Crystallography Open Database

Information card for entry 7215632

Preview

Coordinates	7215632.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C84 H68 N8 Ni4 O24
Calculated formula	C84 H68 N8 Ni4 O24
Title of publication	Four-, and six-connected entangled frameworks based on flexible bis(imidazole) ligands and long dicarboxylate anions
Authors of publication	Yang, Jin; Ma, Jian-Fang; Liu, Ying-Ying; Batten, Stuart R.
Journal of publication	CrystEngComm
Year of publication	2009
Journal volume	11
Journal issue	1
Pages of publication	151 - 159
a	28.442 ± 0.003 Å
b	5.7468 ± 0.0006 Å
c	24.666 ± 0.003 Å
α	90°
β	112.039 ± 0.002°
γ	90°
Cell volume	3737.1 ± 0.7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0547
Residual factor for significantly intense reflections	0.0414
Weighted residual factors for significantly intense reflections	0.09
Weighted residual factors for all reflections included in the refinement	0.0962
Goodness-of-fit parameter for all reflections included in the refinement	1.022
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Duplicate of	7200486
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
218471 (current)	2019-09-18	cif/7/21/56/ Marked entries 7215627-7215632 as duplicates of entries 7200481-7200486.	7215632.cif
218470	2019-09-18	cif/7/21/56/ Updated bibliographic information in entries 7215627-7215632.	7215632.cif
180487	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/56.	7215632.cif
112539	2014-05-02	cif/ Adding structures of 7215627, 7215628, 7215629, 7215630, 7215631, 7215632 via cif-deposit CGI script.	7215632.cif