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#$Date: 2015-09-18 07:53:48 +0300 (Fri, 18 Sep 2015) $
#$Revision: 157722 $
#$URL: svn://www.crystallography.net/cod/cif/7/22/22/7222204.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7222204
loop_
_publ_author_name
'Reading, J.'
'Knee, C.S.'
'Weller, M.T.'
_publ_section_title
;
 Syntheses, structures and properties of some osmates(IV, V) adopting the
 pyrochlore and weberite structures
;
_journal_name_full               'Journal of Materials Chemistry'
_journal_page_first              2376
_journal_page_last               2382
_journal_volume                  12
_journal_year                    2002
_chemical_formula_sum            'O6.63 Os2 Pb2'
_chemical_name_systematic        'Pb2 Os2 O6.63'
_space_group_IT_number           227
_symmetry_space_group_name_Hall  '-F 4vw 2vw 3'
_symmetry_space_group_name_H-M   'F d -3 m :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   10.35128
_cell_length_b                   10.35128
_cell_length_c                   10.35128
_cell_volume                     1109.129
_citation_journal_id_ASTM        JMACEP
_cod_data_source_file            Reading_JMACEP_2002_1967.cif
_cod_data_source_block           O6.63Os2Pb2
_cod_database_code               7222204
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-y,x+1/4,z+1/4
-x+3/4,-y+1/4,z+1/2
y+3/4,-x,z+3/4
x,-y+1/4,-z+1/4
y+3/4,x+1/4,-z+1/2
-x+3/4,y,-z+3/4
-y,-x,-z
z,x,y
-x,z+1/4,y+1/4
-z+3/4,-x+1/4,y+1/2
x+3/4,-z,y+3/4
z,-x+1/4,-y+1/4
x+3/4,z+1/4,-y+1/2
-z+3/4,x,-y+3/4
-x,-z,-y
y,z,x
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z+1/4,y+3/4,-x+1/2
-y+1/4,z+1/2,-x+3/4
-z,-y+1/2,-x+1/2
-y+1/4,-z+1/4,x
z+1/4,-y,x+1/4
-z+1/2,y+1/4,x+3/4
-x,-y,-z
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x-3/4,y-1/4,-z-1/2
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-x,y-1/4,z-1/4
-y-3/4,-x-1/4,z-1/2
x-3/4,-y,z-3/4
y,x,z
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x,z,y
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z,y-1/2,x-1/2
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y,-x+1/4,-z+1/4
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-y-3/4,x+1/2,-z-1/4
-x,y+1/4,z+1/4
-y-3/4,-x+1/4,z
x-3/4,-y+1/2,z-1/4
y,x+1/2,z+1/2
-z,-x+1/2,-y+1/2
x,-z+1/4,-y+1/4
z-3/4,x+1/4,-y
-x-3/4,z+1/2,-y-1/4
-z,x+1/4,y+1/4
-x-3/4,-z+1/4,y
z-3/4,-x+1/2,y-1/4
x,z+1/2,y+1/2
-y,-z+1/2,-x+1/2
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-z-1/4,-y-1/4,x
y-1/4,-z,x-1/4
z,y,x
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z-1/2,-y+1/4,-x-1/4
x+1/2,y,z+1/2
-y+1/2,x+1/4,z+3/4
-x+5/4,-y+1/4,z+1
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z+3/4,-y,x+3/4
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z+1/2,y-1/2,x
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z,-y-1/4,-x-1/4
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-x+5/4,y+1/2,-z+3/4
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z+1/2,x+1/2,y
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-x+1/2,y+1/4,z-1/4
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x-1/4,-y+1/2,z-3/4
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-z+1/2,x+1/4,y-1/4
-x-1/4,-z+1/4,y-1/2
z-1/4,-x+1/2,y-3/4
x+1/2,z+1/2,y
-y+1/2,-z+1/2,-x
-y,z-1/4,x-1/4
-z+1/4,-y-1/4,x-1/2
y+1/4,-z,x-3/4
z+1/2,y,x-1/2
y+1/4,z+1/4,-x
-z+1/4,y+1/2,-x-1/4
z,-y+1/4,-x-3/4
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_U_iso_or_equiv
O2 O-2 0.375 0.375 0.375 0.63 0.0
O1 O-2 0.31961 0.125 0.125 1 0.0
Os1 Os+4 0 0 0 1 0.0
Pb2 Pb+4 0.5 0.5 0.5 0.315 0.0
Pb1 Pb+2 0.5 0.5 0.5 0.685 0.0
