Crystallography Open Database

Information card for entry 7208683

7208682 << 7208683 >> 7208684

Preview

Coordinates	7208683.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	(Ni(Ni(bpy)(solv))8(W(CN)8)6).11H2O
Chemical name	{Ni[Ni(bpy)(solv)]8[W(CN)8]6}.11H2O
Formula	C134.4 H114.8 N64 Ni9 O19 W6
Calculated formula	C134.4 H80 N64 Ni9 O19 W6
Title of publication	Geometrical isomerism in pentadecanuclear high-spin Ni9W6 clusters with symmetrical bidentate ligands detected
Authors of publication	Nowicka, Beata; Stadnicka, Katarzyna; Nitek, Wojciech; Rams, Michał; Sieklucka, Barbara
Journal of publication	CrystEngComm
Year of publication	2012
Journal volume	14
Journal issue	20
Pages of publication	6559
a	18.4747 ± 0.0011 Å
b	18.5055 ± 0.0012 Å
c	27.732 ± 0.002 Å
α	84.222 ± 0.003°
β	85.211 ± 0.004°
γ	87.182 ± 0.003°
Cell volume	9392.1 ± 1.1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1432
Residual factor for significantly intense reflections	0.1125
Weighted residual factors for significantly intense reflections	0.2804
Weighted residual factors for all reflections included in the refinement	0.304
Goodness-of-fit parameter for all reflections included in the refinement	1.141
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7208683.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7208683.cif
71452	2013-01-20	cif/ Adding structures of 7208682, 7208683, 7208684, 7208685, 7208686, 7208687, 7208688 via cif-deposit CGI script.	7208683.cif