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Information card for entry 7224056
Preview
| Coordinates | 7224056.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H66 K4 Nb6 O33 Rh2 |
|---|---|
| Calculated formula | C24 H36 K4 Nb6 O33 Rh2 |
| Title of publication | Unique solubility of polyoxoniobate salts in methanol: coordination to cations and POM methylation |
| Authors of publication | Abramov, Pavel A.; Vicent, Cristian; Kompankov, Nikolay B.; Laricheva, Yuliya A.; Sokolov, Maksim Nailyevich |
| Journal of publication | RSC Adv. |
| Year of publication | 2016 |
| a | 14.6139 ± 0.0005 Å |
| b | 9.3769 ± 0.0003 Å |
| c | 19.9504 ± 0.0005 Å |
| α | 90° |
| β | 95.964 ± 0.001° |
| γ | 90° |
| Cell volume | 2719.07 ± 0.14 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0617 |
| Residual factor for significantly intense reflections | 0.0398 |
| Weighted residual factors for significantly intense reflections | 0.1143 |
| Weighted residual factors for all reflections included in the refinement | 0.157 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.143 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 175271 (current) | 2016-01-29 | cif/ Adding structures of 7224054, 7224055, 7224056 via cif-deposit CGI script. |
7224056.cif |
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Users of the data should acknowledge the original authors of the
structural data.