Crystallography Open Database

Information card for entry 7223950

Preview

Coordinates	7223950.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H25 Cl N2 Se Sn
Calculated formula	C14 H25 Cl N2 Se Sn
SMILES	c12[n](c(cc(C)n1)C)[Sn](C(C)(C)C)(C(C)(C)C)(Cl)[Se]2
Title of publication	Diorganotin(iv) 4,6-dimethyl-2-pyrimidyl selenolates: synthesis, structures and their utility as molecular precursors for the preparation of SnSe2nano-sheets and thin films
Authors of publication	Tyagi, Adish; Kedarnath, G.; Wadawale, Amey; Shah, Alpa Y.; Jain, Vimal K.; Vishwanadh, B.
Journal of publication	RSC Adv.
Year of publication	2016
Journal volume	6
Journal issue	10
Pages of publication	8367
a	9.192 ± 0.003 Å
b	12.655 ± 0.003 Å
c	15.99 ± 0.0018 Å
α	90°
β	92.278 ± 0.019°
γ	90°
Cell volume	1858.6 ± 0.8 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1745
Residual factor for significantly intense reflections	0.0482
Weighted residual factors for significantly intense reflections	0.1019
Weighted residual factors for all reflections included in the refinement	0.1484
Goodness-of-fit parameter for all reflections included in the refinement	1.016
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
174676 (current)	2016-01-21	cif/ Adding structures of 7223948, 7223949, 7223950 via cif-deposit CGI script.	7223950.cif