#------------------------------------------------------------------------------
#$Date: 2023-11-10 21:21:08 +0200 (Fri, 10 Nov 2023) $
#$Revision: 287519 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/21/56/7215648.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7215648
loop_
_publ_author_name
'Alekseev, Evgeny V.'
'Krivovichev, Sergey V.'
'Depmeier, Wulf'
_publ_section_title
;
 Novel layered uranyl arsenates, Ag6[(UO2)2(As2O7)(As4O13)] and
 AI6[(UO2)2(AsO4)2(As2O7)] (AI--Ag and Na): first observation of a linear
 As4O136− anion and structure type evolution
;
_journal_issue                   17
_journal_name_full               'Journal of Materials Chemistry'
_journal_page_first              2583
_journal_paper_doi               10.1039/b818757f
_journal_volume                  19
_journal_year                    2009
_chemical_formula_sum            'As4 Na6 O19 U2'
_chemical_formula_weight         1217.68
_chemical_name_systematic
;
hexsodium diauranyl diortoarsenato diarsenate 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                108.63(3)
_cell_angle_beta                 91.27(2)
_cell_angle_gamma                97.40(2)
_cell_formula_units_Z            4
_cell_length_a                   10.996(3)
_cell_length_b                   11.633(3)
_cell_length_c                   14.057(4)
_cell_measurement_reflns_used    135
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      16
_cell_measurement_theta_min      12
_cell_volume                     1685.9(9)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Stoe Stadi4'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1213
_diffrn_reflns_av_sigmaI/netI    0.1508
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            15919
_diffrn_reflns_theta_full        27.88
_diffrn_reflns_theta_max         27.88
_diffrn_reflns_theta_min         1.53
_exptl_absorpt_coefficient_mu    27.236
_exptl_absorpt_correction_T_max  0.256
_exptl_absorpt_correction_T_min  0.048
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    4.797
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             2136
_exptl_crystal_size_max          0.14
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.05
_refine_diff_density_max         2.918
_refine_diff_density_min         -2.250
_refine_diff_density_rms         0.438
_refine_ls_extinction_coef       0.00047(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.926
_refine_ls_matrix_type           full
_refine_ls_number_parameters     382
_refine_ls_number_reflns         8044
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.926
_refine_ls_R_factor_all          0.1327
_refine_ls_R_factor_gt           0.0475
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0261P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0755
_refine_ls_wR_factor_ref         0.0918
_reflns_number_gt                4177
_reflns_number_total             8044
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b818757f.txt
_cod_data_source_block           O19As4Na6U2
_cod_original_cell_volume        1685.9(8)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7215648
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
U1 U 0.75550(4) 0.08003(4) 0.08919(3) 0.00772(10) Uani 1 1 d .
U2 U 0.76793(4) 0.07202(4) 0.57773(3) 0.00801(11) Uani 1 1 d .
U3 U 0.73768(4) -0.49473(4) -0.06071(3) 0.01157(11) Uani 1 1 d .
U4 U 0.75021(5) -0.49163(4) -0.54923(3) 0.01608(13) Uani 1 1 d .
As1 As 0.76737(11) -0.20508(11) 0.15191(9) 0.0095(3) Uani 1 1 d .
As2 As 0.77038(11) -0.21064(11) -0.12399(8) 0.0087(3) Uani 1 1 d .
As3 As 0.77601(12) -0.21864(12) 0.37271(9) 0.0105(3) Uani 1 1 d .
As4 As 0.74530(11) -0.82766(11) -0.14139(8) 0.0086(3) Uani 1 1 d .
As5 As 0.79288(11) -0.19880(11) -0.34406(9) 0.0076(3) Uani 1 1 d .
As6 As 0.74670(12) 0.41235(12) 0.16870(9) 0.0095(3) Uani 1 1 d .
As7 As 0.70879(11) -0.82381(11) -0.64326(8) 0.0085(3) Uani 1 1 d .
As8 As 0.71679(12) -0.61035(12) -0.33545(9) 0.0112(3) Uani 1 1 d .
Na1 Na 0.9853(5) 0.3284(5) 0.0308(4) 0.0168(12) Uani 1 1 d .
Na2 Na 0.5094(5) -0.7572(6) 0.0006(4) 0.0291(15) Uani 1 1 d .
Na3 Na 1.0341(5) -0.3163(5) -0.5208(4) 0.0197(13) Uani 1 1 d .
Na4 Na 0.4877(5) -0.7609(6) -0.5058(4) 0.0238(14) Uani 1 1 d .
Na5 Na 0.5550(5) 0.5975(5) 0.2054(4) 0.0215(13) Uani 1 1 d .
Na6 Na 0.9742(5) -0.9594(5) -0.0988(4) 0.0212(12) Uani 1 1 d .
Na7 Na 1.0041(5) 0.6460(5) 0.2049(4) 0.0240(13) Uani 1 1 d .
Na8 Na 0.9341(5) -0.9759(5) -0.6627(4) 0.0221(13) Uani 1 1 d .
Na9 Na 0.5618(5) -1.0752(5) -0.2095(4) 0.0183(12) Uani 1 1 d .
Na10 Na 0.4885(5) 0.1204(5) 0.6856(5) 0.0266(13) Uani 1 1 d .
Na11 Na 0.9661(6) -0.3887(6) -0.2812(4) 0.0292(14) Uani 1 1 d .
Na12 Na 0.5280(6) -1.3789(6) -0.3117(5) 0.0377(17) Uani 1 1 d .
O1 O 0.6422(8) -0.2191(8) -0.3549(6) 0.0137(18) Uiso 1 1 d .
O2 O 0.6203(8) -0.2255(8) -0.1405(6) 0.0147(19) Uiso 1 1 d .
O3 O 0.6244(9) -0.2455(8) 0.3612(6) 0.017(2) Uiso 1 1 d .
O4 O 0.6697(8) -0.7018(7) -0.0998(6) 0.0097(17) Uiso 1 1 d .
O5 O 0.6166(9) -0.2248(8) 0.1512(6) 0.018(2) Uiso 1 1 d .
O6 O 0.6884(8) 0.2622(8) 0.1135(6) 0.0164(19) Uiso 1 1 d .
O7 O 0.6233(8) -0.0154(8) 0.5337(6) 0.0136(18) Uiso 1 1 d .
O8 O 0.8276(9) -0.3049(8) 0.0563(6) 0.019(2) Uiso 1 1 d .
O9 O 0.8340(7) -0.0606(7) 0.1739(6) 0.0089(16) Uiso 1 1 d .
O10 O 0.6817(8) 0.4637(8) 0.2789(6) 0.0132(18) Uiso 1 1 d .
O11 O 0.6597(8) -0.7594(8) -0.3883(6) 0.0153(19) Uiso 1 1 d .
O12 O 0.8585(8) -0.3223(7) -0.3986(6) 0.0108(17) Uiso 1 1 d .
O13 O 0.6891(8) 0.4862(8) 0.0945(6) 0.0127(18) Uiso 1 1 d .
O14 O 0.6516(8) -0.6876(8) -0.5979(6) 0.0109(18) Uiso 1 1 d .
O15 O 0.8273(8) -0.3398(7) -0.1381(6) 0.0098(17) Uiso 1 1 d .
O16 O 0.6953(8) -0.9208(7) -0.0737(6) 0.0125(18) Uiso 1 1 d .
O17 O 0.8970(9) 0.4348(8) 0.1787(6) 0.018(2) Uiso 1 1 d .
O18 O 0.8968(8) -0.7958(7) -0.1297(6) 0.0129(17) Uiso 1 1 d .
O19 O 0.6892(7) -0.9061(7) -0.2601(5) 0.0078(16) Uiso 1 1 d .
O20 O 0.8297(8) -0.2453(8) 0.2521(6) 0.0160(18) Uiso 1 1 d .
O21 O 0.9107(8) 0.1657(8) 0.6283(6) 0.0151(18) Uiso 1 1 d .
O22 O 0.8439(8) -0.1538(8) -0.2141(6) 0.0149(18) Uiso 1 1 d .
O23 O 0.8601(8) -0.0763(8) -0.3698(6) 0.0143(18) Uiso 1 1 d .
O24 O 0.8889(9) -0.5314(9) -0.0551(7) 0.021(2) Uiso 1 1 d .
O25 O 0.9113(8) 0.1469(8) 0.0796(6) 0.0135(18) Uiso 1 1 d .
O26 O 0.5891(9) -0.9308(8) -0.6737(7) 0.021(2) Uiso 1 1 d .
O27 O 0.8070(8) -0.8401(8) -0.5556(6) 0.0132(18) Uiso 1 1 d .
O28 O 0.8964(10) -0.5436(10) -0.5782(7) 0.029(2) Uiso 1 1 d .
O29 O 0.8328(8) -0.0739(8) 0.4323(6) 0.0125(17) Uiso 1 1 d .
O30 O 0.8313(8) -0.0938(7) -0.0219(6) 0.0122(17) Uiso 1 1 d .
O31 O 0.6042(8) 0.0082(8) 0.0934(6) 0.0134(18) Uiso 1 1 d .
O32 O 0.7989(8) -0.8200(8) -0.7397(6) 0.0141(18) Uiso 1 1 d .
O33 O 0.8421(9) -0.3190(8) 0.4095(6) 0.0183(19) Uiso 1 1 d .
O34 O 0.6074(11) -0.4401(10) -0.5267(8) 0.035(3) Uiso 1 1 d .
O35 O 0.5905(11) -0.4534(11) -0.0668(8) 0.038(3) Uiso 1 1 d .
O36 O 0.6542(16) -0.5551(16) -0.2238(12) 0.011(3) Uiso 0.50 1 d P
O37 O 0.6782(16) -0.5268(16) -0.4062(12) 0.010(4) Uiso 0.50 1 d P
O38 O 0.8772(15) -0.5858(14) -0.3213(11) 0.006(3) Uiso 0.50 1 d P
O39 O 0.8059(16) -0.5677(15) -0.4136(12) 0.013(4) Uiso 0.50 1 d P
O40 O 0.7962(17) -0.5950(16) -0.2320(12) 0.016(4) Uiso 0.50 1 d P
O41 O 0.5863(17) -0.5446(16) -0.3159(12) 0.017(4) Uiso 0.50 1 d P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O31 U1 O25 177.2(3) . .
O31 U1 O6 91.2(4) . .
O25 U1 O6 90.9(4) . .
O31 U1 O32 98.6(3) . 1_566
O25 U1 O32 83.8(3) . 1_566
O6 U1 O32 76.8(3) . 1_566
O31 U1 O16 87.2(3) . 1_565
O25 U1 O16 91.5(3) . 1_565
O6 U1 O16 75.0(3) . 1_565
O32 U1 O16 151.3(3) 1_566 1_565
O31 U1 O30 97.8(3) . .
O25 U1 O30 79.5(3) . .
O6 U1 O30 148.7(3) . .
O32 U1 O30 130.6(3) 1_566 .
O16 U1 O30 75.6(3) 1_565 .
O31 U1 O9 88.3(3) . .
O25 U1 O9 91.1(3) . .
O6 U1 O9 145.3(3) . .
O32 U1 O9 69.0(3) 1_566 .
O16 U1 O9 139.5(3) 1_565 .
O30 U1 O9 65.2(3) . .
O31 U1 Na6 126.8(3) . 2_745
O25 U1 Na6 51.6(3) . 2_745
O6 U1 Na6 140.3(2) . 2_745
O32 U1 Na6 85.6(2) 1_566 2_745
O16 U1 Na6 113.4(2) 1_565 2_745
O30 U1 Na6 48.1(2) . 2_745
O9 U1 Na6 43.8(2) . 2_745
O31 U1 Na6 134.1(3) . 1_565
O25 U1 Na6 43.2(3) . 1_565
O6 U1 Na6 108.6(2) . 1_565
O32 U1 Na6 125.7(2) 1_566 1_565
O16 U1 Na6 60.5(2) 1_565 1_565
O30 U1 Na6 45.9(2) . 1_565
O9 U1 Na6 96.2(2) . 1_565
Na6 U1 Na6 55.29(16) 2_745 1_565
O31 U1 Na1 151.8(3) . .
O25 U1 Na1 29.1(3) . .
O6 U1 Na1 64.6(2) . .
O32 U1 Na1 90.0(2) 1_566 .
O16 U1 Na1 73.2(2) 1_565 .
O30 U1 Na1 96.7(2) . .
O9 U1 Na1 119.8(2) . .
Na6 U1 Na1 80.38(12) 2_745 .
Na6 U1 Na1 51.33(11) 1_565 .
O31 U1 Na2 68.3(3) . 1_565
O25 U1 Na2 112.6(3) . 1_565
O6 U1 Na2 35.7(2) . 1_565
O32 U1 Na2 106.9(2) 1_566 1_565
O16 U1 Na2 49.3(2) 1_565 1_565
O30 U1 Na2 122.4(2) . 1_565
O9 U1 Na2 155.7(2) . 1_565
Na6 U1 Na2 159.61(13) 2_745 1_565
Na6 U1 Na2 104.63(12) 1_565 1_565
Na1 U1 Na2 83.50(12) . 1_565
O31 U1 Na9 28.8(3) . 2_645
O25 U1 Na9 154.1(3) . 2_645
O6 U1 Na9 70.9(2) . 2_645
O32 U1 Na9 74.4(2) 1_566 2_645
O16 U1 Na9 100.9(2) 1_565 2_645
O30 U1 Na9 125.5(2) . 2_645
O9 U1 Na9 93.9(2) . 2_645
Na6 U1 Na9 137.64(12) 2_745 2_645
Na6 U1 Na9 159.74(11) 1_565 2_645
Na1 U1 Na9 135.12(11) . 2_645
Na2 U1 Na9 62.52(12) 1_565 2_645
O7 U2 O21 176.8(4) . .
O7 U2 O11 84.5(4) . 1_566
O21 U2 O11 93.2(4) . 1_566
O7 U2 O29 82.6(3) . .
O21 U2 O29 100.6(3) . .
O11 U2 O29 137.1(3) 1_566 .
O7 U2 O23 98.1(4) . 1_556
O21 U2 O23 82.8(4) . 1_556
O11 U2 O23 151.2(3) 1_566 1_556
O29 U2 O23 71.4(3) . 1_556
O7 U2 O19 83.1(3) . 1_566
O21 U2 O19 94.1(3) . 1_566
O11 U2 O19 74.8(3) 1_566 1_566
O29 U2 O19 143.0(3) . 1_566
O23 U2 O19 77.0(3) 1_556 1_566
O7 U2 O27 100.3(3) . 1_566
O21 U2 O27 81.1(3) . 1_566
O11 U2 O27 73.6(3) 1_566 1_566
O29 U2 O27 68.8(3) . 1_566
O23 U2 O27 133.1(3) 1_556 1_566
O19 U2 O27 147.7(3) 1_566 1_566
O7 U2 Na10 52.8(3) . .
O21 U2 Na10 124.0(3) . .
O11 U2 Na10 48.9(2) 1_566 .
O29 U2 Na10 135.4(2) . .
O23 U2 Na10 111.0(2) 1_556 .
O19 U2 Na10 43.6(2) 1_566 .
O27 U2 Na10 114.5(2) 1_566 .
O7 U2 Na3 136.8(3) . 2_755
O21 U2 Na3 44.0(3) . 2_755
O11 U2 Na3 73.0(2) 1_566 2_755
O29 U2 Na3 89.3(2) . 2_755
O23 U2 Na3 119.3(2) 1_556 2_755
O19 U2 Na3 123.6(2) 1_566 2_755
O27 U2 Na3 38.4(2) 1_566 2_755
Na10 U2 Na3 121.65(12) . 2_755
O7 U2 Na8 102.3(3) . 1_566
O21 U2 Na8 80.6(3) . 1_566
O11 U2 Na8 112.0(2) 1_566 1_566
O29 U2 Na8 33.8(2) . 1_566
O23 U2 Na8 95.6(2) 1_556 1_566
O19 U2 Na8 171.5(2) 1_566 1_566
O27 U2 Na8 38.4(2) 1_566 1_566
Na10 U2 Na8 144.82(13) . 1_566
Na3 U2 Na8 56.29(12) 2_755 1_566
O7 U2 Na8 129.8(3) . 2_745
O21 U2 Na8 51.6(3) . 2_745
O11 U2 Na8 141.2(2) 1_566 2_745
O29 U2 Na8 73.3(2) . 2_745
O23 U2 Na8 32.7(2) 1_556 2_745
O19 U2 Na8 90.3(2) 1_566 2_745
O27 U2 Na8 110.4(2) 1_566 2_745
Na10 U2 Na8 133.27(13) . 2_745
Na3 U2 Na8 86.99(12) 2_755 2_745
Na8 U2 Na8 81.11(13) 1_566 2_745
O7 U2 Na4 25.0(3) . 2_645
O21 U2 Na4 156.0(3) . 2_645
O11 U2 Na4 107.4(2) 1_566 2_645
O29 U2 Na4 72.9(2) . 2_645
O23 U2 Na4 73.2(2) 1_556 2_645
O19 U2 Na4 79.9(2) 1_566 2_645
O27 U2 Na4 116.1(2) 1_566 2_645
Na10 U2 Na4 66.17(12) . 2_645
Na3 U2 Na4 154.21(11) 2_755 2_645
Na8 U2 Na4 102.24(11) 1_566 2_645
Na8 U2 Na4 104.81(12) 2_745 2_645
O35 U3 O24 177.9(5) . .
O35 U3 O36 68.1(6) . .
O24 U3 O36 111.8(5) . .
O35 U3 O4 95.1(4) . .
O24 U3 O4 86.9(4) . .
O36 U3 O4 75.3(5) . .
O35 U3 O13 85.9(4) . 1_545
O24 U3 O13 95.3(4) . 1_545
O36 U3 O13 139.6(5) . 1_545
O4 U3 O13 76.9(3) . 1_545
O35 U3 O8 95.7(4) . .
O24 U3 O8 82.9(4) . .
O36 U3 O8 134.3(5) . .
O4 U3 O8 150.3(3) . .
O13 U3 O8 76.4(3) 1_545 .
O35 U3 O40 109.3(6) . .
O24 U3 O40 70.6(5) . .
O36 U3 O40 41.2(6) . .
O4 U3 O40 73.1(5) . .
O13 U3 O40 147.3(5) 1_545 .
O8 U3 O40 128.1(5) . .
O35 U3 O15 91.8(4) . .
O24 U3 O15 86.2(4) . .
O36 U3 O15 72.5(5) . .
O4 U3 O15 141.7(3) . .
O13 U3 O15 141.3(3) 1_545 .
O8 U3 O15 65.4(3) . .
O40 U3 O15 69.0(4) . .
O35 U3 Na1 130.7(4) . 2_755
O24 U3 Na1 47.3(3) . 2_755
O36 U3 Na1 112.5(4) . 2_755
O4 U3 Na1 133.8(2) . 2_755
O13 U3 Na1 107.8(2) 1_545 2_755
O8 U3 Na1 46.5(2) . 2_755
O40 U3 Na1 84.5(4) . 2_755
O15 U3 Na1 48.0(2) . 2_755
O35 U3 Na5 38.6(4) . 2_655
O24 U3 Na5 142.4(3) . 2_655
O36 U3 Na5 38.9(4) . 2_655
O4 U3 Na5 65.7(2) . 2_655
O13 U3 Na5 102.4(2) 1_545 2_655
O8 U3 Na5 133.3(2) . 2_655
O40 U3 Na5 76.9(4) . 2_655
O15 U3 Na5 99.5(2) . 2_655
Na1 U3 Na5 147.05(14) 2_755 2_655
O35 U3 Na7 147.1(4) . 2_755
O24 U3 Na7 32.9(3) . 2_755
O36 U3 Na7 78.9(4) . 2_755
O4 U3 Na7 76.4(2) . 2_755
O13 U3 Na7 121.7(2) 1_545 2_755
O8 U3 Na7 107.4(2) . 2_755
O40 U3 Na7 37.8(4) . 2_755
O15 U3 Na7 77.5(2) . 2_755
Na1 U3 Na7 61.95(12) 2_755 2_755
Na5 U3 Na7 111.87(12) 2_655 2_755
O35 U3 Na2 74.8(4) . .
O24 U3 Na2 107.3(3) . .
O36 U3 Na2 91.7(4) . .
O4 U3 Na2 32.9(2) . .
O13 U3 Na2 50.7(2) 1_545 .
O8 U3 Na2 126.3(2) . .
O40 U3 Na2 104.2(4) . .
O15 U3 Na2 162.4(2) . .
Na1 U3 Na2 149.32(13) 2_755 .
Na5 U3 Na2 62.94(13) 2_655 .
Na7 U3 Na2 107.52(13) 2_755 .
O34 U4 O28 177.2(5) . .
O34 U4 O14 88.7(4) . .
O28 U4 O14 91.6(4) . .
O34 U4 O37 70.6(6) . .
O28 U4 O37 112.1(6) . .
O14 U4 O37 73.0(5) . .
O34 U4 O33 94.9(4) . 1_554
O28 U4 O33 83.4(4) . 1_554
O14 U4 O33 150.1(3) . 1_554
O37 U4 O33 136.0(5) . 1_554
O34 U4 O10 83.2(4) . 1_544
O28 U4 O10 94.3(4) . 1_544
O14 U4 O10 74.8(3) . 1_544
O37 U4 O10 138.5(5) . 1_544
O33 U4 O10 76.1(3) 1_554 1_544
O34 U4 O39 108.1(5) . .
O28 U4 O39 74.6(5) . .
O14 U4 O39 75.9(4) . .
O37 U4 O39 37.6(6) . .
O33 U4 O39 130.0(5) 1_554 .
O10 U4 O39 148.3(4) 1_544 .
O34 U4 O12 93.3(4) . .
O28 U4 O12 88.2(4) . .
O14 U4 O12 142.5(3) . .
O37 U4 O12 72.4(4) . .
O33 U4 O12 67.1(3) 1_554 .
O10 U4 O12 142.6(3) 1_544 .
O39 U4 O12 67.9(4) . .
O34 U4 Na3 127.5(4) . .
O28 U4 Na3 52.2(4) . .
O14 U4 Na3 143.7(2) . .
O37 U4 Na3 116.2(4) . .
O33 U4 Na3 41.8(2) 1_554 .
O10 U4 Na3 105.2(2) 1_544 .
O39 U4 Na3 91.4(4) . .
O12 U4 Na3 49.2(2) . .
O34 U4 Na12 52.7(4) . 2_634
O28 U4 Na12 125.9(3) . 2_634
O14 U4 Na12 49.6(3) . 2_634
O37 U4 Na12 92.8(4) . 2_634
O33 U4 Na12 111.4(2) 1_554 2_634
O10 U4 Na12 45.9(2) 1_544 2_634
O39 U4 Na12 117.9(4) . 2_634
O12 U4 Na12 146.0(2) . 2_634
Na3 U4 Na12 149.91(14) . 2_634
O34 U4 Na3 143.7(4) . 2_744
O28 U4 Na3 38.8(4) . 2_744
O14 U4 Na3 73.0(2) . 2_744
O37 U4 Na3 74.1(4) . 2_744
O33 U4 Na3 116.7(2) 1_554 2_744
O10 U4 Na3 119.8(2) 1_544 2_744
O39 U4 Na3 37.8(4) . 2_744
O12 U4 Na3 84.0(2) . 2_744
Na3 U4 Na3 76.32(14) . 2_744
Na12 U4 Na3 122.14(14) 2_634 2_744
O34 U4 Na11 155.6(4) . 2_744
O28 U4 Na11 21.7(3) . 2_744
O14 U4 Na11 89.4(2) . 2_744
O37 U4 Na11 131.6(4) . 2_744
O33 U4 Na11 75.2(2) 1_554 2_744
O10 U4 Na11 72.9(2) 1_544 2_744
O39 U4 Na11 95.0(4) . 2_744
O12 U4 Na11 102.8(2) . 2_744
Na3 U4 Na11 57.49(13) . 2_744
Na12 U4 Na11 109.63(14) 2_634 2_744
Na3 U4 Na11 57.52(12) 2_744 2_744
O5 As1 O9 115.5(4) . .
O5 As1 O8 115.7(4) . .
O9 As1 O8 112.2(4) . .
O5 As1 O20 109.5(4) . .
O9 As1 O20 103.5(4) . .
O8 As1 O20 98.3(4) . .
O5 As1 Na5 44.5(4) . 1_545
O9 As1 Na5 149.3(3) . 1_545
O8 As1 Na5 98.5(3) . 1_545
O20 As1 Na5 72.2(3) . 1_545
O5 As1 Na8 119.9(3) . 1_566
O9 As1 Na8 40.9(3) . 1_566
O8 As1 Na8 124.5(3) . 1_566
O20 As1 Na8 63.6(3) . 1_566
Na5 As1 Na8 120.68(13) 1_545 1_566
O5 As1 Na6 146.4(4) . 2_745
O9 As1 Na6 39.1(3) . 2_745
O8 As1 Na6 74.4(3) . 2_745
O20 As1 Na6 99.9(3) . 2_745
Na5 As1 Na6 168.77(13) 1_545 2_745
Na8 As1 Na6 59.79(13) 1_566 2_745
O5 As1 Na7 136.1(4) . 1_545
O9 As1 Na7 104.2(3) . 1_545
O8 As1 Na7 60.8(3) . 1_545
O20 As1 Na7 39.8(3) . 1_545
Na5 As1 Na7 91.65(14) 1_545 1_545
Na8 As1 Na7 79.03(14) 1_566 1_545
Na6 As1 Na7 77.33(13) 2_745 1_545
O2 As2 O15 115.2(4) . .
O2 As2 O30 114.3(4) . .
O15 As2 O30 113.9(4) . .
O2 As2 O22 111.4(4) . .
O15 As2 O22 103.4(4) . .
O30 As2 O22 96.5(4) . .
O2 As2 Na9 42.2(3) . 1_565
O15 As2 Na9 146.1(3) . 1_565
O30 As2 Na9 99.8(3) . 1_565
O22 As2 Na9 74.5(3) . 1_565
O2 As2 Na6 127.5(3) . 1_565
O15 As2 Na6 116.7(3) . 1_565
O30 As2 Na6 48.2(3) . 1_565
O22 As2 Na6 48.3(3) . 1_565
Na9 As2 Na6 87.62(13) 1_565 1_565
O2 As2 Na11 126.6(3) . .
O15 As2 Na11 41.7(3) . .
O30 As2 Na11 119.1(3) . .
O22 As2 Na11 61.8(3) . .
Na9 As2 Na11 122.72(13) 1_565 .
Na6 As2 Na11 89.19(14) 1_565 .
O3 As3 O29 114.1(4) . .
O3 As3 O33 114.6(5) . .
O29 As3 O33 114.3(4) . .
O3 As3 O20 108.2(4) . .
O29 As3 O20 103.4(4) . .
O33 As3 O20 100.5(4) . .
O3 As3 Na8 122.6(3) . 1_566
O29 As3 Na8 38.0(3) . 1_566
O33 As3 Na8 122.7(3) . 1_566
O20 As3 Na8 65.5(3) . 1_566
O3 As3 Na5 42.1(3) . 1_545
O29 As3 Na5 144.0(3) . 1_545
O33 As3 Na5 101.5(3) . 1_545
O20 As3 Na5 71.8(3) . 1_545
Na8 As3 Na5 122.16(14) 1_566 1_545
O3 As3 Na10 34.2(3) . 2_656
O29 As3 Na10 88.4(3) . 2_656
O33 As3 Na10 148.8(3) . 2_656
O20 As3 Na10 94.3(3) . 2_656
Na8 As3 Na10 88.49(14) 1_566 2_656
Na5 As3 Na10 57.28(13) 1_545 2_656
O3 As3 Na4 36.2(3) . 2_645
O29 As3 Na4 99.0(3) . 2_645
O33 As3 Na4 95.3(3) . 2_645
O20 As3 Na4 144.1(3) . 2_645
Na8 As3 Na4 129.46(14) 1_566 2_645
Na5 As3 Na4 73.52(13) 1_545 2_645
Na10 As3 Na4 58.53(14) 2_656 2_645
O18 As4 O19 113.5(4) . .
O18 As4 O16 110.6(4) . .
O19 As4 O16 104.5(4) . .
O18 As4 O4 114.6(4) . .
O19 As4 O4 107.1(4) . .
O16 As4 O4 105.9(4) . .
O18 As4 Na9 133.2(3) . .
O19 As4 Na9 54.2(3) . .
O16 As4 Na9 50.7(3) . .
O4 As4 Na9 112.0(3) . .
O18 As4 Na6 43.2(3) . .
O19 As4 Na6 106.2(3) . .
O16 As4 Na6 71.9(3) . .
O4 As4 Na6 146.0(3) . .
Na9 As4 Na6 93.02(14) . .
O18 As4 Na2 137.9(3) . .
O19 As4 Na2 108.3(3) . .
O16 As4 Na2 62.2(3) . .
O4 As4 Na2 44.7(3) . .
Na9 As4 Na2 77.15(15) . .
Na6 As4 Na2 127.68(15) . .
O18 As4 Na1 38.0(3) . 1_545
O19 As4 Na1 151.2(3) . 1_545
O16 As4 Na1 93.5(3) . 1_545
O4 As4 Na1 88.9(3) . 1_545
Na9 As4 Na1 141.50(15) . 1_545
Na6 As4 Na1 58.02(13) . 1_545
Na2 As4 Na1 99.89(14) . 1_545
O18 As4 Na10 142.5(3) . 1_544
O19 As4 Na10 36.4(3) . 1_544
O16 As4 Na10 101.2(3) . 1_544
O4 As4 Na10 73.4(3) . 1_544
Na9 As4 Na10 57.71(14) . 1_544
Na6 As4 Na10 140.60(13) . 1_544
Na2 As4 Na10 74.91(14) . 1_544
Na1 As4 Na10 159.41(13) 1_545 1_544
O18 As4 Na7 37.6(3) . 2_755
O19 As4 Na7 96.6(3) . 2_755
O16 As4 Na7 147.8(3) . 2_755
O4 As4 Na7 90.4(3) . 2_755
Na9 As4 Na7 146.68(13) . 2_755
Na6 As4 Na7 79.08(13) . 2_755
Na2 As4 Na7 132.85(15) . 2_755
Na1 As4 Na7 58.59(13) 1_545 2_755
Na10 As4 Na7 110.11(13) 1_544 2_755
O1 As5 O12 115.6(4) . .
O1 As5 O23 114.9(4) . .
O12 As5 O23 111.9(4) . .
O1 As5 O22 109.3(4) . .
O12 As5 O22 104.5(4) . .
O23 As5 O22 98.7(4) . .
O1 As5 Na8 150.4(3) . 2_744
O12 As5 Na8 88.7(3) . 2_744
O23 As5 Na8 36.2(3) . 2_744
O22 As5 Na8 78.1(3) . 2_744
O1 As5 Na9 42.8(3) . 1_565
O12 As5 Na9 148.5(3) . 1_565
O23 As5 Na9 99.5(3) . 1_565
O22 As5 Na9 73.0(3) . 1_565
Na8 As5 Na9 120.40(13) 2_744 1_565
O1 As5 Na11 124.8(3) . .
O12 As5 Na11 40.2(3) . .
O23 As5 Na11 120.3(3) . .
O22 As5 Na11 64.5(3) . .
Na8 As5 Na11 84.51(16) 2_744 .
Na9 As5 Na11 124.44(14) 1_565 .
O1 As5 Na12 35.5(3) . 1_565
O12 As5 Na12 91.4(3) . 1_565
O23 As5 Na12 150.2(3) . 1_565
O22 As5 Na12 92.7(3) . 1_565
Na8 As5 Na12 170.50(15) 2_744 1_565
Na9 As5 Na12 57.83(14) 1_565 1_565
Na11 As5 Na12 89.44(17) . 1_565
O17 As6 O10 114.0(4) . .
O17 As6 O6 112.4(4) . .
O10 As6 O6 107.8(4) . .
O17 As6 O13 111.9(5) . .
O10 As6 O13 105.0(4) . .
O6 As6 O13 105.1(4) . .
O17 As6 Na5 131.3(3) . .
O10 As6 Na5 57.2(3) . .
O6 As6 Na5 115.7(3) . .
O13 As6 Na5 47.9(3) . .
O17 As6 Na1 40.2(3) . .
O10 As6 Na1 152.6(3) . .
O6 As6 Na1 82.6(3) . .
O13 As6 Na1 96.1(3) . .
Na5 As6 Na1 141.53(16) . .
O17 As6 Na2 139.8(3) . 1_565
O10 As6 Na2 104.8(3) . 1_565
O6 As6 Na2 42.1(3) . 1_565
O13 As6 Na2 65.2(3) . 1_565
Na5 As6 Na2 78.75(15) . 1_565
Na1 As6 Na2 99.70(13) . 1_565
O17 As6 Na7 38.1(3) . .
O10 As6 Na7 100.6(3) . .
O6 As6 Na7 147.0(3) . .
O13 As6 Na7 82.8(3) . .
Na5 As6 Na7 93.61(13) . .
Na1 As6 Na7 64.51(13) . .
Na2 As6 Na7 143.15(15) 1_565 .
O26 As7 O27 112.6(5) . .
O26 As7 O32 114.9(4) . .
O27 As7 O32 103.8(4) . .
O26 As7 O14 105.8(4) . .
O27 As7 O14 110.4(4) . .
O32 As7 O14 109.4(4) . .
O26 As7 Na4 66.0(3) . .
O27 As7 Na4 97.5(3) . .
O32 As7 Na4 155.7(3) . .
O14 As7 Na4 50.9(3) . .
O26 As7 Na8 103.1(4) . .
O27 As7 Na8 48.2(3) . .
O32 As7 Na8 65.3(3) . .
O14 As7 Na8 149.6(3) . .
Na4 As7 Na8 139.01(15) . .
O26 As7 Na9 36.5(4) . 2_634
O27 As7 Na9 149.0(3) . 2_634
O32 As7 Na9 95.4(3) . 2_634
O14 As7 Na9 85.1(3) . 2_634
Na4 As7 Na9 71.07(13) . 2_634
Na8 As7 Na9 124.49(13) . 2_634
O26 As7 Na3 147.1(3) . 2_744
O27 As7 Na3 35.4(3) . 2_744
O32 As7 Na3 87.8(3) . 2_744
O14 As7 Na3 86.9(3) . 2_744
Na4 As7 Na3 103.32(14) . 2_744
Na8 As7 Na3 63.51(13) . 2_744
Na9 As7 Na3 171.99(13) 2_634 2_744
O40 As8 O39 109.9(9) . .
O40 As8 O37 140.4(8) . .
O39 As8 O37 55.1(8) . .
O40 As8 O11 108.0(7) . .
O39 As8 O11 108.9(6) . .
O37 As8 O11 111.6(6) . .
O40 As8 O36 60.8(8) . .
O39 As8 O36 142.2(8) . .
O37 As8 O36 106.5(8) . .
O11 As8 O36 108.8(7) . .
O40 As8 O41 113.5(8) . .
O39 As8 O41 114.4(9) . .
O37 As8 O41 59.9(8) . .
O11 As8 O41 101.6(7) . .
O36 As8 O41 53.5(8) . .
O40 As8 O38 55.7(8) . .
O39 As8 O38 55.7(8) . .
O37 As8 O38 105.9(8) . .
O11 As8 O38 112.5(6) . .
O36 As8 O38 111.5(7) . .
O41 As8 O38 145.9(8) . .
O40 As8 Na4 149.5(6) . .
O39 As8 Na4 96.0(6) . .
O37 As8 Na4 68.2(6) . .
O11 As8 Na4 46.2(3) . .
O36 As8 Na4 107.3(6) . .
O41 As8 Na4 66.8(6) . .
O38 As8 Na4 140.7(5) . .
O40 As8 Na11 65.8(6) . .
O39 As8 Na11 51.6(6) . .
O37 As8 Na11 79.6(6) . .
O11 As8 Na11 147.9(3) . .
O36 As8 Na11 95.6(6) . .
O41 As8 Na11 109.7(6) . .
O38 As8 Na11 36.8(5) . .
Na4 As8 Na11 144.43(15) . .
O40 As8 Na3 92.1(6) . 2_744
O39 As8 Na3 37.0(6) . 2_744
O37 As8 Na3 89.8(6) . 2_744
O11 As8 Na3 85.1(3) . 2_744
O36 As8 Na3 152.0(6) . 2_744
O41 As8 Na3 149.4(6) . 2_744
O38 As8 Na3 40.9(5) . 2_744
Na4 As8 Na3 99.87(14) . 2_744
Na11 As8 Na3 64.37(13) . 2_744
O40 As8 Na5 89.9(6) . 2_655
O39 As8 Na5 150.6(6) . 2_655
O37 As8 Na5 95.7(6) . 2_655
O11 As8 Na5 83.9(3) . 2_655
O36 As8 Na5 33.9(6) . 2_655
O41 As8 Na5 36.2(6) . 2_655
O38 As8 Na5 144.5(5) . 2_655
Na4 As8 Na5 73.46(13) . 2_655
Na11 As8 Na5 126.07(13) . 2_655
Na3 As8 Na5 168.93(13) 2_744 2_655
O40 As8 Na12 113.6(6) . 1_565
O39 As8 Na12 94.3(6) . 1_565
O37 As8 Na12 44.0(6) . 1_565
O11 As8 Na12 120.9(3) . 1_565
O36 As8 Na12 62.7(6) . 1_565
O41 As8 Na12 23.1(6) . 1_565
O38 As8 Na12 125.2(5) . 1_565
Na4 As8 Na12 78.86(15) . 1_565
Na11 As8 Na12 88.44(15) . 1_565
Na3 As8 Na12 131.25(15) 2_744 1_565
Na5 As8 Na12 57.06(14) 2_655 1_565
O17 Na1 O18 131.8(4) . 1_565
O17 Na1 O8 145.5(4) . 2_755
O18 Na1 O8 81.8(3) 1_565 2_755
O17 Na1 O25 83.5(3) . .
O18 Na1 O25 83.6(3) 1_565 .
O8 Na1 O25 111.9(4) 2_755 .
O17 Na1 O15 87.6(3) . 2_755
O18 Na1 O15 136.5(4) 1_565 2_755
O8 Na1 O15 64.8(3) 2_755 2_755
O25 Na1 O15 84.1(3) . 2_755
O17 Na1 O24 84.1(3) . 2_755
O18 Na1 O24 121.0(4) 1_565 2_755
O8 Na1 O24 68.8(3) 2_755 2_755
O25 Na1 O24 154.3(4) . 2_755
O15 Na1 O24 73.0(3) 2_755 2_755
O17 Na1 O24 87.0(3) . 1_565
O18 Na1 O24 71.7(3) 1_565 1_565
O8 Na1 O24 99.6(4) 2_755 1_565
O25 Na1 O24 136.5(4) . 1_565
O15 Na1 O24 137.9(4) 2_755 1_565
O24 Na1 O24 64.9(4) 2_755 1_565
O17 Na1 Na6 133.9(3) . 1_565
O18 Na1 Na6 46.0(2) 1_565 1_565
O8 Na1 Na6 72.3(3) 2_755 1_565
O25 Na1 Na6 51.3(2) . 1_565
O15 Na1 Na6 95.5(3) 2_755 1_565
O24 Na1 Na6 140.7(3) 2_755 1_565
O24 Na1 Na6 117.7(3) 1_565 1_565
O17 Na1 U3 101.1(3) . 2_755
O18 Na1 U3 121.8(3) 1_565 2_755
O8 Na1 U3 45.2(2) 2_755 2_755
O25 Na1 U3 131.2(3) . 2_755
O15 Na1 U3 48.2(2) 2_755 2_755
O24 Na1 U3 31.5(2) 2_755 2_755
O24 Na1 U3 92.2(3) 1_565 2_755
Na6 Na1 U3 115.01(18) 1_565 2_755
O17 Na1 As6 26.6(2) . .
O18 Na1 As6 105.3(3) 1_565 .
O8 Na1 As6 170.0(3) 2_755 .
O25 Na1 As6 76.3(2) . .
O15 Na1 As6 111.9(2) 2_755 .
O24 Na1 As6 101.3(3) 2_755 .
O24 Na1 As6 76.5(2) 1_565 .
Na6 Na1 As6 117.64(18) 1_565 .
U3 Na1 As6 125.22(15) 2_755 .
O17 Na1 Na11 42.5(3) . 2_755
O18 Na1 Na11 152.1(3) 1_565 2_755
O8 Na1 Na11 112.5(3) 2_755 2_755
O25 Na1 Na11 69.0(3) . 2_755
O15 Na1 Na11 47.9(2) 2_755 2_755
O24 Na1 Na11 86.8(3) 2_755 2_755
O24 Na1 Na11 125.5(3) 1_565 2_755
Na6 Na1 Na11 113.5(2) 1_565 2_755
U3 Na1 Na11 82.11(16) 2_755 2_755
As6 Na1 Na11 64.26(14) . 2_755
O17 Na1 Na7 133.8(3) . 2_765
O18 Na1 Na7 46.1(2) 1_565 2_765
O8 Na1 Na7 60.1(3) 2_755 2_765
O25 Na1 Na7 128.8(3) . 2_765
O15 Na1 Na7 123.1(3) 2_755 2_765
O24 Na1 Na7 75.0(3) 2_755 2_765
O24 Na1 Na7 46.9(2) 1_565 2_765
Na6 Na1 Na7 81.18(17) 1_565 2_765
U3 Na1 Na7 81.83(15) 2_755 2_765
As6 Na1 Na7 119.74(18) . 2_765
Na11 Na1 Na7 161.8(2) 2_755 2_765
O4 Na2 O6 80.9(3) . 1_545
O4 Na2 O5 80.5(3) . 2_645
O6 Na2 O5 160.9(4) 1_545 2_645
O4 Na2 O2 165.1(4) . 2_645
O6 Na2 O2 87.3(3) 1_545 2_645
O5 Na2 O2 111.7(4) 2_645 2_645
O4 Na2 O35 101.3(4) . 2_645
O6 Na2 O35 107.9(4) 1_545 2_645
O5 Na2 O35 80.1(4) 2_645 2_645
O2 Na2 O35 73.5(4) 2_645 2_645
O4 Na2 O31 110.7(3) . 2_645
O6 Na2 O31 113.0(4) 1_545 2_645
O5 Na2 O31 70.0(3) 2_645 2_645
O2 Na2 O31 82.3(3) 2_645 2_645
O35 Na2 O31 130.9(4) 2_645 2_645
O4 Na2 O16 60.1(3) . .
O6 Na2 O16 62.1(3) 1_545 .
O5 Na2 O16 104.3(3) 2_645 .
O2 Na2 O16 121.7(4) 2_645 .
O35 Na2 O16 159.1(4) 2_645 .
O31 Na2 O16 68.7(3) 2_645 .
O4 Na2 As4 29.8(2) . .
O6 Na2 As4 72.6(2) 1_545 .
O5 Na2 As4 89.1(3) 2_645 .
O2 Na2 As4 151.7(3) 2_645 .
O35 Na2 As4 131.1(3) 2_645 .
O31 Na2 As4 87.3(2) 2_645 .
O16 Na2 As4 30.73(18) . .
O4 Na2 As6 74.2(2) . 1_545
O6 Na2 As6 27.8(2) 1_545 1_545
O5 Na2 As6 145.8(3) 2_645 1_545
O2 Na2 As6 91.2(3) 2_645 1_545
O35 Na2 As6 82.7(3) 2_645 1_545
O31 Na2 As6 140.8(3) 2_645 1_545
O16 Na2 As6 82.7(2) . 1_545
As4 Na2 As6 80.36(13) . 1_545
O4 Na2 U1 84.4(3) . 1_545
O6 Na2 U1 32.6(2) 1_545 1_545
O5 Na2 U1 140.0(3) 2_645 1_545
O2 Na2 U1 90.7(3) 2_645 1_545
O35 Na2 U1 139.4(3) 2_645 1_545
O31 Na2 U1 81.3(2) 2_645 1_545
O16 Na2 U1 37.38(18) . 1_545
As4 Na2 U1 61.59(11) . 1_545
As6 Na2 U1 60.03(10) 1_545 1_545
O4 Na2 Na5 57.7(2) . 2_655
O6 Na2 Na5 132.5(3) 1_545 2_655
O5 Na2 Na5 35.2(3) 2_645 2_655
O2 Na2 Na5 127.9(3) 2_645 2_655
O35 Na2 Na5 63.9(3) 2_645 2_655
O31 Na2 Na5 103.5(2) 2_645 2_655
O16 Na2 Na5 108.0(2) . 2_655
As4 Na2 Na5 80.13(14) . 2_655
As6 Na2 Na5 110.71(19) 1_545 2_655
U1 Na2 Na5 141.31(17) 1_545 2_655
O4 Na2 U3 31.1(2) . .
O6 Na2 U3 79.0(3) 1_545 .
O5 Na2 U3 87.4(3) 2_645 .
O2 Na2 U3 137.2(3) 2_645 .
O35 Na2 U3 72.7(3) 2_645 .
O31 Na2 U3 140.3(2) 2_645 .
O16 Na2 U3 87.0(2) . .
As4 Na2 U3 59.24(10) . .
As6 Na2 U3 59.28(10) 1_545 .
U1 Na2 U3 98.33(13) 1_545 .
Na5 Na2 U3 53.59(12) 2_655 .
O33 Na3 O27 132.9(4) 1_554 2_744
O33 Na3 O39 130.7(5) 1_554 2_744
O27 Na3 O39 84.6(5) 2_744 2_744
O33 Na3 O38 96.3(5) 1_554 2_744
O27 Na3 O38 100.0(5) 2_744 2_744
O39 Na3 O38 38.4(6) 2_744 2_744
O33 Na3 O12 66.5(3) 1_554 .
O27 Na3 O12 111.1(3) 2_744 .
O39 Na3 O12 137.5(5) 2_744 .
O38 Na3 O12 148.5(5) 2_744 .
O33 Na3 O28 128.8(4) 1_554 2_744
O27 Na3 O28 92.5(4) 2_744 2_744
O39 Na3 O28 62.9(5) 2_744 2_744
O38 Na3 O28 97.3(5) 2_744 2_744
O12 Na3 O28 76.7(3) . 2_744
O33 Na3 O21 79.7(3) 1_554 2_755
O27 Na3 O21 67.1(3) 2_744 2_755
O39 Na3 O21 92.3(5) 2_744 2_755
O38 Na3 O21 66.8(5) 2_744 2_755
O12 Na3 O21 130.2(3) . 2_755
O28 Na3 O21 150.0(4) 2_744 2_755
O33 Na3 O28 67.2(4) 1_554 .
O27 Na3 O28 159.3(4) 2_744 .
O39 Na3 O28 82.4(5) 2_744 .
O38 Na3 O28 79.6(5) 2_744 .
O12 Na3 O28 69.5(3) . .
O28 Na3 O28 67.2(4) 2_744 .
O21 Na3 O28 129.4(3) 2_755 .
O33 Na3 U4 43.4(2) 1_554 .
O27 Na3 U4 157.8(3) 2_744 .
O39 Na3 U4 113.6(4) 2_744 .
O38 Na3 U4 102.2(4) 2_744 .
O12 Na3 U4 46.96(19) . .
O28 Na3 U4 85.4(3) 2_744 .
O21 Na3 U4 121.8(3) 2_755 .
O28 Na3 U4 31.3(2) . .
O33 Na3 As8 122.7(3) 1_554 2_744
O27 Na3 As8 74.9(2) 2_744 2_744
O39 Na3 As8 24.5(4) 2_744 2_744
O38 Na3 As8 28.0(4) 2_744 2_744
O12 Na3 As8 161.9(3) . 2_744
O28 Na3 As8 86.2(3) 2_744 2_744
O21 Na3 As8 67.8(2) 2_755 2_744
O28 Na3 As8 98.7(3) . 2_744
U4 Na3 As8 126.86(16) . 2_744
O33 Na3 As7 152.9(3) 1_554 2_744
O27 Na3 As7 25.1(2) 2_744 2_744
O39 Na3 As7 74.5(4) 2_744 2_744
O38 Na3 As7 103.1(4) 2_744 2_744
O12 Na3 As7 102.9(2) . 2_744
O28 Na3 As7 67.5(3) 2_744 2_744
O21 Na3 As7 90.7(2) 2_755 2_744
O28 Na3 As7 134.6(3) . 2_744
U4 Na3 As7 144.79(18) . 2_744
As8 Na3 As7 75.13(11) 2_744 2_744
O33 Na3 Na8 98.7(3) 1_554 2_744
O27 Na3 Na8 43.2(2) 2_744 2_744
O39 Na3 Na8 127.0(4) 2_744 2_744
O38 Na3 Na8 137.4(4) 2_744 2_744
O12 Na3 Na8 73.3(2) . 2_744
O28 Na3 Na8 103.5(3) 2_744 2_744
O21 Na3 Na8 77.1(2) 2_755 2_744
O28 Na3 Na8 142.8(3) . 2_744
U4 Na3 Na8 115.96(17) . 2_744
As8 Na3 Na8 117.04(17) 2_744 2_744
As7 Na3 Na8 54.30(12) 2_744 2_744
O1 Na4 O3 111.7(4) 2_644 2_645
O1 Na4 O14 85.5(3) 2_644 .
O3 Na4 O14 154.6(4) 2_645 .
O1 Na4 O11 166.4(4) 2_644 .
O3 Na4 O11 81.0(3) 2_645 .
O14 Na4 O11 84.2(3) . .
O1 Na4 O34 71.5(4) 2_644 2_644
O3 Na4 O34 77.9(4) 2_645 2_644
O14 Na4 O34 91.0(4) . 2_644
O11 Na4 O34 117.5(4) . 2_644
O1 Na4 O7 81.8(3) 2_644 2_645
O3 Na4 O7 72.8(3) 2_645 2_645
O14 Na4 O7 130.0(3) . 2_645
O11 Na4 O7 98.2(4) . 2_645
O34 Na4 O7 129.0(4) 2_644 2_645
O1 Na4 O26 75.3(3) 2_644 .
O3 Na4 O26 141.5(4) 2_645 .
O14 Na4 O26 59.1(3) . .
O11 Na4 O26 91.8(3) . .
O34 Na4 O26 136.7(4) 2_644 .
O7 Na4 O26 70.8(3) 2_645 .
O1 Na4 As7 91.1(3) 2_644 .
O3 Na4 As7 153.9(3) 2_645 .
O14 Na4 As7 32.7(2) . .
O11 Na4 As7 75.5(2) . .
O34 Na4 As7 123.2(3) 2_644 .
O7 Na4 As7 99.3(3) 2_645 .
O26 Na4 As7 31.0(2) . .
O1 Na4 As8 151.9(3) 2_644 .
O3 Na4 As8 83.4(3) 2_645 .
O14 Na4 As8 73.7(2) . .
O11 Na4 As8 29.3(2) . .
O34 Na4 As8 89.9(3) 2_644 .
O7 Na4 As8 126.1(3) 2_645 .
O26 Na4 As8 108.1(3) . .
As7 Na4 As8 81.63(13) . .
O1 Na4 Na10 137.1(3) 2_644 1_544
O3 Na4 Na10 41.8(3) 2_645 1_544
O14 Na4 Na10 133.3(3) . 1_544
O11 Na4 Na10 50.3(3) . 1_544
O34 Na4 Na10 116.6(3) 2_644 1_544
O7 Na4 Na10 60.1(2) 2_645 1_544
O26 Na4 Na10 106.6(3) . 1_544
As7 Na4 Na10 112.5(2) . 1_544
As8 Na4 Na10 69.82(15) . 1_544
O1 Na4 Na12 42.7(3) 2_644 2_634
O3 Na4 Na12 133.5(3) 2_645 2_634
O14 Na4 Na12 49.7(3) . 2_634
O11 Na4 Na12 131.3(3) . 2_634
O34 Na4 Na12 58.4(3) 2_644 2_634
O7 Na4 Na12 122.0(3) 2_645 2_634
O26 Na4 Na12 78.3(3) . 2_634
As7 Na4 Na12 72.10(16) . 2_634
As8 Na4 Na12 109.7(2) . 2_634
Na10 Na4 Na12 175.0(2) 1_544 2_634
O1 Na4 As3 87.7(3) 2_644 2_645
O3 Na4 As3 24.2(2) 2_645 2_645
O14 Na4 As3 162.6(3) . 2_645
O11 Na4 As3 104.6(3) . 2_645
O34 Na4 As3 71.6(3) 2_644 2_645
O7 Na4 As3 64.6(2) 2_645 2_645
O26 Na4 As3 134.0(3) . 2_645
As7 Na4 As3 163.8(2) . 2_645
As8 Na4 As3 106.55(15) . 2_645
Na10 Na4 As3 59.61(13) 1_544 2_645
Na12 Na4 As3 116.5(2) 2_634 2_645
O36 Na5 O13 131.9(5) 2_655 .
O36 Na5 O41 37.8(6) 2_655 2_655
O13 Na5 O41 132.8(5) . 2_655
O36 Na5 O3 102.4(5) 2_655 1_565
O13 Na5 O3 123.3(4) . 1_565
O41 Na5 O3 78.9(5) 2_655 1_565
O36 Na5 O5 115.5(5) 2_655 1_565
O13 Na5 O5 90.1(4) . 1_565
O41 Na5 O5 137.0(5) 2_655 1_565
O3 Na5 O5 77.8(3) 1_565 1_565
O36 Na5 O35 57.3(5) 2_655 2_655
O13 Na5 O35 77.6(4) . 2_655
O41 Na5 O35 85.5(5) 2_655 2_655
O3 Na5 O35 159.1(4) 1_565 2_655
O5 Na5 O35 105.3(4) 1_565 2_655
O36 Na5 O10 111.1(5) 2_655 .
O13 Na5 O10 64.8(3) . .
O41 Na5 O10 79.4(5) 2_655 .
O3 Na5 O10 83.5(3) 1_565 .
O5 Na5 O10 132.4(4) 1_565 .
O35 Na5 O10 107.4(4) 2_655 .
O36 Na5 As6 126.7(5) 2_655 .
O13 Na5 As6 32.4(2) . .
O41 Na5 As6 106.6(5) 2_655 .
O3 Na5 As6 105.6(3) 1_565 .
O5 Na5 As6 114.2(3) 1_565 .
O35 Na5 As6 92.1(3) 2_655 .
O10 Na5 As6 32.44(19) . .
O36 Na5 Na10 83.4(4) 2_655 2_666
O13 Na5 Na10 139.5(3) . 2_666
O41 Na5 Na10 86.5(4) 2_655 2_666
O3 Na5 Na10 44.1(3) 1_565 2_666
O5 Na5 Na10 52.1(3) 1_565 2_666
O35 Na5 Na10 121.6(4) 2_655 2_666
O10 Na5 Na10 127.6(3) . 2_666
As6 Na5 Na10 145.1(2) . 2_666
O36 Na5 As1 143.5(5) 2_655 1_565
O13 Na5 As1 71.2(3) . 1_565
O41 Na5 As1 151.2(4) 2_655 1_565
O3 Na5 As1 73.3(3) 1_565 1_565
O5 Na5 As1 28.1(2) 1_565 1_565
O35 Na5 As1 119.1(3) 2_655 1_565
O10 Na5 As1 104.5(3) . 1_565
As6 Na5 As1 88.29(13) . 1_565
Na10 Na5 As1 68.32(15) 2_666 1_565
O36 Na5 As3 129.4(4) 2_655 1_565
O13 Na5 As3 95.8(3) . 1_565
O41 Na5 As3 100.2(4) 2_655 1_565
O3 Na5 As3 27.5(2) 1_565 1_565
O5 Na5 As3 72.8(2) 1_565 1_565
O35 Na5 As3 173.3(3) 2_655 1_565
O10 Na5 As3 70.6(2) . 1_565
As6 Na5 As3 82.96(13) . 1_565
Na10 Na5 As3 62.67(14) 2_666 1_565
As1 Na5 As3 56.43(9) 1_565 1_565
O36 Na5 Na12 63.9(5) 2_655 2_645
O13 Na5 Na12 95.6(3) . 2_645
O41 Na5 Na12 37.8(5) 2_655 2_645
O3 Na5 Na12 94.8(3) 1_565 2_645
O5 Na5 Na12 172.3(3) 1_565 2_645
O35 Na5 Na12 81.0(3) 2_655 2_645
O10 Na5 Na12 47.2(3) . 2_645
As6 Na5 Na12 69.32(18) . 2_645
Na10 Na5 Na12 121.0(2) 2_666 2_645
As1 Na5 Na12 151.1(2) 1_565 2_645
As3 Na5 Na12 101.4(2) 1_565 2_645
O18 Na6 O9 97.3(3) . 2_745
O18 Na6 O22 106.1(4) . 1_545
O9 Na6 O22 106.9(3) 2_745 1_545
O18 Na6 O30 117.4(3) . 1_545
O9 Na6 O30 144.9(4) 2_745 1_545
O22 Na6 O30 60.4(3) 1_545 1_545
O18 Na6 O25 81.9(3) . 1_545
O9 Na6 O25 130.9(3) 2_745 1_545
O22 Na6 O25 120.6(3) 1_545 1_545
O30 Na6 O25 63.9(3) 1_545 1_545
O18 Na6 O30 116.9(3) . 2_745
O9 Na6 O30 64.3(3) 2_745 2_745
O22 Na6 O30 136.8(3) 1_545 2_745
O30 Na6 O30 101.3(3) 1_545 2_745
O25 Na6 O30 72.5(3) 1_545 2_745
O18 Na6 O25 172.3(4) . 2_745
O9 Na6 O25 75.1(3) 2_745 2_745
O22 Na6 O25 75.3(3) 1_545 2_745
O30 Na6 O25 70.0(3) 1_545 2_745
O25 Na6 O25 104.1(3) 1_545 2_745
O30 Na6 O25 61.5(3) 2_745 2_745
O18 Na6 Na1 46.6(2) . 1_545
O9 Na6 Na1 96.5(3) 2_745 1_545
O22 Na6 Na1 146.8(3) 1_545 1_545
O30 Na6 Na1 110.7(3) 1_545 1_545
O25 Na6 Na1 48.6(2) 1_545 1_545
O30 Na6 Na1 74.6(2) 2_745 1_545
O25 Na6 Na1 134.6(3) 2_745 1_545
O18 Na6 As4 29.0(2) . .
O9 Na6 As4 122.0(3) 2_745 .
O22 Na6 As4 83.7(2) 1_545 .
O30 Na6 As4 90.5(2) 1_545 .
O25 Na6 As4 77.5(2) 1_545 .
O30 Na6 As4 138.3(3) 2_745 .
O25 Na6 As4 156.5(3) 2_745 .
Na1 Na6 As4 63.85(13) 1_545 .
O18 Na6 Na6 136.0(3) . 2_735
O9 Na6 Na6 107.5(3) 2_745 2_735
O22 Na6 Na6 100.8(3) 1_545 2_735
O30 Na6 Na6 50.8(2) 1_545 2_735
O25 Na6 Na6 54.3(2) 1_545 2_735
O30 Na6 Na6 50.5(2) 2_745 2_735
O25 Na6 Na6 49.8(2) 2_745 2_735
Na1 Na6 Na6 93.9(2) 1_545 2_735
As4 Na6 Na6 126.7(2) . 2_735
O18 Na6 As2 116.4(3) . 1_545
O9 Na6 As2 129.9(3) 2_745 1_545
O22 Na6 As2 31.2(2) 1_545 1_545
O30 Na6 As2 29.26(18) 1_545 1_545
O25 Na6 As2 91.7(2) 1_545 1_545
O30 Na6 As2 121.0(3) 2_745 1_545
O25 Na6 As2 68.8(2) 2_745 1_545
Na1 Na6 As2 133.57(18) 1_545 1_545
As4 Na6 As2 87.73(13) . 1_545
Na6 Na6 As2 73.77(19) 2_735 1_545
O18 Na6 Na8 84.8(3) . 2_734
O9 Na6 Na8 44.2(2) 2_745 2_734
O22 Na6 Na8 70.0(2) 1_545 2_734
O30 Na6 Na8 129.3(3) 1_545 2_734
O25 Na6 Na8 165.0(3) 1_545 2_734
O30 Na6 Na8 107.8(3) 2_745 2_734
O25 Na6 Na8 88.6(2) 2_745 2_734
Na1 Na6 Na8 116.6(2) 1_545 2_734
As4 Na6 Na8 94.15(17) . 2_734
Na6 Na6 Na8 137.7(3) 2_735 2_734
As2 Na6 Na8 100.51(16) 1_545 2_734
O38 Na7 O40 38.4(6) 2_755 2_755
O38 Na7 O20 122.9(5) 2_755 1_565
O40 Na7 O20 154.8(5) 2_755 1_565
O38 Na7 O18 119.2(5) 2_755 2_755
O40 Na7 O18 88.3(5) 2_755 2_755
O20 Na7 O18 93.2(3) 1_565 2_755
O38 Na7 O17 79.0(5) 2_755 .
O40 Na7 O17 93.9(5) 2_755 .
O20 Na7 O17 97.9(4) 1_565 .
O18 Na7 O17 147.9(4) 2_755 .
O38 Na7 O24 93.8(5) 2_755 2_755
O40 Na7 O24 61.3(5) 2_755 2_755
O20 Na7 O24 142.6(4) 1_565 2_755
O18 Na7 O24 72.1(3) 2_755 2_755
O17 Na7 O24 81.0(3) . 2_755
O38 Na7 O21 67.1(4) 2_755 2_766
O40 Na7 O21 79.7(5) 2_755 2_766
O20 Na7 O21 75.9(3) 1_565 2_766
O18 Na7 O21 79.3(3) 2_755 2_766
O17 Na7 O21 132.6(4) . 2_766
O24 Na7 O21 131.3(4) 2_755 2_766
O38 Na7 Na1 140.4(4) 2_755 2_765
O40 Na7 Na1 102.4(5) 2_755 2_765
O20 Na7 Na1 95.9(3) 1_565 2_765
O18 Na7 Na1 43.6(2) 2_755 2_765
O17 Na7 Na1 105.1(3) . 2_765
O24 Na7 Na1 49.6(3) 2_755 2_765
O21 Na7 Na1 122.2(3) 2_766 2_765
O38 Na7 As1 150.7(4) 2_755 1_565
O40 Na7 As1 162.6(5) 2_755 1_565
O20 Na7 As1 27.9(2) 1_565 1_565
O18 Na7 As1 74.7(2) 2_755 1_565
O17 Na7 As1 102.6(3) . 1_565
O24 Na7 As1 115.4(3) 2_755 1_565
O21 Na7 As1 93.0(2) 2_766 1_565
Na1 Na7 As1 68.07(14) 2_765 1_565
O38 Na7 Na11 39.2(4) 2_755 2_755
O40 Na7 Na11 59.7(5) 2_755 2_755
O20 Na7 Na11 119.8(3) 1_565 2_755
O18 Na7 Na11 146.5(3) 2_755 2_755
O17 Na7 Na11 40.1(3) . 2_755
O24 Na7 Na11 83.2(3) 2_755 2_755
O21 Na7 Na11 102.2(3) 2_766 2_755
Na1 Na7 Na11 129.0(2) 2_765 2_755
As1 Na7 Na11 137.7(2) 1_565 2_755
O38 Na7 As4 95.6(4) 2_755 2_755
O40 Na7 As4 64.6(4) 2_755 2_755
O20 Na7 As4 112.5(3) 1_565 2_755
O18 Na7 As4 24.1(2) 2_755 2_755
O17 Na7 As4 146.1(3) . 2_755
O24 Na7 As4 65.9(3) 2_755 2_755
O21 Na7 As4 71.8(2) 2_766 2_755
Na1 Na7 As4 58.88(13) 2_765 2_755
As1 Na7 As4 98.14(15) 1_565 2_755
Na11 Na7 As4 124.04(19) 2_755 2_755
O38 Na7 As6 96.7(4) 2_755 .
O40 Na7 As6 117.5(5) 2_755 .
O20 Na7 As6 74.9(3) 1_565 .
O18 Na7 As6 142.2(3) 2_755 .
O17 Na7 As6 23.8(2) . .
O24 Na7 As6 95.6(3) 2_755 .
O21 Na7 As6 129.5(3) 2_766 .
Na1 Na7 As6 101.03(17) 2_765 .
As1 Na7 As6 79.28(12) 1_565 .
Na11 Na7 As6 60.55(15) 2_755 .
As4 Na7 As6 158.42(17) 2_755 .
O29 Na8 O23 117.4(4) 1_544 2_744
O29 Na8 O9 105.9(4) 1_544 1_544
O23 Na8 O9 124.6(4) 2_744 1_544
O29 Na8 O27 71.3(3) 1_544 .
O23 Na8 O27 116.6(4) 2_744 .
O9 Na8 O27 108.6(4) 1_544 .
O29 Na8 O32 116.9(3) 1_544 .
O23 Na8 O32 118.5(4) 2_744 .
O9 Na8 O32 61.6(3) 1_544 .
O27 Na8 O32 59.1(3) . .
O29 Na8 As7 86.6(3) 1_544 .
O23 Na8 As7 134.1(3) 2_744 .
O9 Na8 As7 78.1(2) 1_544 .
O27 Na8 As7 31.4(2) . .
O32 Na8 As7 31.99(18) . .
O29 Na8 As3 26.9(2) 1_544 1_544
O23 Na8 As3 123.8(3) 2_744 1_544
O9 Na8 As3 83.1(2) 1_544 1_544
O27 Na8 As3 91.8(3) . 1_544
O32 Na8 As3 117.8(2) . 1_544
As7 Na8 As3 95.73(14) . 1_544
O29 Na8 As1 81.4(3) 1_544 1_544
O23 Na8 As1 130.9(3) 2_744 1_544
O9 Na8 As1 27.5(2) 1_544 1_544
O27 Na8 As1 112.3(3) . 1_544
O32 Na8 As1 83.7(2) . 1_544
As7 Na8 As1 88.63(14) . 1_544
As3 Na8 As1 56.47(9) 1_544 1_544
O29 Na8 As5 138.9(3) 1_544 2_744
O23 Na8 As5 25.8(2) 2_744 2_744
O9 Na8 As5 113.3(3) 1_544 2_744
O27 Na8 As5 105.7(3) . 2_744
O32 Na8 As5 92.7(2) . 2_744
As7 Na8 As5 112.29(17) . 2_744
As3 Na8 As5 149.5(2) 1_544 2_744
As1 Na8 As5 132.56(16) 1_544 2_744
O29 Na8 Na6 138.5(3) 1_544 2_734
O23 Na8 Na6 79.9(3) 2_744 2_734
O9 Na8 Na6 44.8(2) 1_544 2_734
O27 Na8 Na6 137.5(3) . 2_734
O32 Na8 Na6 78.5(2) . 2_734
As7 Na8 Na6 108.49(19) . 2_734
As3 Na8 Na6 111.65(17) 1_544 2_734
As1 Na8 Na6 61.29(13) 1_544 2_734
As5 Na8 Na6 71.61(14) 2_744 2_734
O29 Na8 Na3 95.4(3) 1_544 2_744
O23 Na8 Na3 76.3(3) 2_744 2_744
O9 Na8 Na3 133.5(3) 1_544 2_744
O27 Na8 Na3 40.9(2) . 2_744
O32 Na8 Na3 71.9(2) . 2_744
As7 Na8 Na3 62.20(13) . 2_744
As3 Na8 Na3 121.96(18) 1_544 2_744
As1 Na8 Na3 150.8(2) 1_544 2_744
As5 Na8 Na3 65.97(13) 2_744 2_744
Na6 Na8 Na3 126.0(2) 2_734 2_744
O29 Na8 U2 36.4(2) 1_544 1_544
O23 Na8 U2 111.6(3) 2_744 1_544
O9 Na8 U2 123.7(3) 1_544 1_544
O27 Na8 U2 38.5(2) . 1_544
O32 Na8 U2 95.7(2) . 1_544
As7 Na8 U2 64.23(9) . 1_544
As3 Na8 U2 62.16(9) 1_544 1_544
As1 Na8 U2 108.53(14) 1_544 1_544
As5 Na8 U2 118.89(14) 2_744 1_544
Na6 Na8 U2 168.52(19) 2_734 1_544
Na3 Na8 U2 59.91(12) 2_744 1_544
O26 Na9 O2 136.2(4) 2_634 1_545
O26 Na9 O16 135.1(4) 2_634 .
O2 Na9 O16 87.2(3) 1_545 .
O26 Na9 O1 84.7(3) 2_634 1_545
O2 Na9 O1 77.9(3) 1_545 1_545
O16 Na9 O1 122.9(4) . 1_545
O26 Na9 O31 80.6(3) 2_634 2_645
O2 Na9 O31 97.1(3) 1_545 2_645
O16 Na9 O31 83.3(3) . 2_645
O1 Na9 O31 152.6(4) 1_545 2_645
O26 Na9 O19 85.6(3) 2_634 .
O2 Na9 O19 131.9(4) 1_545 .
O16 Na9 O19 64.5(3) . .
O1 Na9 O19 85.8(3) 1_545 .
O31 Na9 O19 115.7(3) 2_645 .
O26 Na9 As4 110.1(3) 2_634 .
O2 Na9 As4 113.4(3) 1_545 .
O16 Na9 As4 32.5(2) . .
O1 Na9 As4 108.2(3) 1_545 .
O31 Na9 As4 98.6(2) 2_645 .
O19 Na9 As4 32.20(17) . .
O26 Na9 Na10 42.9(3) 2_634 1_544
O2 Na9 Na10 176.9(3) 1_545 1_544
O16 Na9 Na10 94.4(3) . 1_544
O1 Na9 Na10 99.0(3) 1_545 1_544
O31 Na9 Na10 85.8(3) 2_645 1_544
O19 Na9 Na10 47.1(2) . 1_544
As4 Na9 Na10 67.24(15) . 1_544
O26 Na9 Na12 89.3(3) 2_634 .
O2 Na9 Na12 50.6(2) 1_545 .
O16 Na9 Na12 135.6(3) . .
O1 Na9 Na12 45.0(3) 1_545 .
O31 Na9 Na12 111.5(3) 2_645 .
O19 Na9 Na12 130.8(3) . .
As4 Na9 Na12 146.7(2) . .
Na10 Na9 Na12 127.1(2) 1_544 .
O26 Na9 As2 153.3(3) 2_634 1_545
O2 Na9 As2 27.3(2) 1_545 1_545
O16 Na9 As2 70.6(2) . 1_545
O1 Na9 As2 71.7(2) 1_545 1_545
O31 Na9 As2 115.1(3) 2_645 1_545
O19 Na9 As2 104.5(2) . 1_545
As4 Na9 As2 89.60(14) . 1_545
Na10 Na9 As2 151.5(2) 1_544 1_545
Na12 Na9 As2 65.21(16) . 1_545
O26 Na9 As5 106.4(3) 2_634 1_545
O2 Na9 As5 73.1(2) 1_545 1_545
O16 Na9 As5 95.9(3) . 1_545
O1 Na9 As5 27.0(2) 1_545 1_545
O31 Na9 As5 170.2(3) 2_645 1_545
O19 Na9 As5 72.2(2) . 1_545
As4 Na9 As5 85.61(13) . 1_545
Na10 Na9 As5 104.03(18) 1_544 1_545
Na12 Na9 As5 62.52(15) . 1_545
As2 Na9 As5 55.78(9) 1_545 1_545
O26 Na9 As7 24.7(2) 2_634 2_634
O2 Na9 As7 112.4(3) 1_545 2_634
O16 Na9 As7 151.7(3) . 2_634
O1 Na9 As7 82.6(2) 1_545 2_634
O31 Na9 As7 74.4(2) 2_645 2_634
O19 Na9 As7 109.9(2) . 2_634
As4 Na9 As7 134.15(18) . 2_634
Na10 Na9 As7 67.08(14) 1_544 2_634
Na12 Na9 As7 70.40(16) . 2_634
As2 Na9 As7 134.97(16) 1_545 2_634
As5 Na9 As7 108.97(13) 1_545 2_634
O26 Na10 O3 121.8(4) 2_645 2_656
O26 Na10 O19 92.1(4) 2_645 1_566
O3 Na10 O19 145.9(4) 2_656 1_566
O26 Na10 O5 95.5(4) 2_645 2_656
O3 Na10 O5 76.9(3) 2_656 2_656
O19 Na10 O5 106.0(4) 1_566 2_656
O26 Na10 O11 140.7(4) 2_645 1_566
O3 Na10 O11 80.1(4) 2_656 1_566
O19 Na10 O11 69.8(3) 1_566 1_566
O5 Na10 O11 122.6(3) 2_656 1_566
O26 Na10 O7 78.8(3) 2_645 .
O3 Na10 O7 114.6(4) 2_656 .
O19 Na10 O7 64.6(3) 1_566 .
O5 Na10 O7 168.5(4) 2_656 .
O11 Na10 O7 61.9(3) 1_566 .
O26 Na10 Na5 140.9(4) 2_645 2_666
O3 Na10 Na5 47.4(3) 2_656 2_666
O19 Na10 Na5 109.1(3) 1_566 2_666
O5 Na10 Na5 47.8(3) 2_656 2_666
O11 Na10 Na5 78.4(3) 1_566 2_666
O7 Na10 Na5 139.8(3) . 2_666
O26 Na10 Na9 45.8(3) 2_645 1_566
O3 Na10 Na9 159.7(3) 2_656 1_566
O19 Na10 Na9 51.2(2) 1_566 1_566
O5 Na10 Na9 87.8(3) 2_656 1_566
O11 Na10 Na9 119.8(3) 1_566 1_566
O7 Na10 Na9 81.0(2) . 1_566
Na5 Na10 Na9 128.0(2) 2_666 1_566
O26 Na10 Na4 125.1(3) 2_645 1_566
O3 Na10 Na4 44.5(3) 2_656 1_566
O19 Na10 Na4 114.3(3) 1_566 1_566
O5 Na10 Na4 119.3(3) 2_656 1_566
O11 Na10 Na4 46.5(2) 1_566 1_566
O7 Na10 Na4 71.9(2) . 1_566
Na5 Na10 Na4 76.28(19) 2_666 1_566
Na9 Na10 Na4 152.9(2) 1_566 1_566
O26 Na10 As3 98.7(3) 2_645 2_656
O3 Na10 As3 24.2(2) 2_656 2_656
O19 Na10 As3 168.7(3) 1_566 2_656
O5 Na10 As3 69.7(2) 2_656 2_656
O11 Na10 As3 103.3(3) 1_566 2_656
O7 Na10 As3 120.8(3) . 2_656
Na5 Na10 As3 60.05(14) 2_666 2_656
Na9 Na10 As3 136.9(2) 1_566 2_656
Na4 Na10 As3 61.85(14) 1_566 2_656
O26 Na10 U2 100.7(3) 2_645 .
O3 Na10 U2 118.0(3) 2_656 .
O19 Na10 U2 43.5(2) 1_566 .
O5 Na10 U2 145.4(3) 2_656 .
O11 Na10 U2 42.3(2) 1_566 .
O7 Na10 U2 29.98(18) . .
Na5 Na10 U2 117.45(19) 2_666 .
Na9 Na10 U2 82.04(15) 1_566 .
Na4 Na10 U2 74.85(15) 1_566 .
As3 Na10 U2 136.18(18) 2_656 .
O26 Na10 As4 100.8(3) 2_645 1_566
O3 Na10 As4 133.7(3) 2_656 1_566
O19 Na10 As4 24.50(18) 1_566 1_566
O5 Na10 As4 82.3(3) 2_656 1_566
O11 Na10 As4 77.2(2) 1_566 1_566
O7 Na10 As4 88.9(2) . 1_566
Na5 Na10 As4 88.56(17) 2_666 1_566
Na9 Na10 As4 55.04(13) 1_566 1_566
Na4 Na10 As4 123.38(19) 1_566 1_566
As3 Na10 As4 147.15(18) 2_656 1_566
U2 Na10 As4 64.74(10) . 1_566
O38 Na11 O17 86.3(5) . 2_755
O38 Na11 O12 101.3(5) . .
O17 Na11 O12 168.8(4) 2_755 .
O38 Na11 O28 88.2(5) . 2_744
O17 Na11 O28 88.5(4) 2_755 2_744
O12 Na11 O28 83.6(4) . 2_744
O38 Na11 O15 87.2(5) . .
O17 Na11 O15 88.6(3) 2_755 .
O12 Na11 O15 99.9(3) . .
O28 Na11 O15 174.7(4) 2_744 .
O38 Na11 O39 35.8(5) . .
O17 Na11 O39 120.8(5) 2_755 .
O12 Na11 O39 65.7(4) . .
O28 Na11 O39 80.8(5) 2_744 .
O15 Na11 O39 97.0(5) . .
O38 Na11 Na1 98.1(4) . 2_755
O17 Na11 Na1 44.1(3) 2_755 2_755
O12 Na11 Na1 140.7(3) . 2_755
O28 Na11 Na1 131.0(3) 2_744 2_755
O15 Na11 Na1 47.3(2) . 2_755
O39 Na11 Na1 128.8(4) . 2_755
O38 Na11 As5 115.3(5) . .
O17 Na11 As5 153.6(3) 2_755 .
O12 Na11 As5 26.7(2) . .
O28 Na11 As5 106.3(3) 2_744 .
O15 Na11 As5 78.1(2) . .
O39 Na11 As5 83.7(4) . .
Na1 Na11 As5 114.10(18) 2_755 .
O38 Na11 As8 27.6(4) . .
O17 Na11 As8 107.7(3) 2_755 .
O12 Na11 As8 82.2(3) . .
O28 Na11 As8 105.7(3) 2_744 .
O15 Na11 As8 71.1(2) . .
O39 Na11 As8 28.3(4) . .
Na1 Na11 As8 101.23(19) 2_755 .
As5 Na11 As8 89.64(15) . .
O38 Na11 As2 106.6(5) . .
O17 Na11 As2 106.7(3) 2_755 .
O12 Na11 As2 79.2(2) . .
O28 Na11 As2 159.2(4) 2_744 .
O15 Na11 As2 26.0(2) . .
O39 Na11 As2 102.4(4) . .
Na1 Na11 As2 62.54(13) 2_755 .
As5 Na11 As2 54.41(9) . .
As8 Na11 As2 83.65(15) . .
O38 Na11 Na7 42.0(4) . 2_755
O17 Na11 Na7 44.6(3) 2_755 2_755
O12 Na11 Na7 143.3(3) . 2_755
O28 Na11 Na7 91.9(3) 2_744 2_755
O15 Na11 Na7 82.9(3) . 2_755
O39 Na11 Na7 77.6(4) . 2_755
Na1 Na11 Na7 64.65(16) 2_755 2_755
As5 Na11 Na7 151.5(2) . 2_755
As8 Na11 Na7 63.96(15) . 2_755
As2 Na11 Na7 108.92(19) . 2_755
O38 Na11 Na3 40.5(4) . 2_744
O17 Na11 Na3 92.1(3) 2_755 2_744
O12 Na11 Na3 88.5(3) . 2_744
O28 Na11 Na3 48.3(3) 2_744 2_744
O15 Na11 Na3 127.4(3) . 2_744
O39 Na11 Na3 40.5(4) . 2_744
Na1 Na11 Na3 127.0(2) 2_755 2_744
As5 Na11 Na3 114.09(18) . 2_744
As8 Na11 Na3 58.74(13) . 2_744
As2 Na11 Na3 141.8(2) . 2_744
Na7 Na11 Na3 62.57(16) 2_755 2_744
O41 Na12 O1 126.2(6) 1_545 1_545
O41 Na12 O10 88.2(6) 1_545 2_645
O1 Na12 O10 144.6(5) 1_545 2_645
O41 Na12 O2 104.4(6) 1_545 1_545
O1 Na12 O2 76.1(3) 1_545 1_545
O10 Na12 O2 105.4(4) 2_645 1_545
O41 Na12 O37 40.1(6) 1_545 1_545
O1 Na12 O37 89.3(5) 1_545 1_545
O10 Na12 O37 120.1(5) 2_645 1_545
O2 Na12 O37 113.8(5) 1_545 1_545
O41 Na12 O14 136.0(6) 1_545 2_634
O1 Na12 O14 80.9(4) 1_545 2_634
O10 Na12 O14 66.7(3) 2_645 2_634
O2 Na12 O14 116.6(4) 1_545 2_634
O37 Na12 O14 124.2(5) 1_545 2_634
O41 Na12 O34 73.8(6) 1_545 2_634
O1 Na12 O34 114.5(4) 1_545 2_634
O10 Na12 O34 63.3(3) 2_645 2_634
O2 Na12 O34 168.4(4) 1_545 2_634
O37 Na12 O34 72.5(5) 1_545 2_634
O14 Na12 O34 62.9(3) 2_634 2_634
O41 Na12 Na9 148.3(6) 1_545 .
O1 Na12 Na9 47.5(2) 1_545 .
O10 Na12 Na9 108.1(3) 2_645 .
O2 Na12 Na9 45.8(2) 1_545 .
O37 Na12 Na9 131.8(5) 1_545 .
O14 Na12 Na9 75.7(3) 2_634 .
O34 Na12 Na9 137.8(4) 2_634 .
O41 Na12 Na5 44.3(5) 1_545 2_645
O1 Na12 Na5 162.2(4) 1_545 2_645
O10 Na12 Na5 50.6(3) 2_645 2_645
O2 Na12 Na5 91.3(3) 1_545 2_645
O37 Na12 Na5 84.3(4) 1_545 2_645
O14 Na12 Na5 116.4(3) 2_634 2_645
O34 Na12 Na5 79.3(3) 2_634 2_645
Na9 Na12 Na5 129.4(2) . 2_645
O41 Na12 Na4 131.4(5) 1_545 2_634
O1 Na12 Na4 42.1(3) 1_545 2_634
O10 Na12 Na4 111.0(3) 2_645 2_634
O2 Na12 Na4 111.9(3) 1_545 2_634
O37 Na12 Na4 94.4(4) 1_545 2_634
O14 Na12 Na4 45.2(2) 2_634 2_634
O34 Na12 Na4 76.3(3) 2_634 2_634
Na9 Na12 Na4 68.77(19) . 2_634
Na5 Na12 Na4 154.8(3) 2_645 2_634
O41 Na12 U4 96.2(5) 1_545 2_634
O1 Na12 U4 116.0(3) 1_545 2_634
O10 Na12 U4 43.2(2) 2_645 2_634
O2 Na12 U4 142.2(3) 1_545 2_634
O37 Na12 U4 102.4(4) 1_545 2_634
O14 Na12 U4 40.8(2) 2_634 2_634
O34 Na12 U4 30.0(2) 2_634 2_634
Na9 Na12 U4 114.4(2) . 2_634
Na5 Na12 U4 81.62(16) 2_645 2_634
Na4 Na12 U4 74.10(17) 2_634 2_634
O41 Na12 As5 104.5(6) 1_545 1_545
O1 Na12 As5 23.9(2) 1_545 1_545
O10 Na12 As5 167.1(3) 2_645 1_545
O2 Na12 As5 69.5(2) 1_545 1_545
O37 Na12 As5 72.4(4) 1_545 1_545
O14 Na12 As5 104.3(3) 2_634 1_545
O34 Na12 As5 122.1(3) 2_634 1_545
Na9 Na12 As5 59.65(14) . 1_545
Na5 Na12 As5 139.3(3) 2_645 1_545
Na4 Na12 As5 62.24(15) 2_634 1_545
U4 Na12 As5 135.1(2) 2_634 1_545
As5 O1 Na4 128.7(5) . 2_644
As5 O1 Na12 120.6(5) . 1_565
Na4 O1 Na12 95.2(4) 2_644 1_565
As5 O1 Na9 110.3(4) . 1_565
Na4 O1 Na9 106.5(4) 2_644 1_565
Na12 O1 Na9 87.5(3) 1_565 1_565
As2 O2 Na9 110.5(5) . 1_565
As2 O2 Na2 119.5(4) . 2_645
Na9 O2 Na2 111.5(4) 1_565 2_645
As2 O2 Na12 114.8(4) . 1_565
Na9 O2 Na12 83.7(3) 1_565 1_565
Na2 O2 Na12 111.3(4) 2_645 1_565
As3 O3 Na10 121.7(5) . 2_656
As3 O3 Na4 119.6(5) . 2_645
Na10 O3 Na4 93.7(4) 2_656 2_645
As3 O3 Na5 110.4(4) . 1_545
Na10 O3 Na5 88.5(4) 2_656 1_545
Na4 O3 Na5 118.4(4) 2_645 1_545
As4 O4 U3 131.5(4) . .
As4 O4 Na2 105.5(4) . .
U3 O4 Na2 116.0(4) . .
As1 O5 Na5 107.4(5) . 1_545
As1 O5 Na2 120.5(5) . 2_645
Na5 O5 Na2 109.5(4) 1_545 2_645
As1 O5 Na10 119.3(5) . 2_656
Na5 O5 Na10 80.1(3) 1_545 2_656
Na2 O5 Na10 111.8(4) 2_645 2_656
As6 O6 U1 136.4(5) . .
As6 O6 Na2 110.1(5) . 1_565
U1 O6 Na2 111.7(4) . 1_565
U2 O7 Na4 138.6(5) . 2_645
U2 O7 Na10 97.2(3) . .
Na4 O7 Na10 100.7(3) 2_645 .
As1 O8 U3 130.6(5) . .
As1 O8 Na1 141.0(5) . 2_755
U3 O8 Na1 88.3(3) . 2_755
As1 O9 Na8 111.6(4) . 1_566
As1 O9 Na6 114.7(4) . 2_745
Na8 O9 Na6 90.9(3) 1_566 2_745
As1 O9 U1 122.7(4) . .
Na8 O9 U1 119.5(3) 1_566 .
Na6 O9 U1 89.3(3) 2_745 .
As6 O10 U4 134.2(5) . 1_566
As6 O10 Na12 123.9(4) . 2_645
U4 O10 Na12 90.8(3) 1_566 2_645
As6 O10 Na5 90.4(4) . .
U4 O10 Na5 126.4(4) 1_566 .
Na12 O10 Na5 82.2(3) 2_645 .
As8 O11 U2 127.4(5) . 1_544
As8 O11 Na4 104.5(4) . .
U2 O11 Na4 120.1(4) 1_544 .
As8 O11 Na10 124.9(4) . 1_544
U2 O11 Na10 88.8(3) 1_544 1_544
Na4 O11 Na10 83.2(3) . 1_544
As5 O12 Na11 113.1(4) . .
As5 O12 U4 120.2(4) . .
Na11 O12 U4 115.4(4) . .
As5 O12 Na3 121.1(4) . .
Na11 O12 Na3 98.4(3) . .
U4 O12 Na3 83.8(3) . .
As6 O13 U3 133.6(5) . 1_565
As6 O13 Na5 99.7(4) . .
U3 O13 Na5 126.1(4) 1_565 .
As7 O14 U4 130.1(5) . .
As7 O14 Na4 96.4(4) . .
U4 O14 Na4 123.9(4) . .
As7 O14 Na12 125.2(4) . 2_634
U4 O14 Na12 89.6(3) . 2_634
Na4 O14 Na12 85.1(3) . 2_634
As2 O15 Na1 117.4(4) . 2_755
As2 O15 U3 122.4(4) . .
Na1 O15 U3 83.8(3) 2_755 .
As2 O15 Na11 112.3(4) . .
Na1 O15 Na11 84.8(3) 2_755 .
U3 O15 Na11 123.0(4) . .
As4 O16 U1 132.0(4) . 1_545
As4 O16 Na9 96.8(4) . .
U1 O16 Na9 130.6(4) 1_545 .
As4 O16 Na2 87.1(3) . .
U1 O16 Na2 93.4(3) 1_545 .
Na9 O16 Na2 96.5(3) . .
As6 O17 Na11 131.1(5) . 2_755
As6 O17 Na1 113.2(4) . .
Na11 O17 Na1 93.3(4) 2_755 .
As6 O17 Na7 118.1(5) . .
Na11 O17 Na7 95.3(4) 2_755 .
Na1 O17 Na7 99.4(4) . .
As4 O18 Na6 107.8(4) . .
As4 O18 Na1 116.5(4) . 1_545
Na6 O18 Na1 87.3(3) . 1_545
As4 O18 Na7 118.2(4) . 2_755
Na6 O18 Na7 129.3(4) . 2_755
Na1 O18 Na7 90.3(3) 1_545 2_755
As4 O19 U2 133.4(4) . 1_544
As4 O19 Na10 119.1(4) . 1_544
U2 O19 Na10 92.8(3) 1_544 1_544
As4 O19 Na9 93.6(3) . .
U2 O19 Na9 126.0(3) 1_544 .
Na10 O19 Na9 81.6(3) 1_544 .
As3 O20 As1 127.3(5) . .
As3 O20 Na7 120.4(5) . 1_545
As1 O20 Na7 112.2(4) . 1_545
U2 O21 Na3 108.6(4) . 2_755
U2 O21 Na7 137.5(4) . 2_766
Na3 O21 Na7 88.2(3) 2_755 2_766
As2 O22 As5 124.8(5) . .
As2 O22 Na6 100.5(4) . 1_565
As5 O22 Na6 131.5(5) . 1_565
As5 O23 Na8 118.0(5) . 2_744
As5 O23 U2 129.3(5) . 1_554
Na8 O23 U2 112.4(4) 2_744 1_554
U3 O24 Na1 101.2(4) . 2_755
U3 O24 Na7 124.5(5) . 2_755
Na1 O24 Na7 95.2(4) 2_755 2_755
U3 O24 Na1 132.1(5) . 1_545
Na1 O24 Na1 115.1(4) 2_755 1_545
Na7 O24 Na1 83.5(3) 2_755 1_545
U1 O25 Na1 129.9(5) . .
U1 O25 Na6 107.9(4) . 1_565
Na1 O25 Na6 80.1(3) . 1_565
U1 O25 Na6 97.1(4) . 2_745
Na1 O25 Na6 132.0(4) . 2_745
Na6 O25 Na6 75.9(3) 1_565 2_745
As7 O26 Na10 147.3(6) . 2_645
As7 O26 Na9 118.8(5) . 2_634
Na10 O26 Na9 91.3(4) 2_645 2_634
As7 O26 Na4 83.0(4) . .
Na10 O26 Na4 109.0(4) 2_645 .
Na9 O26 Na4 93.6(3) 2_634 .
As7 O27 Na3 119.5(5) . 2_744
As7 O27 Na8 100.3(4) . .
Na3 O27 Na8 95.9(4) 2_744 .
As7 O27 U2 130.3(5) . 1_544
Na3 O27 U2 101.0(3) 2_744 1_544
Na8 O27 U2 103.1(3) . 1_544
U4 O28 Na11 143.0(6) . 2_744
U4 O28 Na3 115.8(5) . 2_744
Na11 O28 Na3 95.3(4) 2_744 2_744
U4 O28 Na3 96.6(4) . .
Na11 O28 Na3 88.6(4) 2_744 .
Na3 O28 Na3 112.8(4) 2_744 .
As3 O29 Na8 115.1(4) . 1_566
As3 O29 U2 130.6(5) . .
Na8 O29 U2 109.8(4) 1_566 .
As2 O30 U1 134.2(5) . .
As2 O30 Na6 102.5(4) . 1_565
U1 O30 Na6 92.2(3) . 1_565
As2 O30 Na6 136.8(4) . 2_745
U1 O30 Na6 88.3(3) . 2_745
Na6 O30 Na6 78.7(3) 1_565 2_745
U1 O31 Na9 131.3(4) . 2_645
U1 O31 Na2 130.5(4) . 2_645
Na9 O31 Na2 96.9(3) 2_645 2_645
As7 O32 U1 128.4(5) . 1_544
As7 O32 Na8 82.7(3) . .
U1 O32 Na8 107.1(3) 1_544 .
As3 O33 Na3 133.9(5) . 1_556
As3 O33 U4 129.4(5) . 1_556
Na3 O33 U4 94.8(4) 1_556 1_556
U4 O34 Na4 139.2(6) . 2_644
U4 O34 Na12 97.4(5) . 2_634
Na4 O34 Na12 108.3(4) 2_644 2_634
U3 O35 Na5 115.4(5) . 2_655
U3 O35 Na2 135.8(6) . 2_645
Na5 O35 Na2 106.1(5) 2_655 2_645
O41 O36 O40 120.1(13) . .
O41 O36 As8 63.4(9) . .
O40 O36 As8 57.7(8) . .
O41 O36 U3 157.6(12) . .
O40 O36 U3 74.3(8) . .
As8 O36 U3 131.5(9) . .
O41 O36 Na5 73.1(10) . 2_655
O40 O36 Na5 151.1(12) . 2_655
As8 O36 Na5 122.2(8) . 2_655
U3 O36 Na5 102.7(7) . 2_655
O39 O37 As8 61.1(9) . .
O39 O37 O41 121.0(14) . .
As8 O37 O41 60.6(9) . .
O39 O37 U4 75.7(9) . .
As8 O37 U4 134.8(9) . .
O41 O37 U4 162.9(12) . .
O39 O37 Na12 150.1(11) . 1_565
As8 O37 Na12 109.5(8) . 1_565
O41 O37 Na12 53.1(8) . 1_565
U4 O37 Na12 114.7(7) . 1_565
O40 O38 O39 115.4(13) . .
O40 O38 As8 58.3(8) . .
O39 O38 As8 58.7(8) . .
O40 O38 Na11 107.1(10) . .
O39 O38 Na11 87.7(9) . .
As8 O38 Na11 115.7(8) . .
O40 O38 Na7 70.9(9) . 2_755
O39 O38 Na7 169.3(11) . 2_755
As8 O38 Na7 124.4(8) . 2_755
Na11 O38 Na7 98.8(6) . 2_755
O40 O38 Na3 150.3(11) . 2_744
O39 O38 Na3 68.8(8) . 2_744
As8 O38 Na3 111.1(7) . 2_744
Na11 O38 Na3 102.4(6) . 2_744
Na7 O38 Na3 101.4(6) 2_755 2_744
O37 O39 O38 122.4(13) . .
O37 O39 As8 63.8(9) . .
O38 O39 As8 65.6(9) . .
O37 O39 Na3 159.0(11) . 2_744
O38 O39 Na3 72.8(9) . 2_744
As8 O39 Na3 118.6(9) . 2_744
O37 O39 U4 66.7(9) . .
O38 O39 U4 162.5(12) . .
As8 O39 U4 128.7(9) . .
Na3 O39 U4 103.1(6) 2_744 .
O37 O39 Na11 108.5(10) . .
O38 O39 Na11 56.5(8) . .
As8 O39 Na11 100.1(7) . .
Na3 O39 Na11 91.9(6) 2_744 .
U4 O39 Na11 107.4(6) . .
O38 O40 As8 66.0(9) . .
O38 O40 O36 121.3(14) . .
As8 O40 O36 61.5(8) . .
O38 O40 Na7 70.7(9) . 2_755
As8 O40 Na7 130.9(9) . 2_755
O36 O40 Na7 167.4(11) . 2_755
O38 O40 U3 147.7(11) . .
As8 O40 U3 125.6(9) . .
O36 O40 U3 64.5(8) . .
Na7 O40 U3 103.4(6) 2_755 .
O36 O41 O37 114.4(14) . .
O36 O41 As8 63.1(9) . .
O37 O41 As8 59.5(9) . .
O36 O41 Na12 120.3(11) . 1_565
O37 O41 Na12 86.7(10) . 1_565
As8 O41 Na12 138.3(11) . 1_565
O36 O41 Na5 69.1(9) . 2_655
O37 O41 Na5 171.8(11) . 2_655
As8 O41 Na5 118.9(9) . 2_655
Na12 O41 Na5 97.9(7) 1_565 2_655
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
U1 O31 1.775(9) .
U1 O25 1.814(9) .
U1 O6 2.258(9) .
U1 O32 2.320(8) 1_566
U1 O16 2.366(8) 1_565
U1 O30 2.387(8) .
U1 O9 2.529(8) .
U1 Na6 3.464(5) 2_745
U1 Na6 3.573(5) 1_565
U1 Na1 3.890(6) .
U1 Na2 3.891(7) 1_565
U1 Na9 3.913(5) 2_645
U2 O7 1.757(9) .
U2 O21 1.782(9) .
U2 O11 2.349(9) 1_566
U2 O29 2.393(8) .
U2 O23 2.404(9) 1_556
U2 O19 2.406(7) 1_566
U2 O27 2.426(9) 1_566
U2 Na10 3.488(6) .
U2 Na3 3.660(6) 2_755
U2 Na8 3.795(5) 1_566
U2 Na8 3.878(6) 2_745
U2 Na4 4.116(6) 2_645
U3 O35 1.755(12) .
U3 O24 1.775(10) .
U3 O36 2.304(16) .
U3 O4 2.309(8) .
U3 O13 2.329(9) 1_545
U3 O8 2.367(8) .
U3 O40 2.457(16) .
U3 O15 2.499(8) .
U3 Na1 3.333(5) 2_755
U3 Na5 3.618(5) 2_655
U3 Na7 3.812(5) 2_755
U3 Na2 4.021(7) .
U4 O34 1.752(12) .
U4 O28 1.799(11) .
U4 O14 2.275(8) .
U4 O37 2.314(17) .
U4 O33 2.375(9) 1_554
U4 O10 2.385(8) 1_544
U4 O39 2.442(17) .
U4 O12 2.530(8) .
U4 Na3 3.442(5) .
U4 Na12 3.481(7) 2_634
U4 Na3 3.775(6) 2_744
U4 Na11 4.084(6) 2_744
As1 O5 1.644(10) .
As1 O9 1.673(8) .
As1 O8 1.683(9) .
As1 O20 1.770(9) .
As1 Na5 3.331(6) 1_545
As1 Na8 3.369(5) 1_566
As1 Na6 3.450(6) 2_745
As1 Na7 3.498(6) 1_545
As2 O2 1.640(9) .
As2 O15 1.657(8) .
As2 O30 1.683(8) .
As2 O22 1.772(9) .
As2 Na9 3.347(6) 1_565
As2 Na6 3.362(6) 1_565
As2 Na11 3.499(6) .
As3 O3 1.651(9) .
As3 O29 1.653(8) .
As3 O33 1.657(9) .
As3 O20 1.754(8) .
As3 Na8 3.304(6) 1_566
As3 Na5 3.348(5) 1_545
As3 Na10 3.433(6) 2_656
As3 Na4 3.509(6) 2_645
As4 O18 1.652(9) .
As4 O19 1.683(7) .
As4 O16 1.706(9) .
As4 O4 1.722(8) .
As4 Na9 3.152(5) .
As4 Na6 3.249(5) .
As4 Na2 3.335(6) .
As4 Na1 3.434(5) 1_545
As4 Na10 3.546(6) 1_544
As4 Na7 3.559(6) 2_755
As5 O1 1.640(9) .
As5 O12 1.661(8) .
As5 O23 1.667(9) .
As5 O22 1.787(8) .
As5 Na8 3.383(5) 2_744
As5 Na9 3.394(5) 1_565
As5 Na11 3.398(6) .
As5 Na12 3.489(7) 1_565
As6 O17 1.635(10) .
As6 O10 1.684(8) .
As6 O6 1.700(9) .
As6 O13 1.706(9) .
As6 Na5 3.139(6) .
As6 Na1 3.357(5) .
As6 Na2 3.421(6) 1_565
As6 Na7 3.569(6) .
As7 O26 1.636(10) .
As7 O27 1.692(9) .
As7 O32 1.705(8) .
As7 O14 1.716(8) .
As7 Na4 3.153(6) .
As7 Na8 3.193(6) .
As7 Na9 3.434(6) 2_634
As7 Na3 3.478(5) 2_744
As8 O40 1.627(17) .
As8 O39 1.638(17) .
As8 O37 1.679(18) .
As8 O11 1.682(9) .
As8 O36 1.693(16) .
As8 O41 1.698(18) .
As8 O38 1.747(16) .
As8 Na4 3.327(6) .
As8 Na11 3.403(7) .
As8 Na3 3.473(5) 2_744
As8 Na5 3.533(6) 2_655
As8 Na12 3.544(7) 1_565
Na1 O17 2.357(10) .
Na1 O18 2.362(9) 1_565
Na1 O8 2.419(10) 2_755
Na1 O25 2.469(10) .
Na1 O15 2.492(10) 2_755
Na1 O24 2.496(11) 2_755
Na1 O24 2.625(12) 1_565
Na1 Na6 3.245(7) 1_565
Na1 U3 3.333(5) 2_755
Na1 Na11 3.378(7) 2_755
Na1 Na7 3.423(8) 2_765
Na2 O4 2.432(10) .
Na2 O6 2.442(11) 1_545
Na2 O5 2.455(11) 2_645
Na2 O2 2.498(10) 2_645
Na2 O35 2.712(14) 2_645
Na2 O31 2.891(10) 2_645
Na2 O16 2.953(10) .
Na2 As6 3.421(6) 1_545
Na2 U1 3.891(7) 1_545
Na2 Na5 4.003(9) 2_655
Na3 O33 2.300(11) 1_554
Na3 O27 2.317(10) 2_744
Na3 O39 2.378(18) 2_744
Na3 O38 2.437(16) 2_744
Na3 O12 2.622(10) .
Na3 O28 2.627(13) 2_744
Na3 O21 2.680(11) 2_755
Na3 O28 2.736(12) .
Na3 As8 3.473(5) 2_744
Na3 As7 3.478(5) 2_744
Na3 Na8 3.519(7) 2_744
Na4 O1 2.330(10) 2_644
Na4 O3 2.386(10) 2_645
Na4 O14 2.463(10) .
Na4 O11 2.479(11) .
Na4 O34 2.595(13) 2_644
Na4 O7 2.631(11) 2_645
Na4 O26 2.902(10) .
Na4 Na10 3.394(8) 1_544
Na4 Na12 3.460(9) 2_634
Na4 As3 3.509(6) 2_645
Na5 O36 2.327(18) 2_655
Na5 O13 2.363(10) .
Na5 O41 2.383(19) 2_655
Na5 O3 2.393(10) 1_565
Na5 O5 2.446(11) 1_565
Na5 O35 2.500(13) 2_655
Na5 O10 2.638(11) .
Na5 Na10 3.251(7) 2_666
Na5 As1 3.331(6) 1_565
Na5 As3 3.348(5) 1_565
Na5 Na12 3.380(9) 2_645
Na6 O18 2.337(10) .
Na6 O9 2.398(9) 2_745
Na6 O22 2.552(10) 1_545
Na6 O30 2.569(10) 1_545
Na6 O25 2.571(9) 1_545
Na6 O30 2.581(10) 2_745
Na6 O25 2.736(10) 2_745
Na6 Na1 3.245(7) 1_545
Na6 Na6 3.266(11) 2_735
Na6 As2 3.362(6) 1_545
Na6 Na8 3.400(7) 2_734
Na7 O38 2.396(17) 2_755
Na7 O40 2.400(19) 2_755
Na7 O20 2.421(10) 1_565
Na7 O18 2.466(11) 2_755
Na7 O17 2.494(11) .
Na7 O24 2.514(10) 2_755
Na7 O21 2.694(10) 2_766
Na7 Na1 3.423(8) 2_765
Na7 As1 3.498(6) 1_565
Na7 Na11 3.537(8) 2_755
Na7 As4 3.559(6) 2_755
Na8 O29 2.245(10) 1_544
Na8 O23 2.263(10) 2_744
Na8 O9 2.372(9) 1_544
Na8 O27 2.421(10) .
Na8 O32 2.925(11) .
Na8 As3 3.304(6) 1_544
Na8 As1 3.369(5) 1_544
Na8 As5 3.383(5) 2_744
Na8 Na6 3.400(7) 2_734
Na8 Na3 3.519(7) 2_744
Na8 U2 3.795(5) 1_544
Na9 O26 2.332(11) 2_634
Na9 O2 2.399(11) 1_545
Na9 O16 2.455(9) .
Na9 O1 2.457(9) 1_545
Na9 O31 2.507(10) 2_645
Na9 O19 2.562(10) .
Na9 Na10 3.251(8) 1_544
Na9 Na12 3.329(8) .
Na9 As2 3.347(6) 1_545
Na9 As5 3.394(5) 1_545
Na9 As7 3.434(5) 2_634
Na10 O26 2.213(11) 2_645
Na10 O3 2.265(11) 2_656
Na10 O19 2.409(10) 1_566
Na10 O5 2.603(11) 2_656
Na10 O11 2.629(11) 1_566
Na10 O7 2.800(10) .
Na10 Na5 3.251(7) 2_666
Na10 Na9 3.251(8) 1_566
Na10 Na4 3.394(8) 1_566
Na10 As3 3.433(6) 2_656
Na10 As4 3.546(6) 1_566
Na11 O38 2.260(17) .
Na11 O17 2.288(11) 2_755
Na11 O12 2.384(10) .
Na11 O28 2.501(12) 2_744
Na11 O15 2.516(10) .
Na11 O39 2.709(17) .
Na11 Na1 3.378(7) 2_755
Na11 Na7 3.537(8) 2_755
Na11 Na3 3.663(8) 2_744
Na12 O41 2.092(19) 1_545
Na12 O1 2.356(11) 1_545
Na12 O10 2.502(11) 2_645
Na12 O2 2.587(11) 1_545
Na12 O37 2.611(18) 1_545
Na12 O14 2.650(12) 2_634
Na12 O34 2.792(13) 2_634
Na12 Na5 3.380(9) 2_645
Na12 Na4 3.460(9) 2_634
Na12 U4 3.481(7) 2_634
Na12 As5 3.489(7) 1_545
O1 Na4 2.330(10) 2_644
O1 Na12 2.356(11) 1_565
O1 Na9 2.457(9) 1_565
O2 Na9 2.399(11) 1_565
O2 Na2 2.498(10) 2_645
O2 Na12 2.587(10) 1_565
O3 Na10 2.265(11) 2_656
O3 Na4 2.386(10) 2_645
O3 Na5 2.393(10) 1_545
O5 Na5 2.446(11) 1_545
O5 Na2 2.455(11) 2_645
O5 Na10 2.603(11) 2_656
O6 Na2 2.442(11) 1_565
O7 Na4 2.631(11) 2_645
O8 Na1 2.419(10) 2_755
O9 Na8 2.372(9) 1_566
O9 Na6 2.398(9) 2_745
O10 U4 2.385(8) 1_566
O10 Na12 2.502(11) 2_645
O11 U2 2.349(9) 1_544
O11 Na10 2.629(11) 1_544
O13 U3 2.329(9) 1_565
O14 Na12 2.650(12) 2_634
O15 Na1 2.492(10) 2_755
O16 U1 2.366(8) 1_545
O17 Na11 2.288(11) 2_755
O18 Na1 2.362(9) 1_545
O18 Na7 2.466(11) 2_755
O19 U2 2.406(7) 1_544
O19 Na10 2.409(10) 1_544
O20 Na7 2.421(10) 1_545
O21 Na3 2.680(11) 2_755
O21 Na7 2.694(10) 2_766
O22 Na6 2.552(10) 1_565
O23 Na8 2.263(10) 2_744
O23 U2 2.404(9) 1_554
O24 Na1 2.496(11) 2_755
O24 Na7 2.514(10) 2_755
O24 Na1 2.625(12) 1_545
O25 Na6 2.571(9) 1_565
O25 Na6 2.736(10) 2_745
O26 Na10 2.213(11) 2_645
O26 Na9 2.332(11) 2_634
O27 Na3 2.317(10) 2_744
O27 U2 2.426(8) 1_544
O28 Na11 2.501(12) 2_744
O28 Na3 2.627(13) 2_744
O29 Na8 2.245(10) 1_566
O30 Na6 2.569(10) 1_565
O30 Na6 2.581(10) 2_745
O31 Na9 2.507(10) 2_645
O31 Na2 2.891(10) 2_645
O32 U1 2.320(8) 1_544
O33 Na3 2.300(11) 1_556
O33 U4 2.375(9) 1_556
O34 Na4 2.595(13) 2_644
O34 Na12 2.792(13) 2_634
O35 Na5 2.500(13) 2_655
O35 Na2 2.712(14) 2_645
O36 O41 1.53(2) .
O36 O40 1.68(2) .
O36 Na5 2.327(18) 2_655
O37 O39 1.54(2) .
O37 O41 1.69(2) .
O37 Na12 2.611(18) 1_565
O38 O40 1.58(2) .
O38 O39 1.59(2) .
O38 Na7 2.396(17) 2_755
O38 Na3 2.437(16) 2_744
O39 Na3 2.378(18) 2_744
O40 Na7 2.400(19) 2_755
O41 Na12 2.092(19) 1_565
O41 Na5 2.383(19) 2_655
_cod_duplicate_entry 7200609
