C15 C1 C2 178.62(13) . . . . ? C16 C15 C14 C11 0.3(2) . . . . ? C16 C17 C12 C11 0.3(2) . . . . ? C16 C17 C12 C13 -179.54(14) . . . . ? C13 N1 C10 C11 0.53(17) . . . . ? C13 N1 C10 C19 120.75(13) . . . . ? C13 N1 C10 C18 -117.23(13) . . . . ? C4 C3 C2 C1 -0.6(2) . . . . ? C4 C9 C8 C7 1.7(2) . . . . ? C4 C5 C6 C7 1.3(2) . . . . ? C8 C9 C4 C3 178.51(13) . . . . ? C8 C9 C4 C5 -0.8(2) . . . . ? C8 C7 C6 C5 -0.4(2) . . . . ? C21 C13 C12 C17 -63.95(19) . . . . ? C21 C13 C12 C11 116.20(14) . . . . ? C19 C10 C11 C14 63.32(19) . . . . ? C19 C10 C11 C12 -118.35(13) . . . . ? C12 C17 C16 C15 0.2(2) . . . . ? C6 C5 C4 C3 179.95(13) . . . . ? C6 C5 C4 C9 -0.7(2) . . . . ? C18 C10 C11 C14 -62.97(18) . . . . ? C18 C10 C11 C12 115.36(13) . . . . ? C20 C13 C12 C17 62.68(19) . . . . ? C20 C13 C12 C11 -117.17(13) . . . . ?