#------------------------------------------------------------------------------
#$Date: 2016-02-16 03:10:39 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176453 $
#$URL: svn://www.crystallography.net/cod/cif/7/21/79/7217912.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7217912
loop_
_publ_author_name
'Henkelis, James J.'
'Hardie, Michaele J.'
_publ_section_title
;
 Tuning the coordination chemistry of cyclotriveratrylene ligand pairs
 through alkyl chain aggregation
;
_journal_issue                   35
_journal_name_full               CrystEngComm
_journal_page_first              8138
_journal_paper_doi               10.1039/C4CE00467A
_journal_volume                  16
_journal_year                    2014
_chemical_formula_sum            'C129.5 H163.5 Ag2 B36 Co2 N7.5 O15'
_chemical_formula_weight         2787.94
_chemical_name_systematic
; 
{(+-)-2,7,12-tripropoxy-3,8,13-
tris(2-quinolylmethyl)-10,15-dihydro-5H-tribenzo[a,d,g]
cyclononene}silver(I) cobalt(III) bis(dicarbollide)
nitromethane 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.525(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   19.3628(7)
_cell_length_b                   43.7924(11)
_cell_length_c                   16.6371(6)
_cell_measurement_temperature    100(2)
_cell_volume                     14106.7(8)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'station I19 Diamond light source'
_diffrn_radiation_type           synchrotron
_diffrn_radiation_wavelength     0.68890
_diffrn_reflns_av_R_equivalents  0.0819
_diffrn_reflns_av_sigmaI/netI    0.0555
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       47
_diffrn_reflns_limit_k_min       -48
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            96831
_diffrn_reflns_theta_full        22.50
_diffrn_reflns_theta_max         22.50
_diffrn_reflns_theta_min         1.56
_exptl_absorpt_coefficient_mu    0.567
_exptl_absorpt_correction_T_max  0.9455
_exptl_absorpt_correction_T_min  0.8854
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.313
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             5764
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.10
_refine_diff_density_max         2.432
_refine_diff_density_min         -2.729
_refine_diff_density_rms         0.137
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.377
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           fullcycle
_refine_ls_number_parameters     1633
_refine_ls_number_reflns         20256
_refine_ls_number_restraints     2
_refine_ls_restrained_S_all      1.378
_refine_ls_R_factor_all          0.1350
_refine_ls_R_factor_gt           0.1128
_refine_ls_shift/su_max          0.018
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.2000P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3054
_refine_ls_wR_factor_ref         0.3462
_reflns_number_gt                15562
_reflns_number_total             20256
_reflns_threshold_expression     >2sigma(I)
_cod_duplicate_entry             7216489
_cod_data_source_file            c4ce00467a2.cif
_cod_data_source_block           c:
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/current/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 
;
_cod_original_sg_symbol_H-M      P21/c
_cod_original_formula_sum        'C129.50 H163.50 Ag2 B36 Co2 N7.50 O15'
_cod_database_code               7217912
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag -0.61348(5) 0.682892(15) 0.80069(6) 0.0558(2) Uani 1 1 d . . .
O1 O 0.1577(4) 0.53801(16) 0.4114(8) 0.095(3) Uani 1 1 d . . .
N1 N 0.3790(6) 0.5052(3) 0.5597(8) 0.089(3) Uiso 1 1 d . . .
C1 C 0.1884(6) 0.6214(2) 0.3805(6) 0.055(2) Uani 1 1 d . B .
B1 B 0.1694(7) 0.8011(3) 0.5073(10) 0.071(4) Uani 1 1 d . . .
H1 H 0.1342 0.7825 0.4859 0.085 Uiso 1 1 calc R . .
Ag2 Ag -0.11191(5) 0.683767(15) 0.64763(6) 0.0571(3) Uani 1 1 d . . .
O2 O 0.2908(4) 0.54045(16) 0.4448(6) 0.077(2) Uani 1 1 d . B .
N2 N 0.3963(4) 0.73197(17) 0.8232(5) 0.054(2) Uani 1 1 d . . .
H2 H 0.3834 0.7128 0.8173 0.065 Uiso 1 1 calc R . .
C2 C 0.1524(6) 0.5930(2) 0.3870(7) 0.063(3) Uani 1 1 d . . .
H39 H 0.1041 0.5924 0.3767 0.076 Uiso 1 1 calc R B .
B2 B 0.2265(6) 0.7958(3) 0.5871(8) 0.059(3) Uani 1 1 d . . .
H2A H 0.2281 0.7734 0.6196 0.071 Uiso 1 1 calc R . .
Co3 Co 0.29409(8) 0.86504(3) 0.58304(9) 0.0555(4) Uani 1 1 d . . .
O3 O 0.4516(4) 0.66563(14) 0.6196(4) 0.0572(17) Uani 1 1 d . B .
N3 N -0.1286(5) 0.63467(17) 0.6677(6) 0.058(2) Uani 1 1 d . . .
C3 C 0.1868(6) 0.5662(2) 0.4083(8) 0.068(3) Uani 1 1 d . B .
B3 B 0.2586(7) 0.7999(3) 0.4902(9) 0.065(3) Uani 1 1 d . . .
H3 H 0.2820 0.7803 0.4566 0.078 Uiso 1 1 calc R . .
Co4 Co -0.21562(9) 0.86566(3) 0.86092(10) 0.0649(4) Uani 1 1 d . . .
O4 O 0.3858(4) 0.71390(14) 0.6625(4) 0.0564(17) Uani 1 1 d . . .
N4 N -0.1064(4) 0.73319(17) 0.6255(5) 0.0496(19) Uani 1 1 d . . .
C4 C 0.2595(6) 0.5675(2) 0.4212(7) 0.062(3) Uani 1 1 d . . .
B4 B 0.2075(7) 0.8281(3) 0.4378(11) 0.072(4) Uani 1 1 d . . .
H4 H 0.1970 0.8280 0.3715 0.086 Uiso 1 1 calc R . .
O5 O 0.0409(4) 0.70404(15) 0.6495(5) 0.0580(17) Uani 1 1 d . . .
N5 N -0.1738(13) 0.4945(6) 0.8649(18) 0.205(10) Uani 1 1 d . . .
C5 C 0.2921(6) 0.5955(2) 0.4123(7) 0.059(3) Uani 1 1 d . B .
H5 H 0.3405 0.5966 0.4215 0.070 Uiso 1 1 calc R . .
B5 B 0.1447(8) 0.8400(3) 0.5091(10) 0.074(4) Uani 1 1 d . . .
H5A H 0.0925 0.8481 0.4891 0.089 Uiso 1 1 calc R . .
O6 O -0.0116(4) 0.65353(14) 0.5959(5) 0.064(2) Uani 1 1 d . B .
N6 N -0.6288(4) 0.63436(16) 0.7724(5) 0.050(2) Uani 1 1 d . . .
C6 C 0.2579(6) 0.6214(2) 0.3911(7) 0.057(3) Uani 1 1 d . . .
B6 B 0.1563(7) 0.8203(3) 0.5972(11) 0.068(4) Uani 1 1 d . . .
H6 H 0.1108 0.8150 0.6358 0.081 Uiso 1 1 calc R . .
O7 O -0.1134(4) 0.71414(14) 0.7860(4) 0.0528(16) Uani 1 1 d . . .
N7 N -0.4109(10) 0.5363(4) 0.8151(11) 0.135(5) Uiso 1 1 d . . .
C7 C 0.3016(6) 0.6508(2) 0.3809(7) 0.059(3) Uani 1 1 d . B .
H7A H 0.3459 0.6452 0.3554 0.071 Uiso 1 1 calc R . .
H7B H 0.2768 0.6648 0.3439 0.071 Uiso 1 1 calc R . .
B7 B 0.2402(6) 0.8300(3) 0.6399(8) 0.056(3) Uani 1 1 d . . .
H7 H 0.2494 0.8303 0.7065 0.068 Uiso 1 1 calc R . .
O8 O -0.0488(4) 0.66472(15) 0.8234(5) 0.0605(18) Uani 1 1 d . . .
N8 N -0.2566(18) 0.5294(7) 0.640(2) 0.129(5) Uiso 0.50 1 d PD A 1
C8 C 0.3169(5) 0.6675(2) 0.4581(7) 0.054(2) Uani 1 1 d . . .
B8 B 0.1910(6) 0.8553(2) 0.5871(8) 0.055(3) Uani 1 1 d . . .
H8 H 0.1656 0.8743 0.6210 0.065 Uiso 1 1 calc R . .
O9 O -0.2180(5) 0.5374(2) 0.9933(8) 0.109(4) Uani 1 1 d . . .
C9 C 0.3734(5) 0.6577(2) 0.5039(7) 0.056(3) Uani 1 1 d . B .
H9 H 0.3983 0.6402 0.4870 0.068 Uiso 1 1 calc R . .
B9 B 0.2203(6) 0.8599(3) 0.4959(8) 0.055(3) Uani 1 1 d . . .
H9A H 0.2157 0.8822 0.4633 0.066 Uiso 1 1 calc R . .
O10 O -0.3472(4) 0.53615(19) 1.0334(6) 0.086(3) Uani 1 1 d . . .
C10 C 0.3944(5) 0.6727(2) 0.5732(6) 0.053(2) Uani 1 1 d . . .
B10 B 0.4194(9) 0.9295(4) 0.6534(12) 0.086(5) Uani 1 1 d . . .
H10 H 0.4558 0.9480 0.6729 0.103 Uiso 1 1 calc R . .
O11 O -0.5079(4) 0.65371(14) 0.8446(5) 0.0583(18) Uani 1 1 d . . .
C11 C 0.3602(5) 0.6991(2) 0.5959(6) 0.053(2) Uani 1 1 d . B .
B11 B 0.4467(7) 0.8911(3) 0.6491(10) 0.072(4) Uani 1 1 d . . .
H11 H 0.5005 0.8843 0.6668 0.087 Uiso 1 1 calc R . .
O12 O -0.4572(4) 0.70414(15) 0.7961(4) 0.0560(17) Uani 1 1 d . . .
C12 C 0.3040(5) 0.7093(2) 0.5509(7) 0.053(2) Uani 1 1 d . . .
H12 H 0.2802 0.7272 0.5677 0.063 Uiso 1 1 calc R B .
B12 B 0.4266(9) 0.9121(3) 0.5599(10) 0.077(4) Uani 1 1 d . . .
H13H H 0.4675 0.9192 0.5166 0.093 Uiso 1 1 calc R . .
O13 O -0.4509(10) 0.5318(4) 0.7522(11) 0.167(6) Uiso 1 1 d . . .
C13 C 0.2815(5) 0.6941(2) 0.4812(6) 0.051(2) Uani 1 1 d . B .
B13 B 0.3864(7) 0.9022(3) 0.7219(10) 0.066(3) Uani 1 1 d . . .
H13 H 0.3998 0.9024 0.7875 0.080 Uiso 1 1 calc R . .
O14 O -0.4193(10) 0.5618(4) 0.8497(12) 0.176(6) Uiso 1 1 d . . .
C14 C 0.2176(6) 0.7061(2) 0.4375(7) 0.057(3) Uani 1 1 d . . .
H14A H 0.2207 0.7011 0.3796 0.069 Uiso 1 1 calc R B .
H14B H 0.2155 0.7285 0.4431 0.069 Uiso 1 1 calc R . .
B14 B 0.3321(8) 0.9305(3) 0.6786(9) 0.069(4) Uani 1 1 d . . .
H14 H 0.3092 0.9493 0.7152 0.083 Uiso 1 1 calc R . .
C15 C 0.1522(6) 0.6920(2) 0.4716(6) 0.056(3) Uani 1 1 d . B .
B15 B 0.3564(9) 0.9357(3) 0.5790(10) 0.078(4) Uani 1 1 d . . .
H15 H 0.3491 0.9585 0.5494 0.094 Uiso 1 1 calc R . .
O16 O -0.2537(14) 0.5172(6) 0.7037(17) 0.129(5) Uiso 0.50 1 d PD A 1
C122 C -0.239(2) 0.5307(9) 0.561(2) 0.129(5) Uiso 0.50 1 d P A 1
H12G H -0.2545 0.5500 0.5372 0.193 Uiso 0.50 1 calc PR A 1
H12H H -0.2601 0.5136 0.5316 0.193 Uiso 0.50 1 calc PR A 1
H12I H -0.1882 0.5293 0.5560 0.193 Uiso 0.50 1 calc PR A 1
O17 O -0.3089(14) 0.5488(6) 0.6570(17) 0.129(5) Uiso 0.50 1 d PD A 1
C16 C 0.1260(5) 0.7050(2) 0.5406(6) 0.048(2) Uani 1 1 d . . .
H16 H 0.1457 0.7235 0.5597 0.058 Uiso 1 1 calc R B .
B16 B 0.2905(7) 0.9111(2) 0.5991(7) 0.051(3) Uani 1 1 d . . .
H16A H 0.2367 0.9184 0.5827 0.061 Uiso 1 1 calc R . .
C17 C 0.0727(6) 0.6922(2) 0.5827(6) 0.056(3) Uani 1 1 d . B .
B17 B 0.3071(6) 0.8923(2) 0.6829(7) 0.047(3) Uani 1 1 d . . .
H17 H 0.2657 0.8868 0.7273 0.056 Uiso 1 1 calc R . .
C18 C 0.0424(5) 0.6650(2) 0.5520(7) 0.056(3) Uani 1 1 d . . .
B18 B 0.3716(7) 0.8667(3) 0.6677(8) 0.059(3) Uani 1 1 d . . .
H18 H 0.3759 0.8441 0.6987 0.071 Uiso 1 1 calc R . .
C19 C 0.0653(5) 0.6528(2) 0.4846(7) 0.057(3) Uani 1 1 d . B .
H19 H 0.0433 0.6349 0.4644 0.068 Uiso 1 1 calc R . .
B19 B -0.3383(8) 0.8000(3) 0.9282(11) 0.083(5) Uani 1 1 d . . .
H19A H -0.3726 0.7809 0.9478 0.099 Uiso 1 1 calc R . .
C20 C 0.1220(5) 0.6653(2) 0.4407(6) 0.053(2) Uani 1 1 d . . .
B20 B -0.2753(7) 0.7951(3) 0.8558(9) 0.065(3) Uani 1 1 d . . .
H20 H -0.2689 0.7723 0.8267 0.078 Uiso 1 1 calc R . .
C21 C 0.1443(6) 0.6495(2) 0.3632(7) 0.059(3) Uani 1 1 d . B .
H21A H 0.1028 0.6433 0.3321 0.071 Uiso 1 1 calc R . .
H21B H 0.1710 0.6640 0.3300 0.071 Uiso 1 1 calc R . .
B21 B -0.2487(8) 0.8009(3) 0.9562(9) 0.069(4) Uani 1 1 d . . .
H21 H -0.2245 0.7828 0.9946 0.083 Uiso 1 1 calc R . .
C22 C 0.3637(6) 0.5420(3) 0.4594(10) 0.079(4) Uani 1 1 d . . .
H22A H 0.3740 0.5578 0.5003 0.094 Uiso 1 1 calc R B .
H22B H 0.3879 0.5475 0.4093 0.094 Uiso 1 1 calc R . .
B22 B -0.3068(12) 0.8289(3) 0.9961(12) 0.104(6) Uani 1 1 d . . .
H22 H -0.3209 0.8295 1.0612 0.124 Uiso 1 1 calc R . .
C23 C 0.3875(8) 0.5125(3) 0.4878(8) 0.081(3) Uiso 1 1 d . B .
B23 B -0.3683(11) 0.8393(4) 0.9192(15) 0.119(8) Uani 1 1 d . . .
H23 H -0.4223 0.8466 0.9327 0.142 Uiso 1 1 calc R . .
C24 C 0.4238(9) 0.4944(4) 0.4356(12) 0.107(5) Uiso 1 1 d . . .
H24 H 0.4314 0.5018 0.3827 0.129 Uiso 1 1 calc R B .
B24 B -0.3480(9) 0.8181(3) 0.8340(13) 0.084(5) Uani 1 1 d . . .
H24A H -0.3899 0.8111 0.7910 0.101 Uiso 1 1 calc R . .
C25 C 0.4498(9) 0.4661(4) 0.4559(10) 0.097(4) Uiso 1 1 d . B .
H25 H 0.4734 0.4536 0.4184 0.117 Uiso 1 1 calc R . .
B25 B -0.2630(6) 0.8288(3) 0.7993(9) 0.059(3) Uani 1 1 d . . .
H25A H -0.2498 0.8280 0.7339 0.071 Uiso 1 1 calc R . .
C26 C 0.4399(9) 0.4576(4) 0.5311(11) 0.100(4) Uiso 1 1 d . . .
B26 B -0.2027(7) 0.8190(3) 0.8758(9) 0.062(3) Uani 1 1 d . . .
H26 H -0.1488 0.8116 0.8613 0.074 Uiso 1 1 calc R . .
C27 C 0.4013(8) 0.4772(3) 0.5853(10) 0.093(4) Uiso 1 1 d . B .
B27 B -0.2255(10) 0.8393(3) 0.9608(9) 0.078(4) Uani 1 1 d . . .
H27 H -0.1850 0.8461 1.0058 0.094 Uiso 1 1 calc R . .
B28 B -0.0935(12) 0.9314(4) 0.7982(11) 0.101(6) Uani 1 1 d . . .
H28A H -0.0566 0.9498 0.7798 0.121 Uiso 1 1 calc R . .
B29 B -0.0637(10) 0.8935(4) 0.8097(12) 0.099(6) Uani 1 1 d . . .
H29A H -0.0085 0.8872 0.7989 0.118 Uiso 1 1 calc R . .
B30 B -0.0904(15) 0.9145(4) 0.8954(13) 0.131(9) Uani 1 1 d . . .
H30A H -0.0528 0.9228 0.9420 0.157 Uiso 1 1 calc R . .
B31 B -0.1617(16) 0.9377(4) 0.8681(12) 0.127(9) Uani 1 1 d . . .
H31A H -0.1736 0.9605 0.8956 0.153 Uiso 1 1 calc R . .
B32 B -0.1798(9) 0.9319(3) 0.7669(11) 0.084(5) Uani 1 1 d . . .
H32 H -0.2023 0.9505 0.7284 0.101 Uiso 1 1 calc R . .
B33 B -0.1225(9) 0.9045(3) 0.7297(10) 0.079(4) Uani 1 1 d . . .
H33 H -0.1075 0.9051 0.6649 0.094 Uiso 1 1 calc R . .
B34 B -0.1332(8) 0.8682(3) 0.7821(8) 0.068(4) Uani 1 1 d . . .
H34 H -0.1232 0.8461 0.7506 0.082 Uiso 1 1 calc R . .
C35 C 0.3494(5) 0.74052(19) 0.6903(7) 0.055(3) Uani 1 1 d . . .
H35A H 0.3007 0.7353 0.7017 0.066 Uiso 1 1 calc R . .
H35B H 0.3501 0.7567 0.6488 0.066 Uiso 1 1 calc R . .
B35 B -0.2014(7) 0.8926(2) 0.7630(7) 0.055(3) Uani 1 1 d . . .
H35 H -0.2409 0.8858 0.7168 0.066 Uiso 1 1 calc R . .
C36 C 0.3850(5) 0.7515(2) 0.7656(6) 0.051(2) Uani 1 1 d . . .
B36 B -0.2222(9) 0.9118(3) 0.8431(8) 0.067(4) Uani 1 1 d . . .
H36 H -0.2770 0.9184 0.8551 0.081 Uiso 1 1 calc R . .
C37 C 0.4054(6) 0.7823(2) 0.7712(7) 0.057(3) Uani 1 1 d . . .
H37 H 0.3963 0.7959 0.7280 0.069 Uiso 1 1 calc R . .
C38 C 0.4382(6) 0.7922(2) 0.8386(7) 0.061(3) Uani 1 1 d . . .
H38 H 0.4524 0.8130 0.8425 0.074 Uiso 1 1 calc R . .
C39 C 0.4513(5) 0.7720(2) 0.9032(6) 0.050(2) Uani 1 1 d . . .
C40 C 0.4284(5) 0.7412(2) 0.8934(6) 0.046(2) Uani 1 1 d . . .
C41 C 0.4399(6) 0.7204(3) 0.9578(7) 0.063(3) Uani 1 1 d . . .
H41 H 0.4244 0.6999 0.9538 0.076 Uiso 1 1 calc R . .
C42 C 0.4734(6) 0.7302(3) 1.0255(7) 0.064(3) Uani 1 1 d . . .
H42 H 0.4805 0.7163 1.0684 0.077 Uiso 1 1 calc R . .
C43 C 0.4972(6) 0.7595(3) 1.0336(8) 0.070(3) Uani 1 1 d . . .
H43 H 0.5216 0.7654 1.0809 0.083 Uiso 1 1 calc R . .
C44 C 0.4860(6) 0.7801(3) 0.9747(7) 0.063(3) Uani 1 1 d . . .
H44 H 0.5019 0.8004 0.9816 0.076 Uiso 1 1 calc R . .
C45 C 0.4903(5) 0.6391(2) 0.5990(7) 0.055(3) Uani 1 1 d . . .
H45A H 0.5040 0.6400 0.5418 0.066 Uiso 1 1 calc R B .
H45B H 0.4622 0.6205 0.6072 0.066 Uiso 1 1 calc R . .
C46 C 0.5533(5) 0.6385(2) 0.6525(8) 0.062(3) Uani 1 1 d . B .
H46A H 0.5392 0.6398 0.7094 0.074 Uiso 1 1 calc R . .
H46B H 0.5829 0.6564 0.6407 0.074 Uiso 1 1 calc R . .
C47 C 0.5951(6) 0.6087(2) 0.6391(9) 0.074(3) Uani 1 1 d . . .
H47A H 0.5679 0.5911 0.6572 0.111 Uiso 1 1 calc R B .
H47B H 0.6384 0.6096 0.6697 0.111 Uiso 1 1 calc R . .
H47C H 0.6051 0.6064 0.5818 0.111 Uiso 1 1 calc R . .
C48 C -0.0281(6) 0.6221(2) 0.5888(7) 0.058(3) Uani 1 1 d . . .
H48A H 0.0136 0.6096 0.5992 0.070 Uiso 1 1 calc R B .
H48B H -0.0449 0.6177 0.5337 0.070 Uiso 1 1 calc R . .
C49 C -0.0827(5) 0.6144(2) 0.6483(6) 0.052(2) Uani 1 1 d . B .
C50 C -0.0845(6) 0.5840(3) 0.6751(8) 0.072(3) Uani 1 1 d . . .
H50 H -0.0524 0.5695 0.6553 0.086 Uiso 1 1 calc R B .
C51 C -0.1329(7) 0.5755(3) 0.7298(8) 0.076(4) Uani 1 1 d . B .
H51 H -0.1323 0.5555 0.7519 0.091 Uiso 1 1 calc R . .
C52 C -0.1844(6) 0.5970(2) 0.7537(8) 0.066(3) Uani 1 1 d . . .
C53 C -0.1812(6) 0.6260(2) 0.7234(6) 0.055(3) Uani 1 1 d . B .
C54 C -0.2296(6) 0.6484(2) 0.7467(8) 0.065(3) Uani 1 1 d . . .
H54 H -0.2271 0.6685 0.7252 0.078 Uiso 1 1 calc R B .
C55 C -0.2796(6) 0.6411(3) 0.7998(8) 0.067(3) Uani 1 1 d . B .
H55 H -0.3131 0.6559 0.8146 0.081 Uiso 1 1 calc R . .
C56 C -0.2816(6) 0.6113(2) 0.8331(8) 0.069(3) Uani 1 1 d . . .
H56 H -0.3164 0.6062 0.8706 0.083 Uiso 1 1 calc R B .
C57 C -0.2340(7) 0.5903(3) 0.8115(9) 0.080(4) Uani 1 1 d . B .
H57 H -0.2344 0.5707 0.8360 0.095 Uiso 1 1 calc R . .
C58 C 0.0723(6) 0.7295(2) 0.6876(7) 0.059(3) Uani 1 1 d . . .
H58A H 0.0383 0.7393 0.7232 0.071 Uiso 1 1 calc R . .
H58B H 0.0856 0.7445 0.6461 0.071 Uiso 1 1 calc R . .
C59 C 0.1349(6) 0.7210(2) 0.7361(7) 0.063(3) Uani 1 1 d . . .
H59A H 0.1713 0.7136 0.6994 0.075 Uiso 1 1 calc R . .
H59B H 0.1230 0.7040 0.7727 0.075 Uiso 1 1 calc R . .
C60 C 0.1640(6) 0.7478(3) 0.7863(7) 0.070(3) Uani 1 1 d . . .
H60A H 0.1673 0.7661 0.7524 0.105 Uiso 1 1 calc R . .
H60B H 0.2100 0.7425 0.8070 0.105 Uiso 1 1 calc R . .
H60C H 0.1332 0.7520 0.8314 0.105 Uiso 1 1 calc R . .
C61 C -0.2134(5) 0.6921(2) 0.9640(6) 0.053(2) Uani 1 1 d . . .
C62 C -0.1933(5) 0.7087(2) 0.8978(7) 0.056(3) Uani 1 1 d . . .
H62 H -0.2172 0.7268 0.8832 0.067 Uiso 1 1 calc R . .
C63 C -0.1386(5) 0.6987(2) 0.8535(7) 0.052(2) Uani 1 1 d . . .
C64 C -0.1050(6) 0.6721(2) 0.8721(7) 0.061(3) Uani 1 1 d . . .
C65 C -0.1246(5) 0.6550(2) 0.9379(6) 0.052(2) Uani 1 1 d . . .
H65 H -0.1015 0.6365 0.9508 0.062 Uiso 1 1 calc R . .
C66 C -0.1804(5) 0.6656(2) 0.9864(7) 0.057(3) Uani 1 1 d . . .
C67 C -0.1942(6) 0.6469(2) 1.0623(7) 0.060(3) Uani 1 1 d . . .
H67A H -0.2156 0.6605 1.1026 0.072 Uiso 1 1 calc R . .
H67B H -0.1493 0.6400 1.0846 0.072 Uiso 1 1 calc R . .
C68 C -0.2410(6) 0.6188(2) 1.0511(6) 0.059(3) Uani 1 1 d . . .
C69 C -0.2096(6) 0.5915(2) 1.0284(8) 0.071(3) Uani 1 1 d . . .
H69 H -0.1613 0.5916 1.0191 0.085 Uiso 1 1 calc R . .
C70 C -0.2452(7) 0.5645(2) 1.0186(9) 0.077(4) Uani 1 1 d . . .
C71 C -0.3162(7) 0.5646(2) 1.0370(8) 0.071(3) Uani 1 1 d . . .
C72 C -0.3477(6) 0.5909(2) 1.0578(7) 0.060(3) Uani 1 1 d . . .
H72 H -0.3958 0.5907 1.0689 0.072 Uiso 1 1 calc R . .
C73 C -0.3114(6) 0.6183(2) 1.0634(6) 0.057(3) Uani 1 1 d . . .
C74 C -0.3523(5) 0.6480(2) 1.0811(7) 0.058(3) Uani 1 1 d . . .
H74A H -0.3938 0.6429 1.1127 0.069 Uiso 1 1 calc R . .
H74B H -0.3231 0.6618 1.1139 0.069 Uiso 1 1 calc R . .
C75 C -0.3740(5) 0.6640(2) 1.0057(6) 0.053(2) Uani 1 1 d . . .
C76 C -0.4298(5) 0.6516(2) 0.9609(7) 0.055(3) Uani 1 1 d . . .
H76 H -0.4517 0.6336 0.9800 0.066 Uiso 1 1 calc R . .
C77 C -0.4539(5) 0.6648(2) 0.8903(6) 0.048(2) Uani 1 1 d . . .
C78 C -0.4250(5) 0.6917(2) 0.8638(6) 0.049(2) Uani 1 1 d . . .
C79 C -0.3712(5) 0.7048(2) 0.9064(7) 0.054(2) Uani 1 1 d . . .
H79 H -0.3528 0.7238 0.8890 0.065 Uiso 1 1 calc R . .
C80 C -0.3429(5) 0.6905(2) 0.9756(7) 0.052(2) Uani 1 1 d . . .
C81 C -0.2778(5) 0.7042(2) 1.0110(7) 0.054(2) Uani 1 1 d . . .
H81A H -0.2736 0.6986 1.0685 0.065 Uiso 1 1 calc R . .
H81B H -0.2799 0.7268 1.0072 0.065 Uiso 1 1 calc R . .
C82 C -0.1507(5) 0.7401(2) 0.7596(7) 0.057(3) Uani 1 1 d . . .
H82A H -0.1509 0.7558 0.8023 0.068 Uiso 1 1 calc R . .
H82B H -0.1991 0.7344 0.7471 0.068 Uiso 1 1 calc R . .
C83 C -0.1162(5) 0.7525(2) 0.6850(7) 0.056(2) Uani 1 1 d . . .
C84 C -0.0974(6) 0.7836(2) 0.6821(7) 0.056(3) Uani 1 1 d . . .
H84 H -0.1075 0.7972 0.7249 0.068 Uiso 1 1 calc R . .
C85 C -0.0639(6) 0.7931(3) 0.6149(7) 0.065(3) Uani 1 1 d . . .
H85 H -0.0491 0.8137 0.6118 0.077 Uiso 1 1 calc R . .
C86 C -0.0509(6) 0.7741(2) 0.5519(7) 0.059(3) Uani 1 1 d . . .
C87 C -0.0748(5) 0.7430(2) 0.5573(6) 0.051(2) Uani 1 1 d . . .
C88 C -0.0643(6) 0.7227(2) 0.4935(7) 0.060(3) Uani 1 1 d . . .
H88 H -0.0812 0.7023 0.4966 0.072 Uiso 1 1 calc R . .
C89 C -0.0291(6) 0.7323(3) 0.4258(8) 0.070(3) Uani 1 1 d . . .
H89 H -0.0222 0.7186 0.3823 0.084 Uiso 1 1 calc R . .
C90 C -0.0039(6) 0.7621(3) 0.4212(7) 0.064(3) Uani 1 1 d . . .
H90 H 0.0218 0.7681 0.3756 0.077 Uiso 1 1 calc R . .
C91 C -0.0154(6) 0.7826(3) 0.4807(7) 0.064(3) Uani 1 1 d . . .
H91 H 0.0004 0.8030 0.4747 0.076 Uiso 1 1 calc R . .
C92 C -0.0124(6) 0.6371(2) 0.8432(7) 0.059(3) Uani 1 1 d . . .
H92A H -0.0412 0.6190 0.8303 0.071 Uiso 1 1 calc R . .
H92B H -0.0007 0.6366 0.9013 0.071 Uiso 1 1 calc R . .
C93 C 0.0531(6) 0.6369(2) 0.7933(8) 0.064(3) Uani 1 1 d . . .
H93A H 0.0406 0.6400 0.7360 0.077 Uiso 1 1 calc R . .
H93B H 0.0829 0.6542 0.8102 0.077 Uiso 1 1 calc R . .
C94 C 0.0925(7) 0.6079(3) 0.8019(9) 0.083(4) Uani 1 1 d . . .
H94A H 0.1040 0.6045 0.8587 0.125 Uiso 1 1 calc R . .
H94B H 0.1352 0.6091 0.7708 0.125 Uiso 1 1 calc R . .
H94C H 0.0643 0.5908 0.7818 0.125 Uiso 1 1 calc R . .
C95 C -0.1477(11) 0.5365(4) 0.9815(16) 0.142(8) Uani 1 1 d . . .
H95A H -0.1224 0.5386 1.0332 0.170 Uiso 1 1 calc R . .
H95B H -0.1331 0.5530 0.9449 0.170 Uiso 1 1 calc R . .
C96 C -0.1324(11) 0.5007(4) 0.9386(16) 0.133(7) Uani 1 1 d . . .
C97 C -0.0946(9) 0.4846(4) 0.9785(12) 0.116(6) Uani 1 1 d . . .
H97 H -0.0761 0.4901 1.0296 0.139 Uiso 1 1 calc R . .
C98 C -0.0823(9) 0.4583(3) 0.9411(15) 0.120(7) Uani 1 1 d . . .
C99 C -0.1078(8) 0.4491(3) 0.8643(10) 0.091(4) Uani 1 1 d . . .
C100 C -0.1507(9) 0.4687(3) 0.8300(13) 0.104(5) Uani 1 1 d . . .
H100 H -0.1663 0.4643 0.7769 0.125 Uiso 1 1 calc R . .
C101 C -0.0866(9) 0.4220(3) 0.8358(14) 0.119(6) Uani 1 1 d . . .
H101 H -0.1030 0.4152 0.7848 0.143 Uiso 1 1 calc R . .
C102 C -0.0417(10) 0.4039(4) 0.8791(15) 0.130(7) Uani 1 1 d . . .
H102 H -0.0290 0.3849 0.8560 0.156 Uiso 1 1 calc R . .
C103 C -0.0152(11) 0.4107(4) 0.9491(15) 0.132(7) Uani 1 1 d . . .
H103 H 0.0187 0.3982 0.9744 0.158 Uiso 1 1 calc R . .
C104 C -0.0390(11) 0.4368(5) 0.9838(18) 0.153(8) Uani 1 1 d . . .
H104 H -0.0267 0.4409 1.0381 0.184 Uiso 1 1 calc R . .
C105 C -0.4115(12) 0.5346(5) 1.0677(15) 0.145(7) Uiso 1 1 d . . .
H10A H -0.4440 0.5486 1.0400 0.174 Uiso 1 1 calc R . .
H10B H -0.4089 0.5403 1.1252 0.174 Uiso 1 1 calc R . .
C106 C -0.436(2) 0.5006(8) 1.058(2) 0.226(14) Uiso 1 1 d . . .
H10C H -0.4852 0.4983 1.0718 0.271 Uiso 1 1 calc R . .
H10D H -0.4284 0.4931 1.0027 0.271 Uiso 1 1 calc R . .
C107 C -0.3937(19) 0.4857(7) 1.113(2) 0.224(13) Uiso 1 1 d . . .
H10E H -0.3478 0.4828 1.0897 0.336 Uiso 1 1 calc R . .
H10F H -0.4137 0.4657 1.1258 0.336 Uiso 1 1 calc R . .
H10G H -0.3897 0.4979 1.1620 0.336 Uiso 1 1 calc R . .
C108 C -0.5277(6) 0.6219(2) 0.8560(7) 0.055(3) Uani 1 1 d . . .
H10H H -0.5471 0.6191 0.9104 0.066 Uiso 1 1 calc R . .
H10I H -0.4867 0.6086 0.8511 0.066 Uiso 1 1 calc R . .
C109 C -0.5812(5) 0.6133(2) 0.7931(6) 0.052(2) Uani 1 1 d . . .
C110 C -0.5793(6) 0.5842(2) 0.7621(8) 0.064(3) Uani 1 1 d . . .
H110 H -0.5439 0.5704 0.7782 0.076 Uiso 1 1 calc R . .
C111 C -0.6285(6) 0.5753(2) 0.7082(8) 0.069(3) Uani 1 1 d . . .
H111 H -0.6280 0.5552 0.6870 0.083 Uiso 1 1 calc R . .
C112 C -0.6815(6) 0.5965(2) 0.6831(7) 0.057(3) Uani 1 1 d . . .
C113 C -0.6797(5) 0.6257(2) 0.7163(7) 0.058(3) Uani 1 1 d . . .
C114 C -0.7314(6) 0.6471(2) 0.6944(7) 0.061(3) Uani 1 1 d . . .
H114 H -0.7313 0.6667 0.7190 0.074 Uiso 1 1 calc R . .
C115 C -0.7815(6) 0.6402(2) 0.6389(7) 0.063(3) Uani 1 1 d . . .
H115 H -0.8154 0.6549 0.6242 0.075 Uiso 1 1 calc R . .
C116 C -0.7823(6) 0.6112(2) 0.6040(8) 0.068(3) Uani 1 1 d . . .
H116 H -0.8161 0.6061 0.5645 0.082 Uiso 1 1 calc R . .
C117 C -0.7329(7) 0.5897(3) 0.6278(8) 0.075(3) Uani 1 1 d . . .
H117 H -0.7347 0.5698 0.6052 0.091 Uiso 1 1 calc R . .
C118 C -0.4258(6) 0.7305(2) 0.7589(7) 0.059(3) Uani 1 1 d . . .
H11A H -0.4113 0.7452 0.8011 0.070 Uiso 1 1 calc R . .
H11B H -0.4604 0.7408 0.7240 0.070 Uiso 1 1 calc R . .
C119 C -0.3637(6) 0.7219(3) 0.7091(8) 0.067(3) Uani 1 1 d . . .
H11C H -0.3770 0.7053 0.6715 0.080 Uiso 1 1 calc R . .
H11D H -0.3270 0.7139 0.7452 0.080 Uiso 1 1 calc R . .
C120 C -0.3349(6) 0.7485(3) 0.6612(8) 0.072(3) Uani 1 1 d . . .
H12A H -0.3700 0.7557 0.6228 0.108 Uiso 1 1 calc R . .
H12B H -0.2939 0.7418 0.6319 0.108 Uiso 1 1 calc R . .
H12C H -0.3223 0.7651 0.6979 0.108 Uiso 1 1 calc R . .
C121 C -0.3639(12) 0.5137(5) 0.8417(15) 0.147(7) Uiso 1 1 d . . .
H12D H -0.3266 0.5117 0.8027 0.220 Uiso 1 1 calc R . .
H12E H -0.3880 0.4942 0.8469 0.220 Uiso 1 1 calc R . .
H12F H -0.3445 0.5197 0.8940 0.220 Uiso 1 1 calc R . .
C123 C 0.3040(7) 0.8171(2) 0.5729(9) 0.069(3) Uani 1 1 d . . .
H123 H 0.3554 0.8081 0.5936 0.083 Uiso 1 1 calc R . .
C124 C 0.2923(7) 0.8381(3) 0.4803(8) 0.074(3) Uani 1 1 d . . .
H124 H 0.3363 0.8436 0.4396 0.089 Uiso 1 1 calc R . .
C125 C 0.3449(7) 0.9014(2) 0.5256(9) 0.079(4) Uani 1 1 d . . .
H125 H 0.3319 0.9022 0.4599 0.095 Uiso 1 1 calc R . .
C126 C 0.4025(7) 0.8723(3) 0.5672(9) 0.081(4) Uani 1 1 d . . .
H126 H 0.4291 0.8542 0.5316 0.098 Uiso 1 1 calc R . .
C127 C -0.1118(10) 0.8745(3) 0.8875(10) 0.104(5) Uani 1 1 d . . .
H127 H -0.0876 0.8565 0.9265 0.125 Uiso 1 1 calc R . .
C128 C -0.1677(12) 0.9020(3) 0.9227(10) 0.117(6) Uani 1 1 d . . .
H128 H -0.1806 0.9021 0.9882 0.140 Uiso 1 1 calc R . .
C129 C -0.2958(9) 0.8602(3) 0.9396(9) 0.093(5) Uani 1 1 d . . .
H129 H -0.3048 0.8825 0.9707 0.112 Uiso 1 1 calc R . .
C130 C -0.3201(8) 0.8548(3) 0.8437(12) 0.101(5) Uani 1 1 d . . .
H130 H -0.3454 0.8728 0.8056 0.122 Uiso 1 1 calc R . .
C32B C 0.0848(10) 0.5361(4) 0.4017(12) 0.117(5) Uiso 1 1 d . B 2
H32C H 0.0688 0.5507 0.3599 0.140 Uiso 1 1 calc R B 2
H32D H 0.0617 0.5413 0.4528 0.140 Uiso 1 1 calc R B 2
C33B C 0.0669(19) 0.5035(6) 0.377(2) 0.192(11) Uiso 1 1 d . B 2
H33C H 0.0184 0.5012 0.3588 0.231 Uiso 1 1 calc R B 2
H33D H 0.0988 0.4952 0.3364 0.231 Uiso 1 1 calc R B 2
C34B C 0.078(3) 0.4919(10) 0.451(3) 0.33(2) Uiso 1 1 d . B 2
H34D H 0.0738 0.4697 0.4496 0.498 Uiso 1 1 calc R B 2
H34E H 0.0445 0.5004 0.4887 0.498 Uiso 1 1 calc R B 2
H34F H 0.1250 0.4974 0.4695 0.498 Uiso 1 1 calc R B 2
C29 C 0.4124(12) 0.4376(5) 0.6966(15) 0.139(7) Uiso 1 1 d . B .
H29 H 0.4027 0.4308 0.7495 0.166 Uiso 1 1 calc R . .
C31 C 0.4651(10) 0.4264(4) 0.5652(12) 0.117(5) Uiso 1 1 d . B .
H31 H 0.4887 0.4122 0.5321 0.140 Uiso 1 1 calc R . .
C28 C 0.3862(12) 0.4680(5) 0.6651(13) 0.132(6) Uiso 1 1 d . . .
H28 H 0.3596 0.4809 0.6987 0.158 Uiso 1 1 calc R B .
C30 C 0.4526(11) 0.4200(5) 0.6422(13) 0.122(6) Uiso 1 1 d . . .
H30 H 0.4725 0.4017 0.6628 0.146 Uiso 1 1 calc R B .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 Ag1 N6 176.2(3) 1_455 .
N2 Ag1 O11 112.4(3) 1_455 .
N6 Ag1 O11 71.2(3) . .
C3 O1 C32B 117.4(11) . .
C23 N1 C27 118.9(13) . .
C6 C1 C2 118.4(10) . .
C6 C1 C21 125.2(9) . .
C2 C1 C21 116.4(10) . .
B6 B1 B2 60.2(8) . .
B6 B1 B3 107.9(10) . .
B2 B1 B3 59.9(8) . .
B6 B1 B5 58.5(8) . .
B2 B1 B5 106.6(10) . .
B3 B1 B5 107.4(10) . .
B6 B1 B4 107.3(9) . .
B2 B1 B4 108.3(9) . .
B3 B1 B4 60.7(8) . .
B5 B1 B4 59.7(8) . .
N4 Ag2 N3 174.3(3) . .
N4 Ag2 O6 115.1(3) . .
N3 Ag2 O6 69.6(3) . .
C4 O2 C22 115.9(9) . .
C36 N2 C40 120.3(8) . .
C36 N2 Ag1 120.3(7) . 1_655
C40 N2 Ag1 118.0(6) . 1_655
C3 C2 C1 121.3(11) . .
B1 B2 B6 59.9(8) . .
B1 B2 B3 60.6(8) . .
B6 B2 B3 108.2(10) . .
B1 B2 B7 111.2(9) . .
B6 B2 B7 62.6(7) . .
B3 B2 B7 108.9(9) . .
B1 B2 C123 111.1(10) . .
B6 B2 C123 110.6(8) . .
B3 B2 C123 61.1(8) . .
B7 B2 C123 59.9(7) . .
B16 Co3 B9 100.2(5) . .
B16 Co3 B8 99.6(5) . .
B9 Co3 B8 47.3(5) . .
B16 Co3 B18 84.3(5) . .
B9 Co3 B18 175.1(5) . .
B8 Co3 B18 134.0(5) . .
B16 Co3 B17 47.5(5) . .
B9 Co3 B17 135.8(5) . .
B8 Co3 B17 101.9(5) . .
B18 Co3 B17 48.8(4) . .
B16 Co3 C124 132.1(5) . .
B9 Co3 C124 49.2(5) . .
B8 Co3 C124 84.3(5) . .
B18 Co3 C124 126.3(5) . .
B17 Co3 C124 173.8(5) . .
B16 Co3 B7 130.6(5) . .
B9 Co3 B7 83.7(5) . .
B8 Co3 B7 48.6(5) . .
B18 Co3 B7 94.6(5) . .
B17 Co3 B7 96.7(5) . .
C124 Co3 B7 87.2(5) . .
B16 Co3 C125 47.7(5) . .
B9 Co3 C125 95.1(5) . .
B8 Co3 C125 129.3(5) . .
B18 Co3 C125 86.7(6) . .
B17 Co3 C125 82.8(5) . .
C124 Co3 C125 93.5(5) . .
B7 Co3 C125 177.7(5) . .
B16 Co3 C123 175.6(6) . .
B9 Co3 C123 84.1(5) . .
B8 Co3 C123 83.4(5) . .
B18 Co3 C123 91.3(5) . .
B17 Co3 C123 129.0(5) . .
C124 Co3 C123 51.0(5) . .
B7 Co3 C123 49.7(5) . .
C125 Co3 C123 132.2(5) . .
B16 Co3 C126 84.5(5) . .
B9 Co3 C126 127.6(5) . .
B8 Co3 C126 173.8(5) . .
B18 Co3 C126 50.7(5) . .
B17 Co3 C126 84.3(5) . .
C124 Co3 C126 89.6(5) . .
B7 Co3 C126 131.3(5) . .
C125 Co3 C126 50.9(5) . .
C123 Co3 C126 92.8(5) . .
C10 O3 C45 117.9(8) . .
C49 N3 C53 118.2(8) . .
C49 N3 Ag2 121.8(7) . .
C53 N3 Ag2 117.6(6) . .
O1 C3 C2 125.3(11) . .
O1 C3 C4 116.2(10) . .
C2 C3 C4 118.3(10) . .
B2 B3 B1 59.5(9) . .
B2 B3 C123 60.5(7) . .
B1 B3 C123 109.8(10) . .
B2 B3 B4 108.5(10) . .
B1 B3 B4 61.3(8) . .
C123 B3 B4 110.3(9) . .
B2 B3 C124 108.1(9) . .
B1 B3 C124 110.1(9) . .
C123 B3 C124 60.3(7) . .
B4 B3 C124 61.1(7) . .
B35 Co4 B27 177.3(7) . .
B35 Co4 B36 47.1(5) . .
B27 Co4 B36 132.3(5) . .
B35 Co4 C129 133.4(6) . .
B27 Co4 C129 48.4(7) . .
B36 Co4 C129 99.2(6) . .
B35 Co4 B26 130.6(5) . .
B27 Co4 B26 49.8(5) . .
B36 Co4 B26 176.4(6) . .
C129 Co4 B26 84.3(5) . .
B35 Co4 B34 49.6(5) . .
B27 Co4 B34 128.6(6) . .
B36 Co4 B34 84.4(6) . .
C129 Co4 B34 176.3(5) . .
B26 Co4 B34 92.1(5) . .
B35 Co4 C127 85.7(6) . .
B27 Co4 C127 91.7(7) . .
B36 Co4 C127 84.6(6) . .
C129 Co4 C127 128.2(7) . .
B26 Co4 C127 92.4(6) . .
B34 Co4 C127 51.8(6) . .
B35 Co4 C130 99.2(6) . .
B27 Co4 C130 83.4(7) . .
B36 Co4 C130 98.3(6) . .
C129 Co4 C130 47.6(7) . .
B26 Co4 C130 84.7(5) . .
B34 Co4 C130 132.2(7) . .
C127 Co4 C130 175.1(7) . .
B35 Co4 C128 83.7(6) . .
B27 Co4 C128 94.2(6) . .
B36 Co4 C128 49.6(6) . .
C129 Co4 C128 96.3(7) . .
B26 Co4 C128 129.3(6) . .
B34 Co4 C128 86.0(7) . .
C127 Co4 C128 48.5(8) . .
C130 Co4 C128 131.2(7) . .
B35 Co4 B25 96.7(5) . .
B27 Co4 B25 85.3(6) . .
B36 Co4 B25 131.1(6) . .
C129 Co4 B25 83.9(5) . .
B26 Co4 B25 50.0(5) . .
B34 Co4 B25 93.9(5) . .
C127 Co4 B25 130.9(6) . .
C130 Co4 B25 49.3(5) . .
C128 Co4 B25 179.3(7) . .
C11 O4 C35 117.7(8) . .
C83 N4 C87 119.4(8) . .
C83 N4 Ag2 120.0(7) . .
C87 N4 Ag2 118.2(6) . .
O2 C4 C5 126.0(10) . .
O2 C4 C3 116.0(10) . .
C5 C4 C3 118.0(10) . .
B9 B4 B5 58.8(8) . .
B9 B4 B3 102.0(10) . .
B5 B4 B3 104.7(11) . .
B9 B4 B1 103.1(11) . .
B5 B4 B1 58.9(8) . .
B3 B4 B1 58.0(8) . .
B9 B4 C124 57.6(7) . .
B5 B4 C124 106.7(10) . .
B3 B4 C124 59.4(7) . .
B1 B4 C124 106.1(11) . .
C17 O5 C58 117.6(8) . .
C100 N5 C96 109(2) . .
C6 C5 C4 123.1(10) . .
B8 B5 B6 58.9(8) . .
B8 B5 B9 57.1(8) . .
B6 B5 B9 105.0(10) . .
B8 B5 B1 104.5(10) . .
B6 B5 B1 59.8(8) . .
B9 B5 B1 104.8(10) . .
B8 B5 B4 105.4(10) . .
B6 B5 B4 109.7(10) . .
B9 B5 B4 58.5(8) . .
B1 B5 B4 61.4(8) . .
C18 O6 C48 118.9(7) . .
C18 O6 Ag2 125.7(5) . .
C48 O6 Ag2 111.5(5) . .
C109 N6 C113 117.4(8) . .
C109 N6 Ag1 121.2(7) . .
C113 N6 Ag1 119.7(6) . .
C1 C6 C5 120.8(10) . .
C1 C6 C7 122.0(10) . .
C5 C6 C7 117.2(10) . .
B8 B6 B5 60.3(8) . .
B8 B6 B1 107.1(11) . .
B5 B6 B1 61.7(9) . .
B8 B6 B2 103.8(9) . .
B5 B6 B2 108.9(10) . .
B1 B6 B2 59.9(8) . .
B8 B6 B7 58.0(7) . .
B5 B6 B7 109.0(10) . .
B1 B6 B7 108.3(9) . .
B2 B6 B7 59.1(7) . .
C63 O7 C82 117.1(7) . .
O14 N7 O13 115(2) . .
O14 N7 C121 124(2) . .
O13 N7 C121 121(2) . .
C8 C7 C6 114.5(8) . .
B8 B7 B2 102.5(10) . .
B8 B7 C123 106.0(9) . .
B2 B7 C123 60.8(7) . .
B8 B7 B6 57.0(7) . .
B2 B7 B6 58.3(7) . .
C123 B7 B6 107.8(10) . .
B8 B7 Co3 64.4(6) . .
B2 B7 Co3 118.2(8) . .
C123 B7 Co3 66.0(5) . .
B6 B7 Co3 116.3(8) . .
C64 O8 C92 116.3(8) . .
O16 N8 O17 97(3) . .
O16 N8 C122 150(4) . .
O17 N8 C122 112(3) . .
C9 C8 C13 119.1(10) . .
C9 C8 C7 117.7(9) . .
C13 C8 C7 122.9(10) . .
B9 B8 B6 110.3(10) . .
B9 B8 B7 111.2(9) . .
B6 B8 B7 65.0(8) . .
B9 B8 B5 61.8(8) . .
B6 B8 B5 60.8(9) . .
B7 B8 B5 115.2(9) . .
B9 B8 Co3 66.2(6) . .
B6 B8 Co3 125.7(8) . .
B7 B8 Co3 67.0(6) . .
B5 B8 Co3 124.2(9) . .
C70 O9 C95 116.9(12) . .
C10 C9 C8 122.2(10) . .
B8 B9 B4 112.0(10) . .
B8 B9 C124 111.2(9) . .
B4 B9 C124 64.8(8) . .
B8 B9 B5 61.1(8) . .
B4 B9 B5 62.7(8) . .
C124 B9 B5 115.7(9) . .
B8 B9 Co3 66.5(6) . .
B4 B9 Co3 126.1(8) . .
C124 B9 Co3 66.6(6) . .
B5 B9 Co3 123.9(9) . .
C105 O10 C71 114.9(13) . .
O3 C10 C9 126.1(9) . .
O3 C10 C11 114.6(9) . .
C9 C10 C11 118.9(10) . .
B12 B10 B14 108.1(13) . .
B12 B10 B15 59.8(10) . .
B14 B10 B15 59.8(10) . .
B12 B10 B11 61.2(9) . .
B14 B10 B11 108.9(10) . .
B15 B10 B11 109.0(12) . .
B12 B10 B13 108.0(10) . .
B14 B10 B13 60.4(8) . .
B15 B10 B13 107.8(11) . .
B11 B10 B13 59.6(8) . .
C77 O11 C108 117.8(7) . .
C77 O11 Ag1 126.3(5) . .
C108 O11 Ag1 108.0(6) . .
O4 C11 C12 124.0(9) . .
O4 C11 C10 116.3(9) . .
C12 C11 C10 119.7(10) . .
B13 B11 B10 60.5(8) . .
B13 B11 B12 106.8(10) . .
B10 B11 B12 58.7(9) . .
B13 B11 C126 109.5(10) . .
B10 B11 C126 109.0(12) . .
B12 B11 C126 60.5(8) . .
B13 B11 B18 60.9(7) . .
B10 B11 B18 108.1(10) . .
B12 B11 B18 105.8(11) . .
C126 B11 B18 59.3(7) . .
C78 O12 C118 118.2(8) . .
C11 C12 C13 121.9(9) . .
B10 B12 B15 60.4(10) . .
B10 B12 C125 109.4(11) . .
B15 B12 C125 60.7(9) . .
B10 B12 B11 60.1(9) . .
B15 B12 B11 108.6(11) . .
C125 B12 B11 109.0(10) . .
B10 B12 C126 109.9(10) . .
B15 B12 C126 111.0(11) . .
C125 B12 C126 61.8(8) . .
B11 B12 C126 60.2(8) . .
C12 C13 C8 118.1(9) . .
C12 C13 C14 118.3(9) . .
C8 C13 C14 123.5(9) . .
B17 B13 B11 105.5(10) . .
B17 B13 B14 60.0(8) . .
B11 B13 B14 108.0(11) . .
B17 B13 B10 104.8(11) . .
B11 B13 B10 60.0(8) . .
B14 B13 B10 59.0(8) . .
B17 B13 B18 57.3(7) . .
B11 B13 B18 61.6(7) . .
B14 B13 B18 107.8(11) . .
B10 B13 B18 108.3(11) . .
C13 C14 C15 110.9(8) . .
B15 B14 B17 104.0(9) . .
B15 B14 B10 60.3(10) . .
B17 B14 B10 104.9(9) . .
B15 B14 B16 58.3(8) . .
B17 B14 B16 56.2(7) . .
B10 B14 B16 104.2(11) . .
B15 B14 B13 108.3(10) . .
B17 B14 B13 58.5(7) . .
B10 B14 B13 60.6(9) . .
B16 B14 B13 103.6(9) . .
C16 C15 C20 119.5(10) . .
C16 C15 C14 117.1(9) . .
C20 C15 C14 123.1(9) . .
B16 B15 B12 104.3(9) . .
B16 B15 B14 61.4(8) . .
B12 B15 B14 108.2(12) . .
B16 B15 B10 106.4(11) . .
B12 B15 B10 59.8(10) . .
B14 B15 B10 59.9(9) . .
B16 B15 C125 57.9(7) . .
B12 B15 C125 59.7(8) . .
B14 B15 C125 109.5(10) . .
B10 B15 C125 108.0(11) . .
C17 C16 C15 122.8(9) . .
B17 B16 C125 111.7(9) . .
B17 B16 B15 109.9(10) . .
C125 B16 B15 62.7(8) . .
B17 B16 B14 61.4(7) . .
C125 B16 B14 112.6(10) . .
B15 B16 B14 60.3(8) . .
B17 B16 Co3 66.9(5) . .
C125 B16 Co3 68.2(5) . .
B15 B16 Co3 124.9(8) . .
B14 B16 Co3 124.0(8) . .
C16 C17 O5 127.2(9) . .
C16 C17 C18 117.9(9) . .
O5 C17 C18 114.8(9) . .
B16 B17 B18 110.0(9) . .
B16 B17 B13 111.0(9) . .
B18 B17 B13 64.4(7) . .
B16 B17 B14 62.5(8) . .
B18 B17 B14 114.9(9) . .
B13 B17 B14 61.5(8) . .
B16 B17 Co3 65.6(5) . .
B18 B17 Co3 65.3(6) . .
B13 B17 Co3 123.6(7) . .
B14 B17 Co3 123.7(8) . .
C19 C18 O6 124.3(9) . .
C19 C18 C17 120.3(10) . .
O6 C18 C17 115.4(9) . .
B17 B18 C126 107.4(10) . .
B17 B18 B13 58.3(7) . .
C126 B18 B13 106.9(9) . .
B17 B18 B11 103.0(8) . .
C126 B18 B11 59.5(8) . .
B13 B18 B11 57.5(7) . .
B17 B18 Co3 65.8(6) . .
C126 B18 Co3 67.2(7) . .
B13 B18 Co3 118.8(8) . .
B11 B18 Co3 118.8(9) . .
C18 C19 C20 122.6(9) . .
B20 B19 B24 60.5(9) . .
B20 B19 B21 59.9(8) . .
B24 B19 B21 108.4(10) . .
B20 B19 B22 106.6(11) . .
B24 B19 B22 105.9(11) . .
B21 B19 B22 59.9(10) . .
B20 B19 B23 106.5(10) . .
B24 B19 B23 58.1(10) . .
B21 B19 B23 107.9(12) . .
B22 B19 B23 59.5(11) . .
C15 C20 C19 116.9(9) . .
C15 C20 C21 124.6(9) . .
C19 C20 C21 118.5(9) . .
B19 B20 B21 61.7(9) . .
B19 B20 B25 111.5(9) . .
B21 B20 B25 110.2(10) . .
B19 B20 B24 60.5(9) . .
B21 B20 B24 109.8(11) . .
B25 B20 B24 61.8(8) . .
B19 B20 B26 110.9(10) . .
B21 B20 B26 61.0(8) . .
B25 B20 B26 60.0(8) . .
B24 B20 B26 109.4(10) . .
C1 C21 C20 111.7(9) . .
B27 B21 B20 104.7(10) . .
B27 B21 B19 106.4(11) . .
B20 B21 B19 58.4(9) . .
B27 B21 B22 59.2(9) . .
B20 B21 B22 105.6(12) . .
B19 B21 B22 60.2(10) . .
B27 B21 B26 58.5(7) . .
B20 B21 B26 60.0(8) . .
B19 B21 B26 107.5(11) . .
B22 B21 B26 106.9(10) . .
O2 C22 C23 108.9(10) . .
C129 B22 B27 58.7(10) . .
C129 B22 B21 105.6(11) . .
B27 B22 B21 58.9(8) . .
C129 B22 B23 58.8(10) . .
B27 B22 B23 106.8(12) . .
B21 B22 B23 108.8(13) . .
C129 B22 B19 105.5(14) . .
B27 B22 B19 105.9(11) . .
B21 B22 B19 59.8(9) . .
B23 B22 B19 60.8(11) . .
N1 C23 C24 122.0(15) . .
N1 C23 C22 119.6(13) . .
C24 C23 C22 118.2(14) . .
C129 B23 C130 58.7(10) . .
C129 B23 B24 104.9(12) . .
C130 B23 B24 59.2(10) . .
C129 B23 B22 57.1(11) . .
C130 B23 B22 105.1(14) . .
B24 B23 B22 107.0(13) . .
C129 B23 B19 103.3(14) . .
C130 B23 B19 105.1(11) . .
B24 B23 B19 59.3(10) . .
B22 B23 B19 59.7(11) . .
C23 C24 C25 123.4(17) . .
C130 B24 B23 59.6(9) . .
C130 B24 B19 108.0(15) . .
B23 B24 B19 62.6(11) . .
C130 B24 B20 105.5(12) . .
B23 B24 B20 108.8(15) . .
B19 B24 B20 58.9(8) . .
C130 B24 B25 59.9(8) . .
B23 B24 B25 109.5(13) . .
B19 B24 B25 108.0(12) . .
B20 B24 B25 59.1(8) . .
C26 C25 C24 115.6(17) . .
C130 B25 B20 103.3(9) . .
C130 B25 B26 105.5(11) . .
B20 B25 B26 60.5(8) . .
C130 B25 B24 57.1(7) . .
B20 B25 B24 59.1(7) . .
B26 B25 B24 107.6(10) . .
C130 B25 Co4 64.7(7) . .
B20 B25 Co4 116.0(9) . .
B26 B25 Co4 63.7(6) . .
B24 B25 Co4 115.7(9) . .
C25 C26 C27 119.8(16) . .
C25 C26 C31 123.2(16) . .
C27 C26 C31 116.9(15) . .
B27 B26 B25 107.0(10) . .
B27 B26 B20 104.4(10) . .
B25 B26 B20 59.5(8) . .
B27 B26 B21 59.1(7) . .
B25 B26 B21 108.3(10) . .
B20 B26 B21 59.0(8) . .
B27 B26 Co4 63.9(6) . .
B25 B26 Co4 66.3(6) . .
B20 B26 Co4 117.5(9) . .
B21 B26 Co4 117.6(8) . .
N1 C27 C28 118.6(16) . .
N1 C27 C26 119.9(14) . .
C28 C27 C26 121.5(16) . .
C129 B27 B26 108.7(12) . .
C129 B27 B21 108.0(12) . .
B26 B27 B21 62.4(7) . .
C129 B27 B22 58.6(10) . .
B26 B27 B22 112.2(12) . .
B21 B27 B22 62.0(8) . .
C129 B27 Co4 66.4(7) . .
B26 B27 Co4 66.3(6) . .
B21 B27 Co4 122.6(9) . .
B22 B27 Co4 120.9(12) . .
B33 B28 B32 60.6(10) . .
B33 B28 B29 62.2(10) . .
B32 B28 B29 110.8(11) . .
B33 B28 B30 108.8(10) . .
B32 B28 B30 107.5(15) . .
B29 B28 B30 60.1(12) . .
B33 B28 B31 107.3(13) . .
B32 B28 B31 58.7(12) . .
B29 B28 B31 108.5(12) . .
B30 B28 B31 59.6(13) . .
B28 B29 B30 60.2(11) . .
B28 B29 B34 107.9(13) . .
B30 B29 B34 107.5(14) . .
B28 B29 C127 109.9(15) . .
B30 B29 C127 60.5(10) . .
B34 B29 C127 60.6(8) . .
B28 B29 B33 57.8(10) . .
B30 B29 B33 105.5(15) . .
B34 B29 B33 60.7(8) . .
C127 B29 B33 108.9(12) . .
C128 B30 B31 63.7(14) . .
C128 B30 B29 108.5(12) . .
B31 B30 B29 108.9(14) . .
C128 B30 B28 111.3(17) . .
B31 B30 B28 60.5(13) . .
B29 B30 B28 59.6(11) . .
C128 B30 C127 59.5(10) . .
B31 B30 C127 111.1(15) . .
B29 B30 C127 60.5(10) . .
B28 B30 C127 109.4(13) . .
B36 B31 B32 61.8(10) . .
B36 B31 B30 102.3(11) . .
B32 B31 B30 108.3(17) . .
B36 B31 B28 104.5(12) . .
B32 B31 B28 59.4(12) . .
B30 B31 B28 59.9(14) . .
B36 B31 C128 59.5(9) . .
B32 B31 C128 110.3(11) . .
B30 B31 C128 55.1(11) . .
B28 B31 C128 104.0(15) . .
B31 B32 B28 61.9(14) . .
B31 B32 B33 108.7(15) . .
B28 B32 B33 59.2(10) . .
B31 B32 B36 57.6(10) . .
B28 B32 B36 103.3(12) . .
B33 B32 B36 102.2(10) . .
B31 B32 B35 102.9(10) . .
B28 B32 B35 102.8(11) . .
B33 B32 B35 58.0(8) . .
B36 B32 B35 55.0(7) . .
B35 B33 B28 106.2(12) . .
B35 B33 B32 61.6(8) . .
B28 B33 B32 60.2(11) . .
B35 B33 B29 103.8(11) . .
B28 B33 B29 59.9(10) . .
B32 B33 B29 108.6(13) . .
B35 B33 B34 58.3(7) . .
B28 B33 B34 108.5(11) . .
B32 B33 B34 110.7(11) . .
B29 B33 B34 59.4(8) . .
B35 B34 B29 103.6(10) . .
B35 B34 C127 104.5(11) . .
B29 B34 C127 59.8(9) . .
B35 B34 B33 57.5(8) . .
B29 B34 B33 59.9(8) . .
C127 B34 B33 107.6(10) . .
B35 B34 Co4 63.8(6) . .
B29 B34 Co4 116.7(11) . .
C127 B34 Co4 64.5(8) . .
B33 B34 Co4 116.1(9) . .
O4 C35 C36 107.6(8) . .
B36 B35 B33 109.7(11) . .
B36 B35 B34 111.3(11) . .
B33 B35 B34 64.1(8) . .
B36 B35 B32 62.0(8) . .
B33 B35 B32 60.4(9) . .
B34 B35 B32 114.6(11) . .
B36 B35 Co4 66.8(6) . .
B33 B35 Co4 124.3(9) . .
B34 B35 Co4 66.5(6) . .
B32 B35 Co4 124.6(9) . .
N2 C36 C37 122.4(10) . .
N2 C36 C35 118.5(8) . .
C37 C36 C35 119.1(9) . .
B35 B36 B31 111.9(13) . .
B35 B36 C128 110.0(11) . .
B31 B36 C128 64.1(10) . .
B35 B36 B32 63.0(8) . .
B31 B36 B32 60.6(10) . .
C128 B36 B32 112.9(12) . .
B35 B36 Co4 66.1(5) . .
B31 B36 Co4 126.2(12) . .
C128 B36 Co4 67.0(6) . .
B32 B36 Co4 124.9(9) . .
C38 C37 C36 119.5(10) . .
C37 C38 C39 120.4(9) . .
C44 C39 C38 124.5(9) . .
C44 C39 C40 118.6(9) . .
C38 C39 C40 116.9(9) . .
N2 C40 C41 121.3(9) . .
N2 C40 C39 120.6(8) . .
C41 C40 C39 118.1(9) . .
C42 C41 C40 119.4(10) . .
C41 C42 C43 122.3(12) . .
C44 C43 C42 120.1(12) . .
C43 C44 C39 121.4(10) . .
O3 C45 C46 107.3(8) . .
C45 C46 C47 110.5(9) . .
O6 C48 C49 108.9(8) . .
N3 C49 C50 123.3(10) . .
N3 C49 C48 120.1(9) . .
C50 C49 C48 116.4(9) . .
C51 C50 C49 119.4(11) . .
C50 C51 C52 119.4(11) . .
C53 C52 C57 118.9(11) . .
C53 C52 C51 118.3(10) . .
C57 C52 C51 122.6(11) . .
C52 C53 C54 120.8(10) . .
C52 C53 N3 121.3(9) . .
C54 C53 N3 118.0(9) . .
C55 C54 C53 119.5(11) . .
C54 C55 C56 119.7(11) . .
C57 C56 C55 120.1(11) . .
C56 C57 C52 120.8(12) . .
O5 C58 C59 112.9(8) . .
C58 C59 C60 113.1(9) . .
C66 C61 C62 121.8(10) . .
C66 C61 C81 121.4(9) . .
C62 C61 C81 116.7(9) . .
C63 C62 C61 119.2(9) . .
C62 C63 C64 121.2(10) . .
C62 C63 O7 123.8(9) . .
C64 C63 O7 115.0(9) . .
C63 C64 C65 120.4(9) . .
C63 C64 O8 115.8(9) . .
C65 C64 O8 123.7(10) . .
C64 C65 C66 119.0(9) . .
C61 C66 C65 118.2(10) . .
C61 C66 C67 126.2(9) . .
C65 C66 C67 115.4(9) . .
C66 C67 C68 115.8(9) . .
C73 C68 C69 117.4(10) . .
C73 C68 C67 125.1(10) . .
C69 C68 C67 117.4(10) . .
C70 C69 C68 123.3(11) . .
O9 C70 C69 126.1(11) . .
O9 C70 C71 116.6(11) . .
C69 C70 C71 117.3(11) . .
C72 C71 O10 125.5(11) . .
C72 C71 C70 120.2(10) . .
O10 C71 C70 114.3(10) . .
C71 C72 C73 121.5(11) . .
C68 C73 C72 120.1(10) . .
C68 C73 C74 121.4(10) . .
C72 C73 C74 118.4(10) . .
C75 C74 C73 112.0(8) . .
C80 C75 C76 117.2(10) . .
C80 C75 C74 124.8(10) . .
C76 C75 C74 118.0(9) . .
C77 C76 C75 122.4(9) . .
C78 C77 O11 115.8(8) . .
C78 C77 C76 119.5(9) . .
O11 C77 C76 124.6(8) . .
C77 C78 C79 120.0(9) . .
C77 C78 O12 114.4(9) . .
C79 C78 O12 125.6(9) . .
C78 C79 C80 121.0(9) . .
C75 C80 C79 119.6(10) . .
C75 C80 C81 123.3(10) . .
C79 C80 C81 117.0(9) . .
C80 C81 C61 109.5(8) . .
O7 C82 C83 108.4(8) . .
N4 C83 C84 123.8(10) . .
N4 C83 C82 116.8(9) . .
C84 C83 C82 119.4(9) . .
C85 C84 C83 116.7(10) . .
C84 C85 C86 122.4(10) . .
C85 C86 C91 124.8(10) . .
C85 C86 C87 117.9(10) . .
C91 C86 C87 117.3(10) . .
N4 C87 C88 120.0(9) . .
N4 C87 C86 119.8(9) . .
C88 C87 C86 120.3(9) . .
C89 C88 C87 119.8(10) . .
C88 C89 C90 120.3(11) . .
C91 C90 C89 121.4(11) . .
C90 C91 C86 121.0(10) . .
O8 C92 C93 106.7(8) . .
C94 C93 C92 112.3(10) . .
O9 C95 C96 104.8(15) . .
C97 C96 N5 132(2) . .
C97 C96 C95 114(2) . .
N5 C96 C95 114.1(19) . .
C96 C97 C98 111(2) . .
C97 C98 C99 126.8(18) . .
C97 C98 C104 116(2) . .
C99 C98 C104 117.0(17) . .
C100 C99 C101 127.9(19) . .
C100 C99 C98 114.7(14) . .
C101 C99 C98 117.4(17) . .
C99 C100 N5 125(2) . .
C99 C101 C102 121(2) . .
C103 C102 C101 125(2) . .
C102 C103 C104 116(2) . .
C103 C104 C98 122(3) . .
O10 C105 C106 106(2) . .
C107 C106 C105 102(3) . .
O11 C108 C109 109.1(8) . .
N6 C109 C110 124.1(10) . .
N6 C109 C108 117.9(9) . .
C110 C109 C108 118.0(10) . .
C111 C110 C109 119.3(11) . .
C110 C111 C112 120.1(10) . .
C117 C112 C113 118.4(10) . .
C117 C112 C111 124.2(10) . .
C113 C112 C111 117.4(10) . .
C112 C113 N6 121.7(10) . .
C112 C113 C114 119.4(11) . .
N6 C113 C114 118.9(9) . .
C115 C114 C113 121.6(10) . .
C114 C115 C116 119.0(11) . .
C117 C116 C115 119.4(12) . .
C112 C117 C116 122.1(11) . .
O12 C118 C119 111.9(8) . .
C118 C119 C120 113.0(10) . .
B7 C123 B2 59.3(7) . .
B7 C123 B3 106.2(9) . .
B2 C123 B3 58.4(8) . .
B7 C123 C124 106.9(8) . .
B2 C123 C124 106.2(10) . .
B3 C123 C124 60.2(8) . .
B7 C123 Co3 64.3(5) . .
B2 C123 Co3 115.5(7) . .
B3 C123 Co3 115.7(8) . .
C124 C123 Co3 63.3(5) . .
B9 C124 B3 102.0(9) . .
B9 C124 C123 104.5(9) . .
B3 C124 C123 59.5(7) . .
B9 C124 B4 57.6(8) . .
B3 C124 B4 59.4(7) . .
C123 C124 B4 108.2(9) . .
B9 C124 Co3 64.2(6) . .
B3 C124 Co3 117.1(7) . .
C123 C124 Co3 65.6(5) . .
B4 C124 Co3 117.4(8) . .
B16 C125 B12 105.5(10) . .
B16 C125 B15 59.5(8) . .
B12 C125 B15 59.6(8) . .
B16 C125 C126 106.7(9) . .
B12 C125 C126 60.9(8) . .
B15 C125 C126 109.3(11) . .
B16 C125 Co3 64.0(6) . .
B12 C125 Co3 118.8(9) . .
B15 C125 Co3 118.3(9) . .
C126 C125 Co3 65.6(5) . .
B18 C126 B11 61.2(8) . .
B18 C126 B12 106.4(9) . .
B11 C126 B12 59.3(8) . .
B18 C126 C125 104.0(9) . .
B11 C126 C125 104.7(9) . .
B12 C126 C125 57.3(8) . .
B18 C126 Co3 62.0(6) . .
B11 C126 Co3 115.8(8) . .
B12 C126 Co3 113.9(9) . .
C125 C126 Co3 63.5(6) . .
C128 C127 B29 104.6(12) . .
C128 C127 B30 56.1(12) . .
B29 C127 B30 59.0(11) . .
C128 C127 B34 107.2(12) . .
B29 C127 B34 59.5(9) . .
B30 C127 B34 105.5(11) . .
C128 C127 Co4 66.2(9) . .
B29 C127 Co4 115.8(10) . .
B30 C127 Co4 114.5(13) . .
B34 C127 Co4 63.8(7) . .
B30 C128 C127 64.4(12) . .
B30 C128 B36 104.6(12) . .
C127 C128 B36 106.9(11) . .
B30 C128 B31 61.1(13) . .
C127 C128 B31 112.9(15) . .
B36 C128 B31 56.4(10) . .
B30 C128 Co4 120.7(13) . .
C127 C128 Co4 65.3(7) . .
B36 C128 Co4 63.4(7) . .
B31 C128 Co4 115.9(11) . .
B22 C129 C130 112.5(12) . .
B22 C129 B27 62.7(10) . .
C130 C129 B27 110.1(10) . .
B22 C129 B23 64.2(12) . .
C130 C129 B23 60.8(11) . .
B27 C129 B23 114.4(11) . .
B22 C129 Co4 123.6(10) . .
C130 C129 Co4 67.4(7) . .
B27 C129 Co4 65.2(7) . .
B23 C129 Co4 124.1(11) . .
C129 C130 B24 107.9(13) . .
C129 C130 B23 60.5(12) . .
B24 C130 B23 61.2(10) . .
C129 C130 B25 108.6(12) . .
B24 C130 B25 63.1(8) . .
B23 C130 B25 113.5(10) . .
C129 C130 Co4 64.9(8) . .
B24 C130 Co4 122.1(9) . .
B23 C130 Co4 121.4(14) . .
B25 C130 Co4 66.1(6) . .
O1 C32B C33B 107.8(18) . .
C34B C33B C32B 94(3) . .
C30 C29 C28 116(2) . .
C30 C31 C26 118.4(19) . .
C27 C28 C29 120(2) . .
C31 C30 C29 127(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N2 2.189(7) 1_455
Ag1 N6 2.197(7) .
Ag1 O11 2.513(7) .
O1 C3 1.356(13) .
O1 C32B 1.42(2) .
N1 C23 1.252(17) .
N1 C27 1.365(18) .
C1 C6 1.356(15) .
C1 C2 1.430(14) .
C1 C21 1.522(15) .
B1 B6 1.74(2) .
B1 B2 1.74(2) .
B1 B3 1.755(19) .
B1 B5 1.770(18) .
B1 B4 1.81(2) .
Ag2 N4 2.198(7) .
Ag2 N3 2.200(8) .
Ag2 O6 2.510(6) .
O2 C4 1.384(13) .
O2 C22 1.432(15) .
N2 C36 1.300(13) .
N2 C40 1.378(13) .
N2 Ag1 2.189(7) 1_655
C2 C3 1.394(16) .
B2 B6 1.741(17) .
B2 B3 1.74(2) .
B2 B7 1.755(18) .
B2 C123 1.782(17) .
Co3 B16 2.037(10) .
Co3 B9 2.039(13) .
Co3 B8 2.043(11) .
Co3 B18 2.051(15) .
Co3 B17 2.059(11) .
Co3 C124 2.077(12) .
Co3 B7 2.087(12) .
Co3 C125 2.105(13) .
Co3 C123 2.117(10) .
Co3 C126 2.141(13) .
O3 C10 1.380(12) .
O3 C45 1.426(11) .
N3 C49 1.298(13) .
N3 C53 1.434(14) .
C3 C4 1.422(16) .
B3 C123 1.79(2) .
B3 B4 1.80(2) .
B3 C124 1.804(17) .
Co4 B35 2.032(11) .
Co4 B27 2.035(14) .
Co4 B36 2.044(11) .
Co4 C129 2.055(14) .
Co4 B26 2.074(12) .
Co4 B34 2.077(16) .
Co4 C127 2.089(17) .
Co4 C130 2.095(16) .
Co4 C128 2.104(14) .
Co4 B25 2.119(13) .
O4 C11 1.373(13) .
O4 C35 1.441(11) .
N4 C83 1.317(13) .
N4 C87 1.363(12) .
C4 C5 1.389(15) .
B4 B9 1.712(18) .
B4 B5 1.78(2) .
B4 C124 1.84(2) .
O5 C17 1.376(13) .
O5 C58 1.416(12) .
N5 C100 1.35(3) .
N5 C96 1.48(3) .
C5 C6 1.360(15) .
B5 B8 1.71(2) .
B5 B6 1.71(2) .
B5 B9 1.72(2) .
O6 C18 1.376(12) .
O6 C48 1.416(11) .
N6 C109 1.345(13) .
N6 C113 1.404(14) .
C6 C7 1.547(14) .
B6 B8 1.682(16) .
B6 B7 1.817(19) .
O7 C63 1.402(12) .
O7 C82 1.415(12) .
N7 O14 1.27(2) .
N7 O13 1.31(2) .
N7 C121 1.41(3) .
C7 C8 1.505(16) .
B7 B8 1.700(17) .
B7 C123 1.766(17) .
O8 C64 1.399(12) .
O8 C92 1.437(12) .
N8 O16 1.19(3) .
N8 O17 1.35(3) .
N8 C122 1.37(5) .
C8 C9 1.395(15) .
C8 C13 1.407(14) .
B8 B9 1.637(19) .
O9 C70 1.367(14) .
O9 C95 1.38(2) .
C9 C10 1.383(15) .
B9 C124 1.712(17) .
O10 C105 1.38(2) .
O10 C71 1.384(14) .
C10 C11 1.389(14) .
B10 B12 1.74(2) .
B10 B14 1.75(2) .
B10 B15 1.75(3) .
B10 B11 1.77(2) .
B10 B13 1.77(2) .
O11 C77 1.377(12) .
O11 C108 1.456(11) .
C11 C12 1.388(15) .
B11 B13 1.758(18) .
B11 B12 1.79(2) .
B11 C126 1.80(2) .
B11 B18 1.833(18) .
O12 C78 1.393(12) .
O12 C118 1.448(11) .
C12 C13 1.404(15) .
B12 B15 1.74(2) .
B12 C125 1.74(2) .
B12 C126 1.807(17) .
C13 C14 1.522(15) .
B13 B17 1.718(19) .
B13 B14 1.77(2) .
B13 B18 1.820(17) .
C14 C15 1.522(15) .
B14 B15 1.74(2) .
B14 B17 1.744(15) .
B14 B16 1.76(2) .
C15 C16 1.382(14) .
C15 C20 1.400(14) .
B15 B16 1.705(19) .
B15 C125 1.759(18) .
C16 C17 1.372(15) .
B16 B17 1.650(17) .
B16 C125 1.676(18) .
C17 C18 1.421(14) .
B17 B18 1.699(16) .
C18 C19 1.325(15) .
B18 C126 1.798(18) .
C19 C20 1.434(14) .
B19 B20 1.735(19) .
B19 B24 1.76(3) .
B19 B21 1.79(2) .
B19 B22 1.80(3) .
B19 B23 1.82(2) .
C20 C21 1.531(15) .
B20 B21 1.76(2) .
B20 B25 1.764(18) .
B20 B24 1.76(2) .
B20 B26 1.780(18) .
B21 B27 1.740(17) .
B21 B22 1.79(2) .
B21 B26 1.797(18) .
C22 C23 1.450(17) .
B22 C129 1.68(2) .
B22 B27 1.75(3) .
B22 B23 1.80(3) .
C23 C24 1.37(2) .
B23 C129 1.71(3) .
B23 C130 1.71(2) .
B23 B24 1.74(3) .
C24 C25 1.38(2) .
B24 C130 1.71(2) .
B24 B25 1.81(2) .
C25 C26 1.32(2) .
B25 C130 1.757(18) .
B25 B26 1.77(2) .
C26 C27 1.46(2) .
C26 C31 1.56(2) .
B26 B27 1.730(19) .
C27 C28 1.42(2) .
B27 C129 1.68(2) .
B28 B33 1.73(2) .
B28 B32 1.75(3) .
B28 B29 1.77(3) .
B28 B30 1.78(3) .
B28 B31 1.79(3) .
B29 B30 1.78(3) .
B29 B34 1.80(2) .
B29 C127 1.80(2) .
B29 B33 1.81(2) .
B30 C128 1.66(3) .
B30 B31 1.77(4) .
B30 C127 1.80(2) .
B31 B36 1.68(2) .
B31 B32 1.73(3) .
B31 C128 1.82(2) .
B32 B33 1.75(2) .
B32 B36 1.76(2) .
B32 B35 1.773(16) .
B33 B35 1.710(19) .
B33 B34 1.823(18) .
B34 B35 1.725(19) .
B34 C127 1.82(2) .
C35 C36 1.503(15) .
B35 B36 1.629(18) .
C36 C37 1.408(14) .
B36 C128 1.74(2) .
C37 C38 1.356(16) .
C38 C39 1.414(16) .
C39 C44 1.406(16) .
C39 C40 1.431(13) .
C40 C41 1.421(15) .
C41 C42 1.363(16) .
C42 C43 1.370(15) .
C43 C44 1.345(17) .
C45 C46 1.505(16) .
C46 C47 1.552(14) .
C48 C49 1.493(14) .
C49 C50 1.404(15) .
C50 C51 1.364(17) .
C51 C52 1.429(16) .
C52 C53 1.369(15) .
C52 C57 1.396(17) .
C53 C54 1.415(15) .
C54 C55 1.354(16) .
C55 C56 1.418(16) .
C56 C57 1.356(17) .
C58 C59 1.497(16) .
C59 C60 1.545(16) .
C61 C66 1.373(15) .
C61 C62 1.379(15) .
C61 C81 1.571(14) .
C62 C63 1.368(14) .
C63 C64 1.370(15) .
C64 C65 1.383(15) .
C65 C66 1.432(14) .
C66 C67 1.530(16) .
C67 C68 1.538(15) .
C68 C73 1.380(16) .
C68 C69 1.393(15) .
C69 C70 1.379(17) .
C70 C71 1.411(18) .
C71 C72 1.349(15) .
C72 C73 1.395(15) .
C73 C74 1.552(15) .
C74 C75 1.495(15) .
C75 C80 1.402(14) .
C75 C76 1.415(15) .
C76 C77 1.386(15) .
C77 C78 1.377(13) .
C78 C79 1.380(14) .
C79 C80 1.417(15) .
C80 C81 1.513(14) .
C82 C83 1.516(15) .
C83 C84 1.409(14) .
C84 C85 1.362(16) .
C85 C86 1.364(16) .
C86 C91 1.426(16) .
C86 C87 1.440(14) .
C87 C88 1.401(15) .
C88 C89 1.389(17) .
C89 C90 1.392(15) .
C90 C91 1.358(16) .
C92 C93 1.523(16) .
C93 C94 1.491(15) .
C95 C96 1.75(3) .
C96 C97 1.21(2) .
C97 C98 1.33(2) .
C98 C99 1.42(3) .
C98 C104 1.44(3) .
C99 C100 1.32(2) .
C99 C101 1.34(2) .
C101 C102 1.38(3) .
C102 C103 1.30(3) .
C103 C104 1.36(3) .
C105 C106 1.57(4) .
C106 C107 1.38(4) .
C108 C109 1.514(15) .
C109 C110 1.376(14) .
C110 C111 1.360(17) .
C111 C112 1.440(16) .
C112 C117 1.381(17) .
C112 C113 1.396(15) .
C113 C114 1.415(16) .
C114 C115 1.368(17) .
C115 C116 1.397(16) .
C116 C117 1.397(17) .
C118 C119 1.515(15) .
C119 C120 1.520(16) .
C123 C124 1.808(18) .
C125 C126 1.824(19) .
C127 C128 1.72(3) .
C129 C130 1.68(3) .
C32B C33B 1.52(3) .
C33B C34B 1.35(5) .
C29 C30 1.43(3) .
C29 C28 1.52(3) .
C31 C30 1.33(3) .
