Crystallography Open Database

Information card for entry 7225010

Preview

Coordinates	7225010.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C50 H40 N10 O54 Pb2 Si W12
Calculated formula	C50 H40 N10 O54 Pb2 Si W12
Title of publication	Assembly of two novel 3D organic‒inorganic hybrids based on Keggin-type polyoxometalates: syntheses, crystal structures and properties
Authors of publication	Zhou, En-Long; Qin, Chao; Wang, Xin-Long; Shao, Kui-Zhan; Su, Zhong-Min
Journal of publication	CrystEngComm
Year of publication	2016
Journal volume	18
Journal issue	34
Pages of publication	6370
a	18.517 ± 0.0008 Å
b	15.842 ± 0.0011 Å
c	26.966 ± 0.005 Å
α	90 ± 0.001°
β	92.78 ± 0.001°
γ	90 ± 0.001°
Cell volume	7901.1 ± 1.6 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0508
Residual factor for significantly intense reflections	0.032
Weighted residual factors for significantly intense reflections	0.0549
Weighted residual factors for all reflections included in the refinement	0.0599
Goodness-of-fit parameter for all reflections included in the refinement	1.011
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
186358 (current)	2016-09-10	cif/ Updating files of 7225009, 7225010 Original log message: Adding full bibliography for 7225009--7225010.cif.	7225010.cif
182334	2016-04-28	cif/ Adding structures of 7225009, 7225010 via cif-deposit CGI script.	7225010.cif