Crystallography Open Database

Information card for entry 7217791

Preview

Coordinates	7217791.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H39 Cl Gd Ge N9 S3
Calculated formula	C12 H39 Cl Gd Ge N9 S3
Title of publication	Solvothermal syntheses of lanthanide thiogermanates displaying three new structural moieties
Authors of publication	Zhao, Rongqing; Zhou, Jian; Liu, Xing; Zhang, Li; Tang, Qiuling; Tan, XiaoFeng
Journal of publication	RSC Advances
Year of publication	2014
a	11.5484 ± 0.0014 Å
b	14.6767 ± 0.0017 Å
c	14.4271 ± 0.0017 Å
α	90°
β	96.332 ± 0.002°
γ	90°
Cell volume	2430.4 ± 0.5 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0247
Residual factor for significantly intense reflections	0.0213
Weighted residual factors for significantly intense reflections	0.0588
Weighted residual factors for all reflections included in the refinement	0.064
Goodness-of-fit parameter for all reflections included in the refinement	1.145
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	7217791.cif
122270	2014-08-20	cif/ Adding structures of 7217789, 7217790, 7217791, 7217792, 7217793 via cif-deposit CGI script.	7217791.cif