Crystallography Open Database

Information card for entry 7160140

Preview

Coordinates	7160140.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H37 N3 O2 S Si
Calculated formula	C26 H37 N3 O2 S Si
Title of publication	Facile access to α-silylmethylamidines by BF<sub>3</sub>-catalyzed hydroamination of silylynamides with amines.
Authors of publication	Lu, Fei; Li, Zengzeng; Wang, Yulu; Liu, Guoliang; Niu, Guangguo; Wang, Guanghui; Zhao, Ximei
Journal of publication	Organic & biomolecular chemistry
Year of publication	2024
Journal volume	22
Journal issue	40
Pages of publication	8097 - 8101
a	19.9676 ± 0.0006 Å
b	7.9854 ± 0.0002 Å
c	16.986 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	2708.41 ± 0.14 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	29
Hermann-Mauguin space group symbol	P c a 21
Hall space group symbol	P 2c -2ac
Residual factor for all reflections	0.0663
Residual factor for significantly intense reflections	0.0477
Weighted residual factors for significantly intense reflections	0.1196
Weighted residual factors for all reflections included in the refinement	0.1408
Goodness-of-fit parameter for all reflections included in the refinement	1.066
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
296697 (current)	2024-12-06	cif/ Updating files of 7160140 Original log message: Adding full bibliography for 7160140.cif.	7160140.cif
294726	2024-09-12	cif/ Adding structures of 7160140 via cif-deposit CGI script.	7160140.cif