Crystallography Open Database

Information card for entry 7228053

Preview

Coordinates	7228053.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C15 H15 N O8 Yb
Calculated formula	C15 H15 N O8 Yb
Title of publication	Structural variety in ytterbium dicarboxylate frameworks and in situ study diffraction of their solvothermal crystallisation
Authors of publication	Breeze, Matthew I.; Chamberlain, Thomas W.; Clarkson, Guy J.; de Camargo, Raíssa Pires; Wu, Yue; de Lima, Juliana Fonseca; Millange, Franck; Serra, Osvaldo A.; O'Hare, Dermot; Walton, Richard I.
Journal of publication	CrystEngComm
Year of publication	2017
Journal volume	19
Journal issue	17
Pages of publication	2424
a	8.5054 ± 0.0002 Å
b	10.2435 ± 0.0002 Å
c	10.9144 ± 0.0003 Å
α	63.35 ± 0.002°
β	71.042 ± 0.002°
γ	82.5615 ± 0.0019°
Cell volume	803.65 ± 0.04 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0168
Residual factor for significantly intense reflections	0.0162
Weighted residual factors for significantly intense reflections	0.0362
Weighted residual factors for all reflections included in the refinement	0.0365
Goodness-of-fit parameter for all reflections included in the refinement	1.067
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
196373 (current)	2017-05-06	cif/ Updating files of 7228053, 7228054, 7228055, 7228056 Original log message: Adding full bibliography for 7228053--7228056.cif.	7228053.cif
195337	2017-04-12	cif/ Adding structures of 7228053, 7228054, 7228055, 7228056 via cif-deposit CGI script.	7228053.cif