Crystallography Open Database

Information card for entry 7217124

Preview

Coordinates	7217124.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H44 Ag4 N24 Na O41 P W12
Calculated formula	C28 H44 Ag4 N24 Na O41 P W12
Title of publication	Two unusual organic‒inorganic hybrid 3-D frameworks based on Keggin-type heteropoly blue anion-chains, 40-membered macrocycles, and sodium linker units
Authors of publication	Zhang, He; Yu, Kai; Gao, Song; Wang, Chun-Mei; Wang, Chun-Xiao; Wang, Hai-Yan; Zhou, Bai-Bin
Journal of publication	CrystEngComm
Year of publication	2014
Journal volume	16
Journal issue	36
Pages of publication	8449
a	10.9694 ± 0.0011 Å
b	13.6637 ± 0.0014 Å
c	13.9341 ± 0.0014 Å
α	64.8306 ± 0.0013°
β	73.1694 ± 0.0015°
γ	69.7887 ± 0.0015°
Cell volume	1748.6 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0513
Residual factor for significantly intense reflections	0.0659
Weighted residual factors for significantly intense reflections	0.0942
Weighted residual factors for all reflections included in the refinement	0.1076
Goodness-of-fit parameter for all reflections included in the refinement	1.167
Diffraction radiation wavelength	0.71 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180502 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/71.	7217124.cif
123412	2014-09-08	cif/ Updating files of 7217123, 7217124 Original log message: Adding full bibliography for 7217123--7217124.cif.	7217124.cif
120366	2014-07-15	cif/ Adding structures of 7217123, 7217124 via cif-deposit CGI script.	7217124.cif