Crystallography Open Database

Information card for entry 7221828

Preview

Coordinates	7221828.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H49 N3 Si3
Calculated formula	C22 H49 N3 Si3
SMILES	C1(CCCCC1)/N=C(/N(C1CCCCC1)[Si](C)(C)C)N([Si](C)(C)C)[Si](C)(C)C
Title of publication	Synthesis, Characterization, Thermal Properties of Silicon(IV) Compounds Containing Guanidinato Ligands and Their Potential as CVD Precursors
Authors of publication	Du, Liyong; Chu, Wenxiang; Miao, Hongyan; Xu, Chongying; Ding, Yuqiang
Journal of publication	RSC Adv.
Year of publication	2015
a	9.0667 ± 0.0012 Å
b	11.4557 ± 0.0015 Å
c	14.1193 ± 0.0019 Å
α	100.93 ± 0.003°
β	102.475 ± 0.002°
γ	91.188 ± 0.002°
Cell volume	1403 ± 0.3 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0777
Residual factor for significantly intense reflections	0.0574
Weighted residual factors for significantly intense reflections	0.1809
Weighted residual factors for all reflections included in the refinement	0.2258
Goodness-of-fit parameter for all reflections included in the refinement	1.089
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	7221828.cif
153538	2015-08-20	cif/ Adding structures of 7221828, 7221829 via cif-deposit CGI script.	7221828.cif