#------------------------------------------------------------------------------
#$Date: 2016-03-26 16:45:39 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180354 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/23/7202353.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7202353
loop_
_publ_author_name
'Kato, Masaru'
'Fujihara, Takashi'
'Yano, Daisaku'
'Nagasawa, Akira'
_publ_section_title
;
 Anion influence on the coordination polymer structures of silver(I)
 complexes with 2-methylisothiazol-3(2H)-one
;
_journal_issue                   10
_journal_name_full               CrystEngComm
_journal_page_first              1460
_journal_paper_doi               10.1039/b810652p
_journal_volume                  10
_journal_year                    2008
_chemical_formula_moiety         'C16 H16 Ag2 Cl6 N4 O12 S4'
_chemical_formula_sum            'C16 H16 Ag2 Cl6 N4 O12 S4'
_chemical_formula_weight         1013.05
_chemical_name_common
;bis(5-chloro-2-methylisothiazol-3(2H)-one)silver(i)
perchlorate
;
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                103.273(2)
_cell_angle_beta                 109.719(2)
_cell_angle_gamma                95.579(2)
_cell_formula_units_Z            2
_cell_length_a                   9.6984(6)
_cell_length_b                   13.2334(9)
_cell_length_c                   13.7678(9)
_cell_measurement_reflns_used    2033
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      24.76
_cell_measurement_theta_min      2.66
_cell_volume                     1589.25(18)
_computing_cell_refinement       SMART-W2K/NT
_computing_data_collection       'SMART-W2K/NT (Bruekr, 2003)'
_computing_data_reduction        'SAINT-W2K/NT (Bruker, 2003)'
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  SHELXTL-NT
_computing_structure_refinement  SHELXL-NT
_computing_structure_solution    'SHELXTL-NT (Bruker, 2003)'
_diffrn_ambient_temperature      173(2)
_diffrn_detector_area_resol_mean 8.366
_diffrn_measured_fraction_theta_full 0.991
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'Bruker SMART APEX CCD area-detector'
_diffrn_measurement_method       'φ and ω'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0339
_diffrn_reflns_av_sigmaI/netI    0.0752
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            11716
_diffrn_reflns_theta_full        27.89
_diffrn_reflns_theta_max         27.89
_diffrn_reflns_theta_min         1.61
_diffrn_standards_decay_%        2
_diffrn_standards_interval_time  150
_diffrn_standards_number         60
_exptl_absorpt_coefficient_mu    2.061
_exptl_absorpt_correction_T_max  0.8204
_exptl_absorpt_correction_T_min  0.6833
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Sheldrick 1996)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.117
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    .
_exptl_crystal_description       needle
_exptl_crystal_F_000             992
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.911
_refine_diff_density_min         -0.664
_refine_diff_density_rms         0.146
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.015
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     404
_refine_ls_number_reflns         7529
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.015
_refine_ls_R_factor_all          0.0874
_refine_ls_R_factor_gt           0.0576
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0570P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1172
_refine_ls_wR_factor_ref         0.1304
_reflns_number_gt                5382
_reflns_number_total             7529
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            b810652p.txt
_cod_data_source_block           fuji_agcmi100
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7202353
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag -0.01331(5) 0.42809(4) 0.23171(3) 0.03123(13) Uani 1 1 d . . .
Ag2 Ag 0.0000 0.5000 0.0000 0.03141(16) Uani 1 2 d S . .
Ag3 Ag 0.0000 0.5000 0.5000 0.04015(19) Uani 1 2 d S . .
C1 C 0.1752(6) 0.3154(5) 0.0941(4) 0.0255(12) Uani 1 1 d . . .
C2 C 0.1274(6) 0.2085(5) 0.0908(4) 0.0292(13) Uani 1 1 d . . .
H2 H 0.0467 0.1864 0.1103 0.035 Uiso 1 1 calc R . .
C3 C 0.2094(6) 0.1434(5) 0.0573(4) 0.0298(13) Uani 1 1 d . . .
C4 C 0.3718(6) 0.4208(5) 0.0596(5) 0.0328(14) Uani 1 1 d . . .
H1A H 0.3110 0.4440 -0.0010 0.049 Uiso 1 1 calc R . .
H1B H 0.4665 0.4095 0.0522 0.049 Uiso 1 1 calc R . .
H1C H 0.3915 0.4751 0.1270 0.049 Uiso 1 1 calc R . .
C5 C -0.0707(6) 0.6734(4) 0.1860(4) 0.0248(12) Uani 1 1 d . . .
C6 C 0.0035(6) 0.7716(5) 0.1853(4) 0.0277(12) Uani 1 1 d . . .
H14 H 0.0783 0.7770 0.1556 0.033 Uiso 1 1 calc R . .
C7 C -0.0425(6) 0.8541(5) 0.2301(4) 0.0297(13) Uani 1 1 d . . .
C8 C -0.2711(7) 0.6106(5) 0.2480(5) 0.0405(15) Uani 1 1 d . . .
H16A H -0.2703 0.5409 0.2046 0.061 Uiso 1 1 calc R . .
H16B H -0.3730 0.6245 0.2257 0.061 Uiso 1 1 calc R . .
H16C H -0.2356 0.6122 0.3241 0.061 Uiso 1 1 calc R . .
C9 C 0.1712(6) 0.6782(5) 0.4168(4) 0.0274(12) Uani 1 1 d . . .
C10 C 0.1411(7) 0.7775(5) 0.4698(5) 0.0352(14) Uani 1 1 d . . .
H10 H 0.0669 0.7822 0.5005 0.042 Uiso 1 1 calc R . .
C11 C 0.2286(7) 0.8594(5) 0.4699(5) 0.0396(15) Uani 1 1 d . . .
C12 C 0.3408(7) 0.6183(6) 0.3240(5) 0.0445(17) Uani 1 1 d . . .
H12A H 0.3126 0.5501 0.3353 0.067 Uiso 1 1 calc R . .
H12B H 0.4498 0.6376 0.3503 0.067 Uiso 1 1 calc R . .
H12C H 0.2987 0.6130 0.2471 0.067 Uiso 1 1 calc R . .
C13 C -0.2622(6) 0.3080(5) 0.2971(4) 0.0261(12) Uani 1 1 d . . .
C14 C -0.2591(6) 0.2022(5) 0.2424(5) 0.0307(13) Uani 1 1 d . . .
H6 H -0.1861 0.1846 0.2129 0.037 Uiso 1 1 calc R . .
C15 C -0.3716(6) 0.1309(5) 0.2379(4) 0.0300(13) Uani 1 1 d . . .
C16 C -0.4221(7) 0.4030(5) 0.3795(5) 0.0377(15) Uani 1 1 d . . .
H8A H -0.3446 0.4369 0.4506 0.057 Uiso 1 1 calc R . .
H8B H -0.5174 0.3844 0.3872 0.057 Uiso 1 1 calc R . .
H8C H -0.4318 0.4519 0.3349 0.057 Uiso 1 1 calc R . .
Cl1 Cl 0.20076(18) 0.01141(13) 0.04372(14) 0.0435(4) Uani 1 1 d . . .
Cl2 Cl 0.0143(2) 0.98539(13) 0.24840(14) 0.0489(4) Uani 1 1 d . . .
Cl3 Cl 0.2356(3) 0.99077(15) 0.52233(16) 0.0698(6) Uani 1 1 d . . .
Cl4 Cl -0.41268(19) -0.00193(13) 0.18043(15) 0.0498(4) Uani 1 1 d . . .
Cl5 Cl 0.30670(15) 0.70617(11) 0.03344(11) 0.0279(3) Uani 1 1 d . . .
Cl6 Cl 0.20276(16) 0.29471(13) 0.41666(12) 0.0349(3) Uani 1 1 d . . .
N1 N 0.2916(5) 0.3218(4) 0.0608(4) 0.0247(10) Uani 1 1 d . . .
N2 N -0.1741(5) 0.6910(4) 0.2328(4) 0.0281(10) Uani 1 1 d . . .
N3 N 0.2838(5) 0.6984(4) 0.3819(4) 0.0309(11) Uani 1 1 d . . .
N4 N -0.3808(5) 0.3071(4) 0.3285(4) 0.0291(11) Uani 1 1 d . . .
O1 O 0.1234(4) 0.3955(3) 0.1221(3) 0.0299(9) Uani 1 1 d . . .
O2 O -0.0525(4) 0.5816(3) 0.1521(3) 0.0319(9) Uani 1 1 d . . .
O3 O 0.1057(5) 0.5865(3) 0.4011(3) 0.0353(10) Uani 1 1 d . . .
O4 O -0.1739(4) 0.3922(3) 0.3169(3) 0.0325(9) Uani 1 1 d . . .
O5 O 0.2249(5) 0.6514(4) 0.0808(4) 0.0586(14) Uani 1 1 d . . .
O6 O 0.2894(5) 0.6404(4) -0.0701(3) 0.0490(12) Uani 1 1 d . . .
O7 O 0.4592(5) 0.7306(5) 0.0999(4) 0.0743(19) Uani 1 1 d . . .
O8 O 0.2502(8) 0.7975(5) 0.0212(5) 0.096(2) Uani 1 1 d . . .
O9 O 0.1555(9) 0.3523(6) 0.4920(5) 0.104(3) Uani 1 1 d . . .
O10 O 0.2194(7) 0.3644(6) 0.3515(6) 0.093(2) Uani 1 1 d . . .
O11 O 0.3392(6) 0.2671(6) 0.4610(5) 0.090(2) Uani 1 1 d . . .
O12 O 0.0944(9) 0.2127(6) 0.3454(8) 0.145(4) Uani 1 1 d . . .
S1 S 0.34491(16) 0.20544(12) 0.02458(11) 0.0283(3) Uani 1 1 d . . .
S2 S -0.18048(17) 0.82046(12) 0.27626(12) 0.0331(3) Uani 1 1 d . . .
S3 S 0.35293(18) 0.82795(14) 0.40765(13) 0.0406(4) Uani 1 1 d . . .
S4 S -0.48541(16) 0.18639(12) 0.29819(12) 0.0316(3) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O4 Ag1 O1 158.43(14) . . ?
O4 Ag1 O2 114.87(13) . . ?
O1 Ag1 O2 81.27(13) . . ?
O4 Ag1 O3 82.56(13) . . ?
O1 Ag1 O3 115.92(13) . . ?
O2 Ag1 O3 78.65(12) . . ?
O2 Ag2 O2 179.999(1) 2_565 . ?
O2 Ag2 O1 98.94(13) 2_565 . ?
O2 Ag2 O1 81.06(13) . . ?
O2 Ag2 O1 81.06(13) 2_565 2_565 ?
O2 Ag2 O1 98.94(13) . 2_565 ?
O1 Ag2 O1 180.0 . 2_565 ?
O2 Ag2 O5 96.32(14) 2_565 . ?
O2 Ag2 O5 83.68(14) . . ?
O1 Ag2 O5 93.01(15) . . ?
O1 Ag2 O5 86.99(15) 2_565 . ?
O2 Ag2 O5 83.68(14) 2_565 2_565 ?
O2 Ag2 O5 96.32(14) . 2_565 ?
O1 Ag2 O5 86.98(15) . 2_565 ?
O1 Ag2 O5 93.01(15) 2_565 2_565 ?
O5 Ag2 O5 180.0 . 2_565 ?
O3 Ag3 O3 180.00(11) . 2_566 ?
O3 Ag3 O4 96.92(13) . 2_566 ?
O3 Ag3 O4 83.08(13) 2_566 2_566 ?
O3 Ag3 O4 83.08(13) . . ?
O3 Ag3 O4 96.92(13) 2_566 . ?
O4 Ag3 O4 180.0 2_566 . ?
O3 Ag3 O9 93.4(2) . . ?
O3 Ag3 O9 86.6(2) 2_566 . ?
O4 Ag3 O9 94.11(19) 2_566 . ?
O4 Ag3 O9 85.89(19) . . ?
O3 Ag3 O9 86.6(2) . 2_566 ?
O3 Ag3 O9 93.4(2) 2_566 2_566 ?
O4 Ag3 O9 85.89(19) 2_566 2_566 ?
O4 Ag3 O9 94.11(19) . 2_566 ?
O9 Ag3 O9 179.998(2) . 2_566 ?
O1 C1 N1 121.4(5) . . ?
O1 C1 C2 128.6(5) . . ?
N1 C1 C2 110.1(5) . . ?
C3 C2 C1 112.2(5) . . ?
C3 C2 H2 123.9 . . ?
C1 C2 H2 123.9 . . ?
C2 C3 Cl1 130.1(5) . . ?
C2 C3 S1 113.4(5) . . ?
Cl1 C3 S1 116.5(3) . . ?
N1 C4 H1A 109.5 . . ?
N1 C4 H1B 109.5 . . ?
H1A C4 H1B 109.5 . . ?
N1 C4 H1C 109.5 . . ?
H1A C4 H1C 109.5 . . ?
H1B C4 H1C 109.5 . . ?
O2 C5 N2 120.6(5) . . ?
O2 C5 C6 129.5(5) . . ?
N2 C5 C6 109.9(5) . . ?
C7 C6 C5 113.1(5) . . ?
C7 C6 H14 123.5 . . ?
C5 C6 H14 123.5 . . ?
C6 C7 Cl2 129.7(5) . . ?
C6 C7 S2 113.4(5) . . ?
Cl2 C7 S2 116.9(3) . . ?
N2 C8 H16A 109.5 . . ?
N2 C8 H16B 109.5 . . ?
H16A C8 H16B 109.5 . . ?
N2 C8 H16C 109.5 . . ?
H16A C8 H16C 109.5 . . ?
H16B C8 H16C 109.5 . . ?
O3 C9 N3 122.5(5) . . ?
O3 C9 C10 127.8(6) . . ?
N3 C9 C10 109.7(5) . . ?
C11 C10 C9 111.8(6) . . ?
C11 C10 H10 124.1 . . ?
C9 C10 H10 124.1 . . ?
C10 C11 Cl3 129.0(6) . . ?
C10 C11 S3 114.4(5) . . ?
Cl3 C11 S3 116.6(4) . . ?
N3 C12 H12A 109.5 . . ?
N3 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
N3 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
O4 C13 N4 121.2(5) . . ?
O4 C13 C14 129.0(5) . . ?
N4 C13 C14 109.8(5) . . ?
C15 C14 C13 112.1(5) . . ?
C15 C14 H6 123.9 . . ?
C13 C14 H6 123.9 . . ?
C14 C15 Cl4 128.5(5) . . ?
C14 C15 S4 113.2(5) . . ?
Cl4 C15 S4 118.3(4) . . ?
N4 C16 H8A 109.5 . . ?
N4 C16 H8B 109.5 . . ?
H8A C16 H8B 109.5 . . ?
N4 C16 H8C 109.5 . . ?
H8A C16 H8C 109.5 . . ?
H8B C16 H8C 109.5 . . ?
O8 Cl5 O7 111.4(4) . . ?
O8 Cl5 O5 108.5(4) . . ?
O7 Cl5 O5 109.1(3) . . ?
O8 Cl5 O6 109.2(3) . . ?
O7 Cl5 O6 108.8(3) . . ?
O5 Cl5 O6 109.9(3) . . ?
O12 Cl6 O9 111.6(5) . . ?
O12 Cl6 O11 114.1(5) . . ?
O9 Cl6 O11 113.4(4) . . ?
O12 Cl6 O10 103.4(5) . . ?
O9 Cl6 O10 105.3(4) . . ?
O11 Cl6 O10 107.9(4) . . ?
C1 N1 C4 124.1(5) . . ?
C1 N1 S1 114.8(4) . . ?
C4 N1 S1 121.1(4) . . ?
C5 N2 C8 126.0(5) . . ?
C5 N2 S2 113.9(4) . . ?
C8 N2 S2 120.0(4) . . ?
C9 N3 C12 124.6(5) . . ?
C9 N3 S3 114.9(4) . . ?
C12 N3 S3 120.5(4) . . ?
C13 N4 C16 123.5(5) . . ?
C13 N4 S4 115.0(4) . . ?
C16 N4 S4 121.4(4) . . ?
C1 O1 Ag1 130.4(4) . . ?
C1 O1 Ag2 124.5(3) . . ?
Ag1 O1 Ag2 95.77(13) . . ?
C5 O2 Ag2 131.6(4) . . ?
C5 O2 Ag1 133.9(3) . . ?
Ag2 O2 Ag1 93.77(13) . . ?
C9 O3 Ag3 134.9(4) . . ?
C9 O3 Ag1 132.6(3) . . ?
Ag3 O3 Ag1 91.54(14) . . ?
C13 O4 Ag1 128.3(4) . . ?
C13 O4 Ag3 125.2(3) . . ?
Ag1 O4 Ag3 94.91(13) . . ?
Cl5 O5 Ag2 132.3(3) . . ?
Cl6 O9 Ag3 135.9(4) . . ?
N1 S1 C3 89.4(3) . . ?
N2 S2 C7 89.7(3) . . ?
N3 S3 C11 89.3(3) . . ?
N4 S4 C15 89.9(3) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 O4 2.318(4) . ?
Ag1 O1 2.320(4) . ?
Ag1 O2 2.522(4) . ?
Ag1 O3 2.575(4) . ?
Ag2 O2 2.366(4) 2_565 ?
Ag2 O2 2.366(4) . ?
Ag2 O1 2.490(4) . ?
Ag2 O1 2.490(4) 2_565 ?
Ag2 O5 2.549(5) . ?
Ag2 O5 2.549(5) 2_565 ?
Ag3 O3 2.376(4) . ?
Ag3 O3 2.376(4) 2_566 ?
Ag3 O4 2.499(4) 2_566 ?
Ag3 O4 2.499(4) . ?
Ag3 O9 2.587(7) . ?
Ag3 O9 2.587(7) 2_566 ?
C1 O1 1.254(6) . ?
C1 N1 1.357(7) . ?
C1 C2 1.430(8) . ?
C2 C3 1.337(8) . ?
C2 H2 0.9500 . ?
C3 Cl1 1.704(6) . ?
C3 S1 1.721(6) . ?
C4 N1 1.462(7) . ?
C4 H1A 0.9800 . ?
C4 H1B 0.9800 . ?
C4 H1C 0.9800 . ?
C5 O2 1.250(6) . ?
C5 N2 1.374(7) . ?
C5 C6 1.426(8) . ?
C6 C7 1.320(8) . ?
C6 H14 0.9500 . ?
C7 Cl2 1.705(6) . ?
C7 S2 1.727(6) . ?
C8 N2 1.449(7) . ?
C8 H16A 0.9800 . ?
C8 H16B 0.9800 . ?
C8 H16C 0.9800 . ?
C9 O3 1.250(7) . ?
C9 N3 1.360(7) . ?
C9 C10 1.457(8) . ?
C10 C11 1.310(9) . ?
C10 H10 0.9500 . ?
C11 Cl3 1.707(7) . ?
C11 S3 1.730(7) . ?
C12 N3 1.445(8) . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 O4 1.252(7) . ?
C13 N4 1.359(7) . ?
C13 C14 1.438(8) . ?
C14 C15 1.346(8) . ?
C14 H6 0.9500 . ?
C15 Cl4 1.699(6) . ?
C15 S4 1.716(6) . ?
C16 N4 1.464(7) . ?
C16 H8A 0.9800 . ?
C16 H8B 0.9800 . ?
C16 H8C 0.9800 . ?
Cl5 O8 1.397(5) . ?
Cl5 O7 1.409(5) . ?
Cl5 O5 1.427(5) . ?
Cl5 O6 1.434(4) . ?
Cl6 O12 1.356(7) . ?
Cl6 O9 1.376(6) . ?
Cl6 O11 1.381(5) . ?
Cl6 O10 1.460(6) . ?
N1 S1 1.692(5) . ?
N2 S2 1.695(5) . ?
N3 S3 1.688(5) . ?
N4 S4 1.688(5) . ?
