Crystallography Open Database

Information card for entry 7210305

Preview

Coordinates	7210305.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C10 H104 As4 N2 Na10 O199 Tb6 W44
Calculated formula	C10 H18 As4 N2 Na10 O199 Tb6 W44
Title of publication	Assembly of chainlike polyoxometalate-based lanthanide complexes in one-pot reaction system
Authors of publication	Feng, Xiao-Jia; Han, Hua-Yan; Wang, Yong-Hui; Li, Lu-Lu; Li, Yang-Guang; Wang, En-Bo
Journal of publication	CrystEngComm
Year of publication	2013
Journal volume	15
Journal issue	36
Pages of publication	7267
a	13.085 ± 0.003 Å
b	19.689 ± 0.004 Å
c	22.821 ± 0.005 Å
α	104.33 ± 0.03°
β	95.37 ± 0.03°
γ	104.76 ± 0.03°
Cell volume	5431 ± 2 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1438
Residual factor for significantly intense reflections	0.0865
Weighted residual factors for significantly intense reflections	0.1569
Weighted residual factors for all reflections included in the refinement	0.1729
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180434 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/03.	7210305.cif
87593	2013-08-27	cif/ Adding structures of 7210305, 7210306, 7210307 via cif-deposit CGI script.	7210305.cif