Crystallography Open Database

Information card for entry 7222483

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Structure parameters

Formula	C76 H106 O8 V2
Calculated formula	C76 H106 O8 V2
Title of publication	Vanadium(V) tetra-phenolate complexes: Synthesis, structural studies and ethylene homo-(co-)polymerization capability
Authors of publication	Redshaw, Carl; Walton, Mark; Elsegood, Mark Robert James; Prior, Timothy J.; Michiue, Kenji
Journal of publication	RSC Adv.
Year of publication	2015
a	11.3476 ± 0.0008 Å
b	12.2819 ± 0.0009 Å
c	16.8097 ± 0.0011 Å
α	100.861 ± 0.004°
β	99.097 ± 0.004°
γ	108.087 ± 0.005°
Cell volume	2127.4 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0848
Residual factor for significantly intense reflections	0.0566
Weighted residual factors for significantly intense reflections	0.1479
Weighted residual factors for all reflections included in the refinement	0.1587
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
301865 (current)	2025-08-22	Add cross-references to PubChem compounds in COD range 7/22/ Each referenced PubChem compound corresponds to the full crystal structure.	7222483.cif
176428	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	7222483.cif
161226	2015-10-09	cif/ Adding structures of 7222477, 7222478, 7222479, 7222480, 7222481, 7222482, 7222483 via cif-deposit CGI script.	7222483.cif