Crystallography Open Database

Information card for entry 7225184

Preview

Coordinates	7225184.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	di[tetra(chrysazinato)-tetra(N,N-dimethylformamide)-tetra-cobalt(II)] di(N,N-dimethylformamide) solvate hemihydrate
Formula	C143.05 H120.45 Co8 N10.35 O42.85
Calculated formula	C142 H118 Co8 N10 O42.5
Title of publication	Transition metal coordination complexes of chrysazin
Authors of publication	Beldon, Patrick J.; Henke, Sebastian; Monserrat, Bartomeu; Tominaka, Satoshi; Stock, Norbert; Cheetham, Anthony K.
Journal of publication	CrystEngComm
Year of publication	2016
Journal volume	18
Journal issue	27
Pages of publication	5121
a	15.6278 ± 0.0016 Å
b	15.6996 ± 0.0015 Å
c	29.048 ± 0.003 Å
α	90.9201 ± 0.001°
β	104.139 ± 0.0016°
γ	90.234 ± 0.0013°
Cell volume	6909.9 ± 1.2 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0696
Residual factor for significantly intense reflections	0.0627
Weighted residual factors for significantly intense reflections	0.1777
Weighted residual factors for all reflections included in the refinement	0.1829
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
185227 (current)	2016-08-07	cif/ Updating files of 7225182, 7225183, 7225184, 7225185, 7225186, 7225187, 7225188, 7225189, 7225190, 7225191, 7225192 Original log message: Adding full bibliography for 7225182--7225192.cif.	7225184.cif
182887	2016-05-12	cif/ Adding structures of 7225182, 7225183, 7225184, 7225185, 7225186, 7225187, 7225188, 7225189, 7225190, 7225191, 7225192 via cif-deposit CGI script.	7225184.cif