Crystallography Open Database

Information card for entry 7212776

Preview

Coordinates	7212776.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	H150 K12 O239 P6 Rb6 V8 W39
Calculated formula	K11.982 O203 P6 Rb6 V8 W39
Title of publication	Mixed-valent vanadium substituted polyoxometalates: the wheel shaped [Rb3⊂{VVVIV3O7(H2O)6}2{H6P6W39O147(H2O)3}]15−
Authors of publication	Assran, Awatef S.; Izarova, Natalya V.; Kortz, Ulrich
Journal of publication	CrystEngComm
Year of publication	2010
Journal volume	12
Journal issue	10
Pages of publication	2684
a	22.9885 ± 0.0013 Å
b	22.9885 ± 0.0013 Å
c	21.3679 ± 0.0014 Å
α	90°
β	90°
γ	120°
Cell volume	9779.4 ± 1 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	190
Hermann-Mauguin space group symbol	P -6 2 c
Hall space group symbol	P -6c -2c
Residual factor for all reflections	0.0574
Residual factor for significantly intense reflections	0.045
Weighted residual factors for significantly intense reflections	0.105
Weighted residual factors for all reflections included in the refinement	0.1128
Goodness-of-fit parameter for all reflections included in the refinement	1.104
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180458 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/27.	7212776.cif
93273	2014-01-12	cif/ Adding structures of 7212776 via cif-deposit CGI script.	7212776.cif