Crystallography Open Database

Information card for entry 7229237

Preview

Coordinates	7229237.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C56 H53 Mg N O Si
Calculated formula	C56 H53 Mg N O Si
SMILES	C[Mg](N(c1c(cc(C)cc1C(c1ccccc1)c1ccccc1)C(c1ccccc1)c1ccccc1)[Si](c1ccccc1)(c1ccccc1)c1ccccc1)[O]1CCCC1
Title of publication	Sterically bulky amido magnesium methyl complexes: syntheses, structures and catalysis
Authors of publication	Ma, Mengtao; Li, Jia; Shen, Xingchao; Yu, Zhijuan; Yao, Weiwei; Pullarkat, Sumod A.
Journal of publication	RSC Adv.
Year of publication	2017
Journal volume	7
Journal issue	72
Pages of publication	45401
a	10.8664 ± 0.0004 Å
b	38.1625 ± 0.0015 Å
c	11.184 ± 0.0004 Å
α	90°
β	106.527 ± 0.001°
γ	90°
Cell volume	4446.3 ± 0.3 Å³
Cell temperature	135 ± 2 K
Ambient diffraction temperature	135 ± 2 K
Number of distinct elements	6
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0571
Residual factor for significantly intense reflections	0.0453
Weighted residual factors for significantly intense reflections	0.0986
Weighted residual factors for all reflections included in the refinement	0.1041
Goodness-of-fit parameter for all reflections included in the refinement	1.017
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
201254 (current)	2017-09-25	cif/ Adding structures of 7229234, 7229235, 7229236, 7229237 via cif-deposit CGI script.	7229237.cif