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Information card for entry 7224308
Preview
| Coordinates | 7224308.cif |
|---|---|
| Original paper (by DOI) | HTML |
| External links | PubChem |
| Formula | C22 H33 B Br Ge N3 |
|---|---|
| Calculated formula | C22 H33 B Br Ge N3 |
| SMILES | [Ge]1(Br)N(B(N(C(C)C)C(C)C)[NH]1c1c(C)cccc1C)c1c(C)cccc1C |
| Title of publication | Synthesis and reactivity of a germylene stabilized by a boraguanidinate ligand |
| Authors of publication | Böserle, Jiří; Alonso, Mercedes; Jambor, Roman; R°užička, Aleš; Dostál, Libor |
| Journal of publication | RSC Adv. |
| Year of publication | 2016 |
| Journal volume | 6 |
| Journal issue | 23 |
| Pages of publication | 19377 |
| a | 8.352 ± 0.0004 Å |
| b | 10.479 ± 0.0005 Å |
| c | 13.5181 ± 0.001 Å |
| α | 95.684 ± 0.005° |
| β | 100.864 ± 0.006° |
| γ | 90.338 ± 0.004° |
| Cell volume | 1155.83 ± 0.12 Å3 |
| Cell temperature | 150 ± 1 K |
| Ambient diffraction temperature | 150 ± 1 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0477 |
| Residual factor for significantly intense reflections | 0.0306 |
| Weighted residual factors for significantly intense reflections | 0.0627 |
| Weighted residual factors for all reflections included in the refinement | 0.0703 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.085 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301865 (current) | 2025-08-22 | Add cross-references to PubChem compounds in COD range 7/22/ Each referenced PubChem compound corresponds to the full crystal structure. |
7224308.cif |
| 176720 | 2016-02-18 | cif/ Adding structures of 7224296, 7224297, 7224298, 7224299, 7224300, 7224301, 7224302, 7224303, 7224304, 7224305, 7224306, 7224307, 7224308 via cif-deposit CGI script. |
7224308.cif |
All data in the COD and the database itself are dedicated to the
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Users of the data should acknowledge the original authors of the
structural data.