Crystallography Open Database

Information card for entry 7217800

Preview

Coordinates	7217800.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H72 F6 Ge14 N14 Ni2 O31
Calculated formula	C18 H56 F6 Ge14 N12 Ni2 O29
Title of publication	A family of germanates constructed from Ge7clusters co-templated by metal complexes and organic/inorganic species
Authors of publication	Ren, Xiaoyan; Pan, Qinhe; Liu, Jiancong; Li, Yi; Wang, Fuxiang; Li, Jiyang; Xu, Yan; Li, Li
Journal of publication	CrystEngComm
Year of publication	2014
Journal volume	16
Journal issue	40
Pages of publication	9545
a	8.8089 ± 0.0018 Å
b	22.436 ± 0.005 Å
c	31.193 ± 0.006 Å
α	90°
β	90°
γ	90°
Cell volume	6165 ± 2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	57
Hermann-Mauguin space group symbol	P b c m
Hall space group symbol	-P 2c 2b
Residual factor for all reflections	0.0355
Residual factor for significantly intense reflections	0.0296
Weighted residual factors for significantly intense reflections	0.0774
Weighted residual factors for all reflections included in the refinement	0.0796
Goodness-of-fit parameter for all reflections included in the refinement	1.064
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180509 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/78.	7217800.cif
124696	2014-10-06	cif/ Updating files of 7217797, 7217798, 7217799, 7217800 Original log message: Adding full bibliography for 7217797--7217800.cif.	7217800.cif
122327	2014-08-22	cif/ Adding structures of 7217797, 7217798, 7217799, 7217800 via cif-deposit CGI script.	7217800.cif