Crystallography Open Database

Information card for entry 7229751

Preview

Coordinates	7229751.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C135 H103 Cu F66 N8 O34 Sm3
Calculated formula	C135 H103 Cu F66 N8 O34 Sm3
Title of publication	Nitronyl nitroxide bridged 3d‒4f hetero-tri-spin chains: synthesis strategy, crystal structure and magnetic properties
Authors of publication	Zhu, Mei; Jia, Lingjie; Li, Yang; Li, Yungai; Zhang, Li; Zhang, Wei; Lü, Yaohong
Journal of publication	CrystEngComm
Year of publication	2018
Journal volume	20
Journal issue	4
Pages of publication	420
a	20.197 ± 0.003 Å
b	43.511 ± 0.006 Å
c	20.091 ± 0.003 Å
α	90°
β	113.503 ± 0.003°
γ	90°
Cell volume	16191 ± 4 Å³
Cell temperature	113 ± 2 K
Ambient diffraction temperature	113 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0653
Residual factor for significantly intense reflections	0.053
Weighted residual factors for significantly intense reflections	0.1455
Weighted residual factors for all reflections included in the refinement	0.155
Goodness-of-fit parameter for all reflections included in the refinement	0.997
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
228993 (current)	2019-11-17	cif/ Updating files of 7229746, 7229747, 7229748, 7229749, 7229750, 7229751, 7229752, 7229753 Original log message: Adding full bibliography for 7229746--7229753.cif.	7229751.cif
204281	2017-12-15	cif/ Adding structures of 7229746, 7229747, 7229748, 7229749, 7229750, 7229751, 7229752, 7229753 via cif-deposit CGI script.	7229751.cif