Crystallography Open Database

Information card for entry 7208197

7208196 << 7208197 >> 7208198

Preview

Coordinates	7208197.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[Ni(en)(tren)]4Sb14S25
Formula	C32 H104 N24 Ni4 S25 Sb14
Calculated formula	C32 H104 N24 Ni4 S25 Sb14
Title of publication	Using a Ni2+ complex as a structure-directing molecule: solvothermal synthesis and properties of [Ni(en)(tren)]4Sb14S25 featuring an unprecedented three-dimensional network architecture
Authors of publication	Seidlhofer, Beatrix; Näther, Christian; Bensch, Wolfgang
Journal of publication	CrystEngComm
Year of publication	2012
Journal volume	14
Journal issue	17
Pages of publication	5441
a	16.5428 ± 0.0003 Å
b	25.8974 ± 0.0004 Å
c	22.5225 ± 0.0004 Å
α	90°
β	98.881 ± 0.001°
γ	90°
Cell volume	9533.3 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0469
Residual factor for significantly intense reflections	0.0357
Weighted residual factors for significantly intense reflections	0.0763
Weighted residual factors for all reflections included in the refinement	0.08
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180412 (current)	2016-03-26	cif/7/20/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/20/81.	7208197.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7208197.cif
64217	2012-08-11	cif/ Adding structures of 7208197 via cif-deposit CGI script.	7208197.cif