Crystallography Open Database

Information card for entry 7216173

Preview

Coordinates	7216173.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H42 K4 N4 O15 Pd2
Calculated formula	C40 H42 K4 N4 O15 Pd2
Title of publication	Solid-state cis‒trans isomerism in bis(oxamato)palladate(ii) complexes: synthesis, structural studies and catalytic activity
Authors of publication	Fortea-Pérez, Francisco R.; Marino, Nadia; Armentano, Donatella; De Munno, Giovanni; Julve, Miguel; Stiriba, Salah-Eddine
Journal of publication	CrystEngComm
Year of publication	2014
Journal volume	16
Journal issue	30
Pages of publication	6971
a	16.317 ± 0.002 Å
b	25.271 ± 0.002 Å
c	13.9855 ± 0.0014 Å
α	90°
β	124.893 ± 0.006°
γ	90°
Cell volume	4730.1 ± 0.9 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0203
Residual factor for significantly intense reflections	0.0199
Weighted residual factors for significantly intense reflections	0.049
Weighted residual factors for all reflections included in the refinement	0.0493
Goodness-of-fit parameter for all reflections included in the refinement	1.046
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180492 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/61.	7216173.cif
121580	2014-08-08	cif/ Updating files of 7216172, 7216173, 7216174, 7216175, 7216176 Original log message: Adding full bibliography for 7216172--7216176.cif.	7216173.cif
114585	2014-05-28	cif/ Adding structures of 7216172, 7216173, 7216174, 7216175, 7216176 via cif-deposit CGI script.	7216173.cif