Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7219093
Preview
| Coordinates | 7219093.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C88 H148 N6 Nd2 O9 Si4 |
|---|---|
| Calculated formula | C88 H124 N6 Nd2 O9 Si4 |
| Title of publication | Carboxylation of terminal alkynes with CO2catalyzed by bis(amidate) rare-earth metal amides |
| Authors of publication | Cheng, Hao; Zhao, Bei; Yao, Yingming; Lu, Chengrong |
| Journal of publication | Green Chem. |
| Year of publication | 2015 |
| Journal volume | 17 |
| Journal issue | 3 |
| Pages of publication | 1675 |
| a | 13.883 ± 0.003 Å |
| b | 14.024 ± 0.003 Å |
| c | 15.361 ± 0.004 Å |
| α | 109.019 ± 0.003° |
| β | 106.371 ± 0.002° |
| γ | 98.531 ± 0.004° |
| Cell volume | 2616 ± 1.1 Å3 |
| Cell temperature | 223 ± 2 K |
| Ambient diffraction temperature | 223 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0957 |
| Residual factor for significantly intense reflections | 0.0737 |
| Weighted residual factors for significantly intense reflections | 0.1654 |
| Weighted residual factors for all reflections included in the refinement | 0.1846 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.105 |
| Diffraction radiation wavelength | 0.71075 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 180521 (current) | 2016-03-26 | cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/90. |
7219093.cif |
| 135055 | 2015-04-06 | cif/ Updating files of 7219093, 7219094, 7219095 Original log message: Adding full bibliography for 7219093--7219095.cif. |
7219093.cif |
| 128800 | 2014-12-17 | cif/ Adding structures of 7219093, 7219094, 7219095 via cif-deposit CGI script. |
7219093.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.