Crystallography Open Database

Information card for entry 7216484

Preview

Coordinates	7216484.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H22 Ag4 Mo12 N12 Na O42 P
Calculated formula	C24 H18 Ag4 Mo12 N12 Na O41 P
Title of publication	Syntheses, crystal structures and properties of inorganic‒organic hybrids constructed from Keggin-type polyoxometalates and silver coordination compounds
Authors of publication	Zhou, Wei-Li; Liang, Jun; Qin, Chao; Shao, Kui-Zhan; Wang, Fang-Ming; Su, Zhong-Min
Journal of publication	CrystEngComm
Year of publication	2014
Journal volume	16
Journal issue	32
Pages of publication	7410
a	12.977 ± 0.005 Å
b	20.255 ± 0.005 Å
c	21.995 ± 0.005 Å
α	90 ± 0.005°
β	97.708 ± 0.005°
γ	90 ± 0.005°
Cell volume	5729 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0389
Residual factor for significantly intense reflections	0.0265
Weighted residual factors for significantly intense reflections	0.0517
Weighted residual factors for all reflections included in the refinement	0.0553
Goodness-of-fit parameter for all reflections included in the refinement	1.004
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180495 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/64.	7216484.cif
121636	2014-08-08	cif/ Updating files of 7216483, 7216484, 7216485, 7216486 Original log message: Adding full bibliography for 7216483--7216486.cif.	7216484.cif
116347	2014-06-10	cif/ Adding structures of 7216483, 7216484, 7216485, 7216486 via cif-deposit CGI script.	7216484.cif