Crystallography Open Database

Information card for entry 7225506

Preview

Coordinates	7225506.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C17 H29 Cl4 N3 Si2 Zr
Calculated formula	C17 H29 Cl4 N3 Si2 Zr
SMILES	[Zr]1(Cl)(Cl)(Cl)(Cl)[n]2c(cccc2)C2=[N]1[Si](N([Si](C)(C)C)C(=C2)C(C)(C)C)(C)C
Title of publication	Synthesis, mechanism and ethylene polymerization catalysis of Ge(IV), Sn(II) and Zr(IV) complexes derived from substituted β-diketiminates
Authors of publication	Xiao, Xia; Hao, Xiaomin; Bai, Jianliang; Chao, Jianbin; Cao, Wei; Chen, Xia
Journal of publication	RSC Adv.
Year of publication	2016
a	10.139 ± 0.002 Å
b	12.05 ± 0.002 Å
c	12.659 ± 0.003 Å
α	118.34 ± 0.03°
β	110.25 ± 0.03°
γ	91.62 ± 0.03°
Cell volume	1241.9 ± 0.7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0674
Residual factor for significantly intense reflections	0.0545
Weighted residual factors for significantly intense reflections	0.112
Weighted residual factors for all reflections included in the refinement	0.1181
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
183427 (current)	2016-06-11	cif/ Adding structures of 7225506, 7225507, 7225508 via cif-deposit CGI script.	7225506.cif