Crystallography Open Database

Information card for entry 7214286

Preview

Coordinates	7214286.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C15.1 H33.38 Al4 Na3 O15.1
Calculated formula	C15.095 H33.38 Al4 Na3 O15.095
Title of publication	One-pot Solvothermal Synthesis of Well-ordered Layered Sodium Aluminoalcoholate Complex: A Useful Precursor for the Preparation of Porous Al2O3 Particles.
Authors of publication	Li, Xiansen; Michaelis, Vladimir K.; Ong, Ta-Chung; Smith, Stacey J.; McKay, Ian; Müller, Peter; Griffin, Robert G.; Wang, Evelyn N.
Journal of publication	CrystEngComm / RSC
Year of publication	2014
Journal volume	16
Journal issue	14
Pages of publication	2950 - 2958
a	11.2481 ± 0.0012 Å
b	13.1877 ± 0.0014 Å
c	18.235 ± 0.002 Å
α	90°
β	105.738 ± 0.002°
γ	90°
Cell volume	2603.5 ± 0.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0633
Residual factor for significantly intense reflections	0.0405
Weighted residual factors for significantly intense reflections	0.0994
Weighted residual factors for all reflections included in the refinement	0.111
Goodness-of-fit parameter for all reflections included in the refinement	1.046
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7214286.cif
116200	2014-06-07	cif/ Updating files of 7214286 Original log message: Adding full bibliography for 7214286.cif.	7214286.cif
108280	2014-03-30	cif/ Adding structures of 7214286 via cif-deposit CGI script.	7214286.cif