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Information card for entry 7230485
Preview
| Coordinates | 7230485.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C28 H49 Fe O P3 Si |
|---|---|
| Calculated formula | C28 H49 Fe O P3 Si |
| Title of publication | Transfer hydrogenation of aldehydes catalyzed by silyl hydrido iron complexes bearing a [PSiP] pincer ligand |
| Authors of publication | Zhang, Peng; Li, Xiaoyan; Qi, Xinghao; Sun, Hongjian; Fuhr, Olaf; Fenske, Dieter |
| Journal of publication | RSC Advances |
| Year of publication | 2018 |
| Journal volume | 8 |
| Journal issue | 25 |
| Pages of publication | 14092 |
| a | 13.567 ± 0.0005 Å |
| b | 16.78 ± 0.0005 Å |
| c | 13.9927 ± 0.0005 Å |
| α | 90° |
| β | 106.554 ± 0.003° |
| γ | 90° |
| Cell volume | 3053.46 ± 0.19 Å3 |
| Cell temperature | 153.15 K |
| Ambient diffraction temperature | 153.15 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0498 |
| Residual factor for significantly intense reflections | 0.0352 |
| Weighted residual factors for significantly intense reflections | 0.0877 |
| Weighted residual factors for all reflections included in the refinement | 0.0924 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.973 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 207379 (current) | 2018-04-17 | cif/ Adding structures of 7230485, 7230486 via cif-deposit CGI script. |
7230485.cif |
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Users of the data should acknowledge the original authors of the
structural data.