Crystallography Open Database

Information card for entry 7225714

Preview

Coordinates	7225714.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Bis(diisobutylammonium) octachlorodiantimonate(III)
Formula	C8 H20 Cl4 N Sb
Calculated formula	C8 H20 Cl4 N Sb
Title of publication	Enormous lattice distortion through an isomorphous phase transition in an organic‒inorganic hybrid based on haloantimonate(iii)
Authors of publication	Wojciechowska, Martyna; Szklarz, Przemysław; Białońska, Agata; Baran, Jan; Janicki, Rafał; Medycki, Wojciech; Durlak, Piotr; Piecha-Bisiorek, Anna; Jakubas, Ryszard
Journal of publication	CrystEngComm
Year of publication	2016
Journal volume	18
Journal issue	33
Pages of publication	6184
a	5.79 ± 0.002 Å
b	19.485 ± 0.003 Å
c	14.275 ± 0.003 Å
α	90°
β	101.28 ± 0.03°
γ	90°
Cell volume	1579.4 ± 0.7 Å³
Cell temperature	250 ± 2 K
Ambient diffraction temperature	250 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0728
Residual factor for significantly intense reflections	0.0343
Weighted residual factors for significantly intense reflections	0.0589
Weighted residual factors for all reflections included in the refinement	0.0645
Goodness-of-fit parameter for all reflections included in the refinement	0.822
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
186362 (current)	2016-09-10	cif/ Updating files of 7225712, 7225713, 7225714, 7225715 Original log message: Adding full bibliography for 7225712--7225715.cif.	7225714.cif
183998	2016-06-28	cif/ Adding structures of 7225712, 7225713, 7225714, 7225715 via cif-deposit CGI script.	7225714.cif