Crystallography Open Database

Information card for entry 7219348

7219347 << 7219348 >> 7219349

Preview

Coordinates	7219348.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C148 H142 Cl Ir4 N20 O37 Pb2
Calculated formula	C148 H142 Cl Ir4 N20 O37 Pb2
Title of publication	Four new lead(ii)‒iridium(iii) heterobimetallic coordination frameworks: synthesis, structures, luminescence and oxygen-sensing properties
Authors of publication	Chen, Yi-Ting; Lin, Chun-Yen; Lee, Gene-Hsiang; Ho, Mei-Lin
Journal of publication	CrystEngComm
Year of publication	2015
Journal volume	17
Journal issue	10
Pages of publication	2129
a	29.4296 ± 0.0007 Å
b	8.7352 ± 0.0002 Å
c	30.6568 ± 0.0007 Å
α	90°
β	99.2586 ± 0.0007°
γ	90°
Cell volume	7778.4 ± 0.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/n 1
Hall space group symbol	-P 2yac
Residual factor for all reflections	0.0539
Residual factor for significantly intense reflections	0.0429
Weighted residual factors for significantly intense reflections	0.1263
Weighted residual factors for all reflections included in the refinement	0.1368
Goodness-of-fit parameter for all reflections included in the refinement	1.092
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180524 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/93.	7219348.cif
133178	2015-03-06	cif/ Updating files of 7219347, 7219348, 7219349, 7219350 Original log message: Adding full bibliography for 7219347--7219350.cif.	7219348.cif
130026	2015-01-22	cif/ Adding structures of 7219347, 7219348, 7219349, 7219350 via cif-deposit CGI script.	7219348.cif