Crystallography Open Database

Information card for entry 7231712

Preview

Coordinates	7231712.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H69 N10 Na Ni7 O91 P2 W21
Calculated formula	C18 H24 N10 Na Ni7 O91 P2 W21
Title of publication	Steam-assisted assemblies of {Ni6PW9}-based inorganic‒organic hybrid chains: synthesis, crystal structures and properties
Authors of publication	Yin, Ying-Xue; Chen, Wei-Chao; Yao, Wei; Qin, Chao; Su, Zhong-Min
Journal of publication	CrystEngComm
Year of publication	2018
Journal volume	20
Journal issue	46
Pages of publication	7507
a	12.947 ± 0.003 Å
b	20.737 ± 0.005 Å
c	22.751 ± 0.004 Å
α	97.442 ± 0.01°
β	90.63 ± 0.009°
γ	93.308 ± 0.01°
Cell volume	6046 ± 2 Å³
Cell temperature	294 ± 2 K
Ambient diffraction temperature	294 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1247
Residual factor for significantly intense reflections	0.0893
Weighted residual factors for significantly intense reflections	0.2191
Weighted residual factors for all reflections included in the refinement	0.2539
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
229028 (current)	2019-11-17	cif/ Updating files of 7231711, 7231712, 7231713 Original log message: Adding full bibliography for 7231711--7231713.cif.	7231712.cif
211696	2018-10-30	cif/ Adding structures of 7231711, 7231712, 7231713 via cif-deposit CGI script.	7231712.cif