Crystallography Open Database

Information card for entry 7213592

Preview

Coordinates	7213592.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H239 Fe6 Ge6 K9 N26 O282 Sm6 W60
Calculated formula	C12 H60 Fe6 Ge6 K9 N12 O282 Sm6 W60
Title of publication	Syntheses, structures and properties of two multi-iron‒samarium/multi-iron substituted germanotungstates
Authors of publication	Wang, Jun; Zhao, Jun-Wei; Zhao, Hai-Yan; Yang, Bai-Feng; He, Huan; Yang, Guo-Yu
Journal of publication	CrystEngComm
Year of publication	2014
Journal volume	16
Journal issue	2
Pages of publication	252
a	20.8479 ± 0.0005 Å
b	35.6759 ± 0.0009 Å
c	38.2974 ± 0.0008 Å
α	90°
β	92.107 ± 0.002°
γ	90°
Cell volume	28465.1 ± 1.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	9
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0795
Residual factor for significantly intense reflections	0.0491
Weighted residual factors for significantly intense reflections	0.1024
Weighted residual factors for all reflections included in the refinement	0.1127
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180466 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/35.	7213592.cif
105131	2014-03-11	cif/ Adding structures of 7213592, 7213593 via cif-deposit CGI script.	7213592.cif