#------------------------------------------------------------------------------
#$Date: 2023-11-10 21:21:08 +0200 (Fri, 10 Nov 2023) $
#$Revision: 287519 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/21/56/7215647.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7215647
loop_
_publ_author_name
'Alekseev, Evgeny V.'
'Krivovichev, Sergey V.'
'Depmeier, Wulf'
_publ_section_title
;
 Novel layered uranyl arsenates, Ag6[(UO2)2(As2O7)(As4O13)] and
 AI6[(UO2)2(AsO4)2(As2O7)] (AI--Ag and Na): first observation of a linear
 As4O136− anion and structure type evolution
;
_journal_issue                   17
_journal_name_full               'Journal of Materials Chemistry'
_journal_page_first              2583
_journal_paper_doi               10.1039/b818757f
_journal_volume                  19
_journal_year                    2009
_chemical_formula_sum            'Ag6 As4 O19 U2'
_chemical_formula_weight         1726.96
_chemical_name_systematic
;
hexasilver diauranyl diortoarsenato diarsenate 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                108.69(8)
_cell_angle_beta                 91.94(7)
_cell_angle_gamma                97.63(6)
_cell_formula_units_Z            4
_cell_length_a                   11.218(3)
_cell_length_b                   11.729(3)
_cell_length_c                   14.146(4)
_cell_measurement_reflns_used    135
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      16
_cell_measurement_theta_min      12
_cell_volume                     1741.7(12)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Stoe Stadi4'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1739
_diffrn_reflns_av_sigmaI/netI    0.2527
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            13754
_diffrn_reflns_theta_full        26.02
_diffrn_reflns_theta_max         26.02
_diffrn_reflns_theta_min         1.52
_exptl_absorpt_coefficient_mu    32.760
_exptl_absorpt_correction_T_max  0.147
_exptl_absorpt_correction_T_min  0.055
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   ShelxA
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    6.585
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             3000
_exptl_crystal_size_max          0.11
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.06
_refine_diff_density_max         3.321
_refine_diff_density_min         -2.405
_refine_diff_density_rms         0.529
_refine_ls_extinction_coef       0.000059(15)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.905
_refine_ls_matrix_type           full
_refine_ls_number_parameters     383
_refine_ls_number_reflns         6877
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.905
_refine_ls_R_factor_all          0.2100
_refine_ls_R_factor_gt           0.0669
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0483P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1039
_refine_ls_wR_factor_ref         0.1365
_reflns_number_gt                2721
_reflns_number_total             6877
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b818757f.txt
_cod_data_source_block           O19As4Ag6U2
_cod_original_cell_volume        1741.8(9)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7215647
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
U1 U 0.75793(9) 0.07725(8) 0.09068(7) 0.0188(3) Uani 1 1 d .
U2 U 0.76564(9) 0.07009(8) 0.58021(7) 0.0191(3) Uani 1 1 d .
U3 U 0.73728(10) -0.49477(8) -0.05577(8) 0.0221(3) Uani 1 1 d .
U4 U 0.75032(11) -0.49353(8) -0.54603(8) 0.0280(3) Uani 1 1 d .
As1 As 0.7641(2) -0.2073(2) 0.15648(19) 0.0184(7) Uani 1 1 d .
As2 As 0.7680(3) -0.2116(2) -0.1195(2) 0.0213(7) Uani 1 1 d .
As3 As 0.7792(3) -0.2181(2) 0.3773(2) 0.0201(7) Uani 1 1 d .
As4 As 0.7461(2) -0.8274(2) -0.13942(19) 0.0176(6) Uani 1 1 d .
As5 As 0.7869(2) -0.2008(2) -0.3383(2) 0.0192(7) Uani 1 1 d .
As6 As 0.7472(2) 0.4092(2) 0.1702(2) 0.0191(7) Uani 1 1 d .
As7 As 0.7052(2) -0.8266(2) -0.6429(2) 0.0196(6) Uani 1 1 d .
As8 As 0.7169(3) -0.6113(2) -0.3341(2) 0.0221(7) Uani 1 1 d .
Ag1 Ag 0.9807(2) -0.67829(18) 0.03126(17) 0.0299(6) Uani 1 1 d .
Ag2 Ag 0.5056(2) -0.7585(2) -0.00128(18) 0.0347(6) Uani 1 1 d .
Ag3 Ag 0.4886(2) -0.7598(2) -0.50410(19) 0.0402(7) Uani 1 1 d .
Ag4 Ag 1.0339(2) -0.3081(2) -0.5168(2) 0.0461(7) Uani 1 1 d .
Ag5 Ag 1.0047(2) -0.35718(18) 0.20599(19) 0.0349(6) Uani 1 1 d .
Ag6 Ag 0.5532(2) -1.07813(17) -0.20221(16) 0.0292(5) Uani 1 1 d .
Ag7 Ag 0.5485(2) 0.59480(18) 0.20883(17) 0.0303(6) Uani 1 1 d .
Ag8 Ag 0.9451(2) -0.96365(19) -0.65894(19) 0.0370(6) Uani 1 1 d .
Ag9 Ag 0.4900(2) -0.86944(18) -0.3049(2) 0.0400(7) Uani 1 1 d .
Ag10 Ag 0.9768(2) -0.95656(19) -0.1064(2) 0.0419(7) Uani 1 1 d .
Ag11 Ag 0.9705(3) -0.3857(2) -0.2832(2) 0.0571(8) Uani 1 1 d .
Ag12 Ag 0.4748(3) -0.6215(2) -0.7009(2) 0.0529(8) Uani 1 1 d .
O1 O 0.6717(17) -0.7071(14) -0.0970(14) 0.029(4) Uiso 1 1 d .
O2 O 0.8429(16) -0.0751(14) 0.4406(13) 0.025(4) Uiso 1 1 d .
O3 O 0.8276(15) -0.2464(13) 0.2540(12) 0.019(4) Uiso 1 1 d .
O4 O 0.6324(16) -0.2456(14) 0.3654(13) 0.025(4) Uiso 1 1 d .
O5 O 0.6906(17) 0.4622(15) 0.2812(14) 0.029(4) Uiso 1 1 d .
O6 O 0.8014(15) -0.8499(13) -0.5598(12) 0.022(4) Uiso 1 1 d .
O7 O 0.8146(15) -0.3443(13) -0.1356(13) 0.022(4) Uiso 1 1 d .
O8 O 0.8982(16) 0.4361(13) 0.1832(13) 0.022(4) Uiso 1 1 d .
O9 O 0.8815(18) -0.5251(15) -0.0455(14) 0.033(5) Uiso 1 1 d .
O10 O 0.6572(16) -0.6906(14) -0.5970(13) 0.023(4) Uiso 1 1 d .
O11 O 0.8287(14) -0.0984(12) -0.0195(12) 0.017(3) Uiso 1 1 d .
O12 O 0.6412(18) -0.2211(16) -0.3476(15) 0.036(5) Uiso 1 1 d .
O13 O 0.6142(16) -0.2327(13) 0.1538(13) 0.021(4) Uiso 1 1 d .
O14 O 0.6988(15) -0.9042(12) -0.2589(12) 0.017(3) Uiso 1 1 d .
O15 O 0.6658(16) -0.7628(13) -0.3879(13) 0.023(4) Uiso 1 1 d .
O16 O 0.8230(14) -0.0598(12) 0.1774(11) 0.015(3) Uiso 1 1 d .
O17 O 0.6990(16) 0.4909(14) 0.1036(13) 0.022(4) Uiso 1 1 d .
O18 O 0.8263(14) -0.3044(12) 0.0644(12) 0.017(3) Uiso 1 1 d .
O19 O 0.8933(16) -0.7976(14) -0.1343(13) 0.028(4) Uiso 1 1 d .
O20 O 0.9165(15) 0.1434(13) 0.0918(12) 0.021(4) Uiso 1 1 d .
O21 O 0.8361(16) -0.1584(14) -0.2137(13) 0.024(4) Uiso 1 1 d .
O22 O 0.6197(16) -0.2264(13) -0.1335(13) 0.020(4) Uiso 1 1 d .
O23 O 0.7841(18) -0.8277(15) -0.7375(14) 0.036(5) Uiso 1 1 d .
O24 O 0.8531(15) -0.3274(13) -0.3934(12) 0.018(4) Uiso 1 1 d .
O25 O 0.9098(18) 0.1585(15) 0.6291(15) 0.033(5) Uiso 1 1 d .
O26 O 0.6267(14) -0.0166(12) 0.5303(11) 0.013(3) Uiso 1 1 d .
O27 O 0.8570(16) -0.0755(14) -0.3630(13) 0.025(4) Uiso 1 1 d .
O28 O 0.8456(17) -0.3209(15) 0.4164(14) 0.032(4) Uiso 1 1 d .
O29 O 0.7118(16) -0.9219(14) -0.0730(13) 0.025(4) Uiso 1 1 d .
O30 O 0.6904(16) 0.2627(14) 0.1141(13) 0.023(4) Uiso 1 1 d .
O31 O 0.6088(15) 0.0025(13) 0.0819(12) 0.021(4) Uiso 1 1 d .
O32 O 0.5829(17) -0.9322(14) -0.6721(13) 0.028(4) Uiso 1 1 d .
O33 O 0.5929(19) -0.4516(17) -0.0613(16) 0.041(5) Uiso 1 1 d .
O34 O 0.8960(18) -0.5450(16) -0.5704(15) 0.036(5) Uiso 1 1 d .
O35 O 0.609(2) -0.4390(18) -0.5272(17) 0.049(6) Uiso 1 1 d .
O36 O 0.805(3) -0.567(3) -0.417(3) 0.024(9) Uiso 0.453(19) 1 d P
O37 O 0.681(3) -0.525(2) -0.404(2) 0.016(7) Uiso 0.547(19) 1 d P
O38 O 0.776(3) -0.586(3) -0.232(2) 0.012(8) Uiso 0.453(19) 1 d P
O39 O 0.668(3) -0.558(2) -0.217(2) 0.019(7) Uiso 0.547(19) 1 d P
O40 O 0.869(5) -0.579(5) -0.325(4) 0.061(16) Uiso 0.453(19) 1 d P
O41 O 0.588(4) -0.545(3) -0.321(3) 0.047(11) Uiso 0.547(19) 1 d P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O31 U1 O20 175.1(6) . .
O31 U1 O23 98.8(7) . 1_566
O20 U1 O23 84.9(7) . 1_566
O31 U1 O30 91.3(7) . .
O20 U1 O30 92.7(6) . .
O23 U1 O30 76.3(6) 1_566 .
O31 U1 O29 85.8(7) . 1_565
O20 U1 O29 92.4(7) . 1_565
O23 U1 O29 151.7(6) 1_566 1_565
O30 U1 O29 75.7(6) . 1_565
O31 U1 O11 94.0(6) . .
O20 U1 O11 81.1(6) . .
O23 U1 O11 132.8(6) 1_566 .
O30 U1 O11 148.9(6) . .
O29 U1 O11 74.2(6) 1_565 .
O31 U1 O16 88.4(7) . .
O20 U1 O16 89.9(7) . .
O23 U1 O16 68.5(6) 1_566 .
O30 U1 O16 144.3(5) . .
O29 U1 O16 139.8(5) 1_565 .
O11 U1 O16 66.6(5) . .
O31 U1 Ag10 126.9(5) . 2_745
O20 U1 Ag10 49.6(5) . 2_745
O23 U1 Ag10 88.4(5) 1_566 2_745
O30 U1 Ag10 140.9(4) . 2_745
O29 U1 Ag10 111.2(4) 1_565 2_745
O11 U1 Ag10 49.1(4) . 2_745
O16 U1 Ag10 45.7(4) . 2_745
O31 U1 Ag10 129.2(5) . 1_565
O20 U1 Ag10 46.7(5) . 1_565
O23 U1 Ag10 131.3(5) 1_566 1_565
O30 U1 Ag10 106.8(4) . 1_565
O29 U1 Ag10 55.4(4) 1_565 1_565
O11 U1 Ag10 48.1(4) . 1_565
O16 U1 Ag10 100.8(4) . 1_565
Ag10 U1 Ag10 58.11(9) 2_745 1_565
O26 U2 O25 178.8(8) . .
O26 U2 O15 86.0(6) . 1_566
O25 U2 O15 94.4(7) . 1_566
O26 U2 O14 88.2(6) . 1_566
O25 U2 O14 92.9(7) . 1_566
O15 U2 O14 76.0(6) 1_566 1_566
O26 U2 O27 99.6(6) . 1_556
O25 U2 O27 80.6(7) . 1_556
O15 U2 O27 150.6(6) 1_566 1_556
O14 U2 O27 75.4(5) 1_566 1_556
O26 U2 O2 84.2(6) . .
O25 U2 O2 94.8(7) . .
O15 U2 O2 139.6(6) 1_566 .
O14 U2 O2 142.5(6) 1_566 .
O27 U2 O2 69.8(6) 1_556 .
O26 U2 O6 96.2(7) . 1_566
O25 U2 O6 82.9(8) . 1_566
O15 U2 O6 74.2(6) 1_566 1_566
O14 U2 O6 149.4(5) 1_566 1_566
O27 U2 O6 132.9(5) 1_556 1_566
O2 U2 O6 68.1(5) . 1_566
O26 U2 Ag9 57.1(4) . 1_566
O25 U2 Ag9 124.0(6) . 1_566
O15 U2 Ag9 48.7(4) 1_566 1_566
O14 U2 Ag9 44.6(4) 1_566 1_566
O27 U2 Ag9 111.1(4) 1_556 1_566
O2 U2 Ag9 141.2(4) . 1_566
O6 U2 Ag9 114.7(4) 1_566 1_566
O26 U2 Ag4 134.3(5) . 2_755
O25 U2 Ag4 45.0(7) . 2_755
O15 U2 Ag4 73.2(4) 1_566 2_755
O14 U2 Ag4 123.6(3) 1_566 2_755
O27 U2 Ag4 118.5(4) 1_556 2_755
O2 U2 Ag4 86.1(4) . 2_755
O6 U2 Ag4 39.4(4) 1_566 2_755
Ag9 U2 Ag4 121.57(7) 1_566 2_755
O9 U3 O33 175.6(8) . .
O9 U3 O39 109.8(10) . .
O33 U3 O39 72.7(10) . .
O9 U3 O17 92.1(8) . 1_545
O33 U3 O17 87.5(8) . 1_545
O39 U3 O17 144.5(9) . 1_545
O9 U3 O1 87.2(7) . .
O33 U3 O1 97.0(8) . .
O39 U3 O1 74.7(9) . .
O17 U3 O1 79.0(6) 1_545 .
O9 U3 O18 81.2(7) . .
O33 U3 O18 94.5(7) . .
O39 U3 O18 135.7(9) . .
O17 U3 O18 73.5(5) 1_545 .
O1 U3 O18 149.6(6) . .
O9 U3 O38 78.1(10) . .
O33 U3 O38 104.1(11) . .
O39 U3 O38 31.7(11) . .
O17 U3 O38 151.7(8) 1_545 .
O1 U3 O38 74.2(9) . .
O18 U3 O38 129.6(8) . .
O9 U3 O7 88.4(8) . .
O33 U3 O7 89.1(8) . .
O39 U3 O7 69.7(9) . .
O17 U3 O7 140.8(5) 1_545 .
O1 U3 O7 140.2(6) . .
O18 U3 O7 67.8(5) . .
O38 U3 O7 66.2(8) . .
O9 U3 Ag1 46.7(6) . 2_745
O33 U3 Ag1 129.3(6) . 2_745
O39 U3 Ag1 108.2(8) . 2_745
O17 U3 Ag1 107.1(4) 1_545 2_745
O1 U3 Ag1 133.0(4) . 2_745
O18 U3 Ag1 48.3(4) . 2_745
O38 U3 Ag1 85.5(8) . 2_745
O7 U3 Ag1 49.0(4) . 2_745
O9 U3 Ag7 143.9(6) . 2_655
O33 U3 Ag7 40.0(6) . 2_655
O39 U3 Ag7 40.5(8) . 2_655
O17 U3 Ag7 106.9(4) 1_545 2_655
O1 U3 Ag7 67.5(5) . 2_655
O18 U3 Ag7 133.1(4) . 2_655
O38 U3 Ag7 70.6(8) . 2_655
O7 U3 Ag7 95.0(4) . 2_655
Ag1 U3 Ag7 143.25(7) 2_745 2_655
O35 U4 O34 176.9(10) . .
O35 U4 O10 91.4(8) . .
O34 U4 O10 90.2(7) . .
O35 U4 O37 72.2(11) . .
O34 U4 O37 110.8(10) . .
O10 U4 O37 74.7(8) . .
O35 U4 O36 110.7(12) . .
O34 U4 O36 72.4(11) . .
O10 U4 O36 75.6(9) . .
O37 U4 O36 38.4(12) . .
O35 U4 O5 84.0(9) . 1_544
O34 U4 O5 93.7(8) . 1_544
O10 U4 O5 75.6(6) . 1_544
O37 U4 O5 141.1(9) . 1_544
O36 U4 O5 147.8(9) . 1_544
O35 U4 O28 94.2(8) . 1_554
O34 U4 O28 83.2(8) . 1_554
O10 U4 O28 150.4(6) . 1_554
O37 U4 O28 134.5(7) . 1_554
O36 U4 O28 128.5(10) . 1_554
O5 U4 O28 76.2(6) 1_544 1_554
O35 U4 O24 92.5(8) . .
O34 U4 O24 88.0(7) . .
O10 U4 O24 141.5(6) . .
O37 U4 O24 70.2(8) . .
O36 U4 O24 67.3(9) . .
O5 U4 O24 142.9(6) 1_544 .
O28 U4 O24 67.3(6) 1_554 .
O35 U4 Ag4 125.1(7) . .
O34 U4 Ag4 53.2(6) . .
O10 U4 Ag4 143.4(4) . .
O37 U4 Ag4 116.4(7) . .
O36 U4 Ag4 92.4(9) . .
O5 U4 Ag4 102.4(5) 1_544 .
O28 U4 Ag4 38.9(5) 1_554 .
O24 U4 Ag4 50.8(4) . .
O35 U4 Ag12 53.6(7) . .
O34 U4 Ag12 125.8(6) . .
O10 U4 Ag12 52.2(5) . .
O37 U4 Ag12 96.3(7) . .
O36 U4 Ag12 120.9(9) . .
O5 U4 Ag12 45.2(5) 1_544 .
O28 U4 Ag12 110.2(5) 1_554 .
O24 U4 Ag12 146.1(4) . .
Ag4 U4 Ag12 145.79(9) . .
O13 As1 O18 116.0(7) . .
O13 As1 O16 114.2(8) . .
O18 As1 O16 112.9(7) . .
O13 As1 O3 109.8(8) . .
O18 As1 O3 96.2(8) . .
O16 As1 O3 105.6(7) . .
O22 As2 O11 113.6(8) . .
O22 As2 O7 111.7(8) . .
O11 As2 O7 116.1(8) . .
O22 As2 O21 111.1(9) . .
O11 As2 O21 98.7(8) . .
O7 As2 O21 104.5(8) . .
O4 As3 O2 116.9(8) . .
O4 As3 O28 114.0(9) . .
O2 As3 O28 111.0(9) . .
O4 As3 O3 106.7(8) . .
O2 As3 O3 104.7(8) . .
O28 As3 O3 101.7(8) . .
O19 As4 O14 106.7(8) . .
O19 As4 O1 116.8(8) . .
O14 As4 O1 109.6(9) . .
O19 As4 O29 107.4(9) . .
O14 As4 O29 107.4(8) . .
O1 As4 O29 108.6(9) . .
O12 As5 O27 116.2(9) . .
O12 As5 O24 116.1(8) . .
O27 As5 O24 111.6(8) . .
O12 As5 O21 108.3(9) . .
O27 As5 O21 98.3(8) . .
O24 As5 O21 103.9(8) . .
O17 As6 O30 109.0(9) . .
O17 As6 O8 108.4(9) . .
O30 As6 O8 113.7(8) . .
O17 As6 O5 104.6(9) . .
O30 As6 O5 110.1(8) . .
O8 As6 O5 110.6(9) . .
O23 As7 O32 113.6(9) . .
O23 As7 O6 104.3(9) . .
O32 As7 O6 111.0(9) . .
O23 As7 O10 109.5(9) . .
O32 As7 O10 106.8(8) . .
O6 As7 O10 111.7(8) . .
O38 As8 O37 135.1(15) . .
O38 As8 O40 65(2) . .
O37 As8 O40 100(2) . .
O38 As8 O15 110.6(13) . .
O37 As8 O15 114.1(11) . .
O40 As8 O15 112.7(18) . .
O38 As8 O36 115.8(19) . .
O37 As8 O36 53.6(16) . .
O40 As8 O36 53(2) . .
O15 As8 O36 107.2(12) . .
O38 As8 O39 47.1(16) . .
O37 As8 O39 110.5(14) . .
O40 As8 O39 108(2) . .
O15 As8 O39 110.5(11) . .
O36 As8 O39 142.3(14) . .
O38 As8 O41 107.7(18) . .
O37 As8 O41 57.4(17) . .
O40 As8 O41 143(2) . .
O15 As8 O41 104.2(14) . .
O36 As8 O41 110.8(19) . .
O39 As8 O41 61.9(17) . .
O19 Ag1 O8 133.7(6) . 1_545
O19 Ag1 O20 90.0(6) . 1_545
O8 Ag1 O20 83.2(5) 1_545 1_545
O19 Ag1 O18 80.1(5) . 2_745
O8 Ag1 O18 143.9(5) 1_545 2_745
O20 Ag1 O18 113.9(5) 1_545 2_745
O19 Ag1 Ag10 46.2(4) . .
O8 Ag1 Ag10 139.0(4) 1_545 .
O20 Ag1 Ag10 57.2(3) 1_545 .
O18 Ag1 Ag10 70.8(3) 2_745 .
O19 Ag1 U3 118.3(4) . 2_745
O8 Ag1 U3 100.5(4) 1_545 2_745
O20 Ag1 U3 129.3(4) 1_545 2_745
O18 Ag1 U3 43.6(3) 2_745 2_745
Ag10 Ag1 U3 112.22(10) . 2_745
O22 Ag2 O1 163.8(6) 2_645 .
O22 Ag2 O13 112.7(6) 2_645 2_645
O1 Ag2 O13 81.2(6) . 2_645
O22 Ag2 O30 88.8(6) 2_645 1_545
O1 Ag2 O30 77.4(6) . 1_545
O13 Ag2 O30 158.5(6) 2_645 1_545
O4 Ag3 O12 109.8(6) 2_645 2_644
O4 Ag3 O10 157.3(5) 2_645 .
O12 Ag3 O10 84.8(6) 2_644 .
O4 Ag3 O15 86.0(6) 2_645 .
O12 Ag3 O15 163.3(6) 2_644 .
O10 Ag3 O15 81.9(6) . .
O28 Ag4 O6 136.6(6) 1_554 2_744
O28 Ag4 O36 129.6(10) 1_554 2_744
O6 Ag4 O36 84.4(9) 2_744 2_744
O28 Ag4 O40 99.7(14) 1_554 2_744
O6 Ag4 O40 98.6(13) 2_744 2_744
O36 Ag4 O40 34.7(16) 2_744 2_744
O28 Ag4 Ag8 98.9(4) 1_554 2_744
O6 Ag4 Ag8 46.7(4) 2_744 2_744
O36 Ag4 Ag8 129.8(8) 2_744 2_744
O40 Ag4 Ag8 141.4(12) 2_744 2_744
O28 Ag4 U4 41.6(5) 1_554 .
O6 Ag4 U4 159.3(4) 2_744 .
O36 Ag4 U4 111.2(8) 2_744 .
O40 Ag4 U4 101.9(12) 2_744 .
Ag8 Ag4 U4 114.42(11) 2_744 .
O28 Ag4 U2 108.8(5) 1_554 2_755
O6 Ag4 U2 41.2(4) 2_744 2_755
O36 Ag4 U2 82.9(8) 2_744 2_755
O40 Ag4 U2 74.3(12) 2_744 2_755
Ag8 Ag4 U2 67.77(8) 2_744 2_755
U4 Ag4 U2 149.95(10) . 2_755
O8 Ag5 O40 78.6(13) 1_545 2_745
O8 Ag5 O3 97.1(5) 1_545 .
O40 Ag5 O3 124.3(13) 2_745 .
O8 Ag5 O19 150.4(5) 1_545 2_745
O40 Ag5 O19 117.2(13) 2_745 2_745
O3 Ag5 O19 93.5(5) . 2_745
O32 Ag6 O22 140.1(6) 2_634 1_545
O32 Ag6 O12 83.5(6) 2_634 1_545
O22 Ag6 O12 76.4(6) 1_545 1_545
O32 Ag6 O29 134.4(6) 2_634 .
O22 Ag6 O29 85.5(6) 1_545 .
O12 Ag6 O29 114.2(6) 1_545 .
O32 Ag6 O31 85.4(6) 2_634 2_645
O22 Ag6 O31 99.8(6) 1_545 2_645
O12 Ag6 O31 156.7(6) 1_545 2_645
O29 Ag6 O31 88.1(5) . 2_645
O32 Ag6 Ag12 91.9(4) 2_634 2_634
O22 Ag6 Ag12 49.6(4) 1_545 2_634
O12 Ag6 Ag12 46.4(4) 1_545 2_634
O29 Ag6 Ag12 131.4(4) . 2_634
O31 Ag6 Ag12 113.9(3) 2_645 2_634
O32 Ag6 Ag9 42.6(4) 2_634 .
O22 Ag6 Ag9 174.1(4) 1_545 .
O12 Ag6 Ag9 99.9(5) 1_545 .
O29 Ag6 Ag9 91.9(4) . .
O31 Ag6 Ag9 85.4(4) 2_645 .
Ag12 Ag6 Ag9 130.70(10) 2_634 .
O41 Ag7 O39 43.0(13) 2_655 2_655
O41 Ag7 O13 138.2(10) 2_655 1_565
O39 Ag7 O13 113.0(9) 2_655 1_565
O41 Ag7 O4 80.6(10) 2_655 1_565
O39 Ag7 O4 107.3(8) 2_655 1_565
O13 Ag7 O4 77.2(6) 1_565 1_565
O41 Ag7 O17 135.0(10) 2_655 .
O39 Ag7 O17 136.4(7) 2_655 .
O13 Ag7 O17 86.7(6) 1_565 .
O4 Ag7 O17 115.1(6) 1_565 .
O41 Ag7 O33 89.4(10) 2_655 2_655
O39 Ag7 O33 57.6(8) 2_655 2_655
O13 Ag7 O33 103.1(7) 1_565 2_655
O4 Ag7 O33 164.1(6) 1_565 2_655
O17 Ag7 O33 80.7(6) . 2_655
O41 Ag7 Ag9 88.0(8) 2_655 2_655
O39 Ag7 Ag9 82.4(6) 2_655 2_655
O13 Ag7 Ag9 51.2(4) 1_565 2_655
O4 Ag7 Ag9 47.8(4) 1_565 2_655
O17 Ag7 Ag9 134.7(4) . 2_655
O33 Ag7 Ag9 120.1(5) 2_655 2_655
O41 Ag7 Ag12 40.7(9) 2_655 1_566
O39 Ag7 Ag12 69.4(8) 2_655 1_566
O13 Ag7 Ag12 175.2(4) 1_565 1_566
O4 Ag7 Ag12 98.1(4) 1_565 1_566
O17 Ag7 Ag12 94.3(4) . 1_566
O33 Ag7 Ag12 81.7(5) 2_655 1_566
Ag9 Ag7 Ag12 126.33(10) 2_655 1_566
O41 Ag7 U3 77.3(10) 2_655 2_655
O39 Ag7 U3 36.7(7) 2_655 2_655
O13 Ag7 U3 96.5(4) 1_565 2_655
O4 Ag7 U3 137.9(4) 1_565 2_655
O17 Ag7 U3 105.9(4) . 2_655
O33 Ag7 U3 26.4(5) 2_655 2_655
Ag9 Ag7 U3 95.84(11) 2_655 2_655
Ag12 Ag7 U3 87.81(9) 1_566 2_655
O27 Ag8 O6 127.7(6) 2_744 .
O27 Ag8 O2 117.0(7) 2_744 1_544
O6 Ag8 O2 68.9(5) . 1_544
O27 Ag8 O16 126.0(5) 2_744 1_544
O6 Ag8 O16 100.6(5) . 1_544
O2 Ag8 O16 100.6(5) 1_544 1_544
O27 Ag8 Ag4 82.7(4) 2_744 2_744
O6 Ag8 Ag4 45.7(4) . 2_744
O2 Ag8 Ag4 95.1(4) 1_544 2_744
O16 Ag8 Ag4 133.0(4) 1_544 2_744
O27 Ag8 Ag10 77.9(5) 2_744 2_734
O6 Ag8 Ag10 138.6(4) . 2_734
O2 Ag8 Ag10 133.7(4) 1_544 2_734
O16 Ag8 Ag10 48.3(4) 1_544 2_734
Ag4 Ag8 Ag10 131.09(11) 2_744 2_734
O32 Ag9 O4 118.3(6) 2_634 2_645
O32 Ag9 O13 100.0(6) 2_634 2_645
O4 Ag9 O13 77.4(6) 2_645 2_645
O32 Ag9 O14 90.1(6) 2_634 .
O4 Ag9 O14 148.7(6) 2_645 .
O13 Ag9 O14 112.1(6) 2_645 .
O32 Ag9 Ag7 146.2(4) 2_634 2_655
O4 Ag9 Ag7 50.2(4) 2_645 2_655
O13 Ag9 Ag7 49.0(4) 2_645 2_655
O14 Ag9 Ag7 112.5(3) . 2_655
O32 Ag9 Ag6 44.3(5) 2_634 .
O4 Ag9 Ag6 156.9(4) 2_645 .
O13 Ag9 Ag6 90.2(4) 2_645 .
O14 Ag9 Ag6 54.2(4) . .
Ag7 Ag9 Ag6 131.97(11) 2_655 .
O32 Ag9 U2 95.4(4) 2_634 1_544
O4 Ag9 U2 117.9(4) 2_645 1_544
O13 Ag9 U2 149.2(4) 2_645 1_544
O14 Ag9 U2 40.9(4) . 1_544
Ag7 Ag9 U2 118.22(10) 2_655 1_544
Ag6 Ag9 U2 82.47(8) . 1_544
O19 Ag10 O16 102.5(6) . 2_745
O19 Ag10 Ag1 48.2(4) . .
O16 Ag10 Ag1 100.2(3) 2_745 .
O19 Ag10 Ag8 88.6(4) . 2_734
O16 Ag10 Ag8 48.1(4) 2_745 2_734
Ag1 Ag10 Ag8 123.15(12) . 2_734
O19 Ag10 U1 145.4(4) . 2_745
O16 Ag10 U1 45.2(4) 2_745 2_745
Ag1 Ag10 U1 115.83(11) . 2_745
Ag8 Ag10 U1 76.99(9) 2_734 2_745
O19 Ag10 U1 83.2(4) . 1_545
O16 Ag10 U1 157.5(4) 2_745 1_545
Ag1 Ag10 U1 67.10(9) . 1_545
Ag8 Ag10 U1 154.44(10) 2_734 1_545
U1 Ag10 U1 121.89(9) 2_745 1_545
O8 Ag11 O40 88.0(16) 2_755 .
O8 Ag11 O24 174.1(6) 2_755 .
O40 Ag11 O24 95.5(16) . .
O8 Ag11 O34 89.6(6) 2_755 2_744
O40 Ag11 O34 90.3(14) . 2_744
O24 Ag11 O34 85.7(6) . 2_744
O41 Ag12 O12 119.9(12) 2_644 2_644
O41 Ag12 O5 94.1(12) 2_644 1_544
O12 Ag12 O5 141.7(7) 2_644 1_544
O41 Ag12 O22 109.3(12) 2_644 2_644
O12 Ag12 O22 76.5(6) 2_644 2_644
O5 Ag12 O22 110.3(6) 1_544 2_644
O41 Ag12 Ag7 48.2(11) 2_644 1_544
O12 Ag12 Ag7 162.3(5) 2_644 1_544
O5 Ag12 Ag7 55.7(5) 1_544 1_544
O22 Ag12 Ag7 94.6(4) 2_644 1_544
O41 Ag12 Ag6 152.4(11) 2_644 2_634
O12 Ag12 Ag6 49.4(4) 2_644 2_634
O5 Ag12 Ag6 106.8(4) 1_544 2_634
O22 Ag12 Ag6 46.8(4) 2_644 2_634
Ag7 Ag12 Ag6 132.93(11) 1_544 2_634
O41 Ag12 U4 95.6(11) 2_644 .
O12 Ag12 U4 112.4(5) 2_644 .
O5 Ag12 U4 41.6(4) 1_544 .
O22 Ag12 U4 145.0(4) 2_644 .
Ag7 Ag12 U4 83.70(9) 1_544 .
Ag6 Ag12 U4 112.06(12) 2_634 .
As4 O1 U3 131.3(10) . .
As4 O1 Ag2 109.4(9) . .
U3 O1 Ag2 113.9(7) . .
As3 O2 Ag8 115.5(8) . 1_566
As3 O2 U2 127.3(9) . .
Ag8 O2 U2 108.1(6) 1_566 .
As1 O3 As3 127.5(9) . .
As1 O3 Ag5 113.1(7) . .
As3 O3 Ag5 119.5(8) . .
As3 O4 Ag9 123.7(9) . 2_645
As3 O4 Ag3 123.2(10) . 2_645
Ag9 O4 Ag3 92.5(6) 2_645 2_645
As3 O4 Ag7 113.9(8) . 1_545
Ag9 O4 Ag7 82.0(6) 2_645 1_545
Ag3 O4 Ag7 113.2(7) 2_645 1_545
As6 O5 U4 138.7(11) . 1_566
As6 O5 Ag12 118.3(9) . 1_566
U4 O5 Ag12 93.2(7) 1_566 1_566
As7 O6 Ag4 117.5(8) . 2_744
As7 O6 Ag8 105.3(8) . .
Ag4 O6 Ag8 87.6(6) 2_744 .
As7 O6 U2 131.4(9) . 1_544
Ag4 O6 U2 99.4(6) 2_744 1_544
Ag8 O6 U2 106.9(6) . 1_544
As2 O7 U3 125.7(8) . .
As6 O8 Ag11 130.0(10) . 2_755
As6 O8 Ag1 110.5(8) . 1_565
Ag11 O8 Ag1 93.0(6) 2_755 1_565
As6 O8 Ag5 119.7(8) . 1_565
Ag11 O8 Ag5 97.3(6) 2_755 1_565
Ag1 O8 Ag5 100.0(6) 1_565 1_565
As7 O10 U4 134.2(10) . .
As7 O10 Ag3 96.5(7) . .
U4 O10 Ag3 121.3(7) . .
As2 O11 U1 134.2(9) . .
As5 O12 Ag12 121.6(11) . 2_644
As5 O12 Ag3 126.0(11) . 2_644
Ag12 O12 Ag3 97.6(7) 2_644 2_644
As5 O12 Ag6 113.3(9) . 1_565
Ag12 O12 Ag6 84.3(6) 2_644 1_565
Ag3 O12 Ag6 105.5(8) 2_644 1_565
As1 O13 Ag7 110.6(9) . 1_545
As1 O13 Ag2 118.6(9) . 2_645
Ag7 O13 Ag2 112.0(6) 1_545 2_645
As1 O13 Ag9 120.0(8) . 2_645
Ag7 O13 Ag9 79.8(5) 1_545 2_645
Ag2 O13 Ag9 109.4(7) 2_645 2_645
As4 O14 U2 139.0(9) . 1_544
As4 O14 Ag9 112.4(7) . .
U2 O14 Ag9 94.5(6) 1_544 .
As8 O15 U2 131.0(10) . 1_544
As8 O15 Ag3 101.3(8) . .
U2 O15 Ag3 121.4(6) 1_544 .
As1 O16 U1 127.0(8) . .
As1 O16 Ag8 113.3(8) . 1_566
U1 O16 Ag8 117.4(5) . 1_566
As1 O16 Ag10 111.1(7) . 2_745
U1 O16 Ag10 89.1(5) . 2_745
Ag8 O16 Ag10 83.7(5) 1_566 2_745
As6 O17 U3 133.8(9) . 1_565
As6 O17 Ag7 102.1(8) . .
U3 O17 Ag7 123.9(8) 1_565 .
As1 O18 U3 129.7(8) . .
As1 O18 Ag1 141.7(8) . 2_745
U3 O18 Ag1 88.1(5) . 2_745
As4 O19 Ag10 109.4(9) . .
As4 O19 Ag1 112.3(8) . .
Ag10 O19 Ag1 85.5(7) . .
As4 O19 Ag5 121.1(10) . 2_745
Ag10 O19 Ag5 126.3(8) . 2_745
Ag1 O19 Ag5 91.2(5) . 2_745
U1 O20 Ag1 123.5(9) . 1_565
As5 O21 As2 127.4(10) . .
As2 O22 Ag6 112.0(8) . 1_565
As2 O22 Ag2 121.6(9) . 2_645
Ag6 O22 Ag2 108.8(6) 1_565 2_645
As2 O22 Ag12 114.5(8) . 2_644
Ag6 O22 Ag12 83.6(6) 1_565 2_644
Ag2 O22 Ag12 109.8(6) 2_645 2_644
As7 O23 U1 135.9(11) . 1_544
As5 O24 Ag11 114.7(8) . .
As5 O24 U4 120.5(9) . .
Ag11 O24 U4 117.0(6) . .
As5 O27 Ag8 117.7(9) . 2_744
As5 O27 U2 128.4(9) . 1_554
Ag8 O27 U2 113.9(7) 2_744 1_554
As3 O28 Ag4 130.6(9) . 1_556
As3 O28 U4 128.3(10) . 1_556
Ag4 O28 U4 99.5(8) 1_556 1_556
As4 O29 U1 136.9(9) . 1_545
As4 O29 Ag6 97.7(8) . .
U1 O29 Ag6 125.0(7) 1_545 .
As6 O30 U1 135.8(10) . .
As6 O30 Ag2 110.7(9) . 1_565
U1 O30 Ag2 112.1(6) . 1_565
U1 O31 Ag6 125.4(7) . 2_645
As7 O32 Ag9 145.4(11) . 2_634
As7 O32 Ag6 115.1(9) . 2_634
Ag9 O32 Ag6 93.1(6) 2_634 2_634
U3 O33 Ag7 113.6(8) . 2_655
U4 O34 Ag11 139.8(11) . 2_744
O40 O36 O37 116(3) . .
O40 O36 As8 63(3) . .
O37 O36 As8 62.4(18) . .
O40 O36 U4 162(3) . .
O37 O36 U4 68.9(19) . .
As8 O36 U4 129(2) . .
O40 O36 Ag4 76(2) . 2_744
O37 O36 Ag4 161(2) . 2_744
As8 O36 Ag4 116.6(18) . 2_744
U4 O36 Ag4 104.6(14) . 2_744
O36 O37 O41 126(3) . .
O36 O37 As8 63.9(19) . .
O41 O37 As8 62.1(19) . .
O36 O37 U4 72.6(19) . .
O41 O37 U4 160(2) . .
As8 O37 U4 134.3(15) . .
O39 O38 As8 76(2) . .
O39 O38 O40 132(4) . .
As8 O38 O40 63(2) . .
O39 O38 U3 64.5(18) . .
As8 O38 U3 139.8(19) . .
O40 O38 U3 146(2) . .
O38 O39 As8 57.2(19) . .
O38 O39 O41 115(3) . .
As8 O39 O41 59.1(16) . .
O38 O39 U3 84(2) . .
As8 O39 U3 140.7(17) . .
O41 O39 U3 153.6(19) . .
O38 O39 Ag7 157(2) . 2_655
As8 O39 Ag7 115.1(15) . 2_655
O41 O39 Ag7 67.7(17) . 2_655
U3 O39 Ag7 102.8(12) . 2_655
O36 O40 As8 65(3) . .
O36 O40 O38 114(4) . .
As8 O40 O38 52(2) . .
O36 O40 Ag11 92(3) . .
As8 O40 Ag11 123(3) . .
O38 O40 Ag11 109(3) . .
O36 O40 Ag5 165(3) . 2_745
As8 O40 Ag5 121(3) . 2_745
O38 O40 Ag5 76(3) . 2_745
Ag11 O40 Ag5 96(2) . 2_745
O36 O40 Ag4 70(2) . 2_744
As8 O40 Ag4 114(3) . 2_744
O38 O40 Ag4 149(3) . 2_744
Ag11 O40 Ag4 102(2) . 2_744
Ag5 O40 Ag4 95.6(19) 2_745 2_744
O37 O41 As8 60.5(17) . .
O37 O41 O39 111(3) . .
As8 O41 O39 58.9(17) . .
O37 O41 Ag12 94(2) . 2_644
As8 O41 Ag12 143(2) . 2_644
O39 O41 Ag12 116(2) . 2_644
O37 O41 Ag7 174(2) . 2_655
As8 O41 Ag7 116(2) . 2_655
O39 O41 Ag7 69.3(17) . 2_655
Ag12 O41 Ag7 91.1(14) 2_644 2_655
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
U1 O31 1.763(16) .
U1 O20 1.841(17) .
U1 O23 2.317(19) 1_566
U1 O30 2.325(16) .
U1 O29 2.359(19) 1_565
U1 O11 2.401(14) .
U1 O16 2.477(16) .
U1 Ag10 3.490(3) 2_745
U1 Ag10 3.738(4) 1_565
U2 O26 1.734(15) .
U2 O25 1.785(19) .
U2 O15 2.313(16) 1_566
U2 O14 2.359(16) 1_566
U2 O27 2.429(18) 1_556
U2 O2 2.429(15) .
U2 O6 2.472(18) 1_566
U2 Ag9 3.590(3) 1_566
U2 Ag4 3.705(4) 2_755
U3 O9 1.71(2) .
U3 O33 1.77(2) .
U3 O39 2.23(3) .
U3 O17 2.364(18) 1_545
U3 O1 2.374(16) .
U3 O18 2.394(14) .
U3 O38 2.46(3) .
U3 O7 2.466(17) .
U3 Ag1 3.467(3) 2_745
U3 Ag7 3.639(4) 2_655
U4 O35 1.78(2) .
U4 O34 1.82(2) .
U4 O10 2.279(16) .
U4 O37 2.31(3) .
U4 O36 2.36(4) .
U4 O5 2.38(2) 1_544
U4 O28 2.384(18) 1_554
U4 O24 2.516(15) .
U4 Ag4 3.538(4) .
U4 Ag12 3.579(4) .
As1 O13 1.665(17) .
As1 O18 1.674(14) .
As1 O16 1.695(14) .
As1 O3 1.745(18) .
As2 O22 1.647(18) .
As2 O11 1.649(15) .
As2 O7 1.656(16) .
As2 O21 1.796(18) .
As3 O4 1.627(18) .
As3 O2 1.674(15) .
As3 O28 1.72(2) .
As3 O3 1.786(16) .
As4 O19 1.636(18) .
As4 O14 1.670(16) .
As4 O1 1.688(17) .
As4 O29 1.685(19) .
As5 O12 1.62(2) .
As5 O27 1.715(17) .
As5 O24 1.718(14) .
As5 O21 1.719(18) .
As6 O17 1.667(19) .
As6 O30 1.671(15) .
As6 O8 1.674(18) .
As6 O5 1.674(18) .
As7 O23 1.627(19) .
As7 O32 1.664(17) .
As7 O6 1.679(19) .
As7 O10 1.686(16) .
As8 O38 1.49(4) .
As8 O37 1.69(3) .
As8 O40 1.68(6) .
As8 O15 1.703(15) .
As8 O36 1.71(4) .
As8 O39 1.71(3) .
As8 O41 1.72(4) .
Ag1 O19 2.405(18) .
Ag1 O8 2.428(16) 1_545
Ag1 O20 2.534(17) 1_545
Ag1 O18 2.589(16) 2_745
Ag1 Ag10 3.214(4) .
Ag1 U3 3.467(3) 2_745
Ag2 O22 2.445(17) 2_645
Ag2 O1 2.463(19) .
Ag2 O13 2.468(19) 2_645
Ag2 O30 2.529(19) 1_545
Ag3 O4 2.413(18) 2_645
Ag3 O12 2.45(2) 2_644
Ag3 O10 2.531(18) .
Ag3 O15 2.548(19) .
Ag4 O28 2.25(2) 1_554
Ag4 O6 2.385(16) 2_744
Ag4 O36 2.49(4) 2_744
Ag4 O40 2.57(5) 2_744
Ag4 Ag8 3.328(5) 2_744
Ag4 U2 3.705(4) 2_755
Ag5 O8 2.472(16) 1_545
Ag5 O40 2.52(6) 2_745
Ag5 O3 2.511(16) .
Ag5 O19 2.518(18) 2_745
Ag6 O32 2.35(2) 2_634
Ag6 O22 2.430(18) 1_545
Ag6 O12 2.526(18) 1_545
Ag6 O29 2.575(17) .
Ag6 O31 2.580(16) 2_645
Ag6 Ag12 3.313(4) 2_634
Ag6 Ag9 3.357(4) .
Ag7 O41 2.40(4) 2_655
Ag7 O39 2.42(3) 2_655
Ag7 O13 2.428(17) 1_565
Ag7 O4 2.456(16) 1_565
Ag7 O17 2.471(16) .
Ag7 O33 2.55(2) 2_655
Ag7 Ag9 3.164(3) 2_655
Ag7 Ag12 3.216(4) 1_566
Ag7 U3 3.639(4) 2_655
Ag8 O27 2.197(18) 2_744
Ag8 O6 2.423(16) .
Ag8 O2 2.429(18) 1_544
Ag8 O16 2.492(16) 1_544
Ag8 Ag4 3.328(5) 2_744
Ag8 Ag10 3.330(4) 2_734
Ag9 O32 2.276(16) 2_634
Ag9 O4 2.365(19) 2_645
Ag9 O13 2.505(16) 2_645
Ag9 O14 2.529(17) .
Ag9 Ag7 3.164(3) 2_655
Ag9 U2 3.590(3) 1_544
Ag10 O19 2.329(18) .
Ag10 O16 2.500(16) 2_745
Ag10 Ag8 3.330(4) 2_734
Ag10 U1 3.490(3) 2_745
Ag10 U1 3.738(4) 1_545
Ag11 O8 2.270(19) 2_755
Ag11 O40 2.28(5) .
Ag11 O24 2.326(18) .
Ag11 O34 2.578(19) 2_744
Ag12 O41 2.10(4) 2_644
Ag12 O12 2.41(2) 2_644
Ag12 O5 2.541(19) 1_544
Ag12 O22 2.539(16) 2_644
Ag12 Ag7 3.216(4) 1_544
Ag12 Ag6 3.313(4) 2_634
O2 Ag8 2.429(18) 1_566
O4 Ag9 2.365(19) 2_645
O4 Ag3 2.413(18) 2_645
O4 Ag7 2.456(16) 1_545
O5 U4 2.38(2) 1_566
O5 Ag12 2.541(19) 1_566
O6 Ag4 2.385(16) 2_744
O6 U2 2.472(18) 1_544
O8 Ag11 2.270(19) 2_755
O8 Ag1 2.428(16) 1_565
O8 Ag5 2.472(16) 1_565
O12 Ag12 2.41(2) 2_644
O12 Ag3 2.45(2) 2_644
O12 Ag6 2.526(18) 1_565
O13 Ag7 2.428(17) 1_545
O13 Ag2 2.468(19) 2_645
O13 Ag9 2.505(16) 2_645
O14 U2 2.359(16) 1_544
O15 U2 2.313(16) 1_544
O16 Ag8 2.492(16) 1_566
O16 Ag10 2.500(16) 2_745
O17 U3 2.364(18) 1_565
O18 Ag1 2.589(16) 2_745
O19 Ag5 2.518(18) 2_745
O20 Ag1 2.534(17) 1_565
O22 Ag6 2.430(18) 1_565
O22 Ag2 2.445(17) 2_645
O22 Ag12 2.539(16) 2_644
O23 U1 2.316(19) 1_544
O27 Ag8 2.197(17) 2_744
O27 U2 2.429(18) 1_554
O28 Ag4 2.25(2) 1_556
O28 U4 2.384(18) 1_556
O29 U1 2.359(19) 1_545
O30 Ag2 2.529(19) 1_565
O31 Ag6 2.580(16) 2_645
O32 Ag9 2.276(16) 2_634
O32 Ag6 2.35(2) 2_634
O33 Ag7 2.55(2) 2_655
O34 Ag11 2.578(19) 2_744
O36 O40 1.51(7) .
O36 O37 1.54(5) .
O36 Ag4 2.49(4) 2_744
O37 O41 1.64(5) .
O38 O39 1.30(4) .
O38 O40 1.72(6) .
O39 O41 1.77(5) .
O39 Ag7 2.42(3) 2_655
O40 Ag5 2.52(6) 2_745
O40 Ag4 2.57(5) 2_744
O41 Ag12 2.10(4) 2_644
O41 Ag7 2.40(4) 2_655
_cod_duplicate_entry 7200608
