Crystallography Open Database

Information card for entry 7223634

Preview

Coordinates	7223634.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C83 H75 Gd4 N O37
Calculated formula	C83 H75 Gd4 N O37
Title of publication	[Ln4@Ln4] matryoshka tetrahedron: a novel secondary building unit
Authors of publication	Zhao, Jie; Wang, Xin; Zhao, Jing; Luo, Rui; Shen, Xuan; Zhu, Dunru; Jing, Su
Journal of publication	CrystEngComm
Year of publication	2016
Journal volume	18
Journal issue	6
Pages of publication	863
a	21.2232 ± 0.0006 Å
b	21.2232 ± 0.0006 Å
c	19.346 ± 0.0011 Å
α	90°
β	90°
γ	90°
Cell volume	8713.9 ± 0.6 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	86
Hermann-Mauguin space group symbol	P 42/n :2
Hall space group symbol	-P 4bc
Residual factor for all reflections	0.0438
Residual factor for significantly intense reflections	0.0329
Weighted residual factors for significantly intense reflections	0.0825
Weighted residual factors for all reflections included in the refinement	0.0874
Goodness-of-fit parameter for all reflections included in the refinement	1.071
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
175964 (current)	2016-02-05	cif/ Updating files of 7223633, 7223634, 7223635 Original log message: Adding full bibliography for 7223633--7223635.cif.	7223634.cif
171760	2015-12-30	cif/ Adding structures of 7223633, 7223634, 7223635 via cif-deposit CGI script.	7223634.cif