Crystallography Open Database

Information card for entry 7201040

7201039 << 7201040 >> 7201041

Preview

Coordinates	7201040.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H70 Ge Mo12 N11 Ni4 O47
Calculated formula	C27 H56 Ge Mo12 N11 Ni4 O45
Title of publication	The first ε-Keggin core of molybdogermanate in extended architectures of nickel(II) with N-donor ligands: syntheses, crystal structures and magnetic properties
Authors of publication	Wang, Wenju; Xu, Lin; Gao, Guanggang; Liu, Li; Liu, Xizheng
Journal of publication	CrystEngComm
Year of publication	2009
Journal volume	11
Journal issue	11
Pages of publication	2488
a	14.544 ± 0.002 Å
b	15.039 ± 0.003 Å
c	18.655 ± 0.003 Å
α	112.528 ± 0.003°
β	106.237 ± 0.003°
γ	97.703 ± 0.002°
Cell volume	3482.3 ± 1 Å³
Cell temperature	273 ± 2 K
Ambient diffraction temperature	273 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1017
Residual factor for significantly intense reflections	0.0574
Weighted residual factors for significantly intense reflections	0.129
Weighted residual factors for all reflections included in the refinement	0.1551
Goodness-of-fit parameter for all reflections included in the refinement	1.004
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180341 (current)	2016-03-26	cif/7/20/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/20/10.	7201040.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7201040.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7201040.cif
1167	2010-05-13	cif/ Adding data from the rest of 2009 RSC journals, Inorg-Chem-2008 and Chem-Comm-2010_18-19.	7201040.cif