Crystallography Open Database

Information card for entry 7213289

Preview

Coordinates	7213289.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	N,N-Dimethyl-diindole[3,2-a;2,3-c]N-methylcarbazole
Formula	C27 H21 N3
Calculated formula	C27 H21 N3
Title of publication	Oxidative trimerization of indole: on the formation of dications and radical cations by reaction of indole and nitrosobenzene in the presence of acids
Authors of publication	Greci, Lucedio; Tommasi, Giampaolo; Petrucci, Rita; Marrosu, Giancarlo; Trazza, Antonio; Sgarabotto, Paolo; Righi, Lara; Alberti, Angelo
Journal of publication	Journal of the Chemical Society, Perkin Transactions 2
Year of publication	2000
Journal issue	11
Pages of publication	2337
a	22.465 ± 0.004 Å
b	8.017 ± 0.002 Å
c	21.376 ± 0.004 Å
α	90°
β	100.1 ± 0.1°
γ	90°
Cell volume	3790.2 ± 1.8 Å³
Cell temperature	298 K
Ambient diffraction temperature	298 K
Number of distinct elements	3
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.049
Weighted residual factors for all reflections included in the refinement	0.054
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	X
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7213289.cif
96018	2014-01-28	cif/ Adding structures of 7213289 via cif-deposit CGI script.	7213289.cif