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Information card for entry 7160130
Preview
| Coordinates | 7160130.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C19 H21 N O5 |
|---|---|
| Calculated formula | C19 H21 N O5 |
| Title of publication | Brønsted acid-promoted synthesis of highly functionalized tetrahydrocarbazoles from diethyl (<i>E</i>)-5-diazo-4-oxohex-2-enedioate. |
| Authors of publication | Arunkumar, Vemula; Balamurugan, Rengarajan |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2024 |
| Journal volume | 22 |
| Journal issue | 47 |
| Pages of publication | 9214 - 9218 |
| a | 8.4646 ± 0.0007 Å |
| b | 21.096 ± 0.002 Å |
| c | 10.1483 ± 0.001 Å |
| α | 90° |
| β | 105.96 ± 0.004° |
| γ | 90° |
| Cell volume | 1742.3 ± 0.3 Å3 |
| Cell temperature | 288 ± 2 K |
| Ambient diffraction temperature | 288 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.089 |
| Residual factor for significantly intense reflections | 0.0676 |
| Weighted residual factors for significantly intense reflections | 0.1814 |
| Weighted residual factors for all reflections included in the refinement | 0.1976 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.0575 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 296687 (current) | 2024-12-06 | cif/ Updating files of 7160128, 7160129, 7160130 Original log message: Adding full bibliography for 7160128--7160130.cif. |
7160130.cif |
| 294353 | 2024-09-04 | cif/ Adding structures of 7160128, 7160129, 7160130 via cif-deposit CGI script. |
7160130.cif |
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Users of the data should acknowledge the original authors of the
structural data.