Crystallography Open Database

Information card for entry 7231750

Preview

Coordinates	7231750.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H26 N2 O13 Pb2
Calculated formula	C24 H11 N O9 Pb2
Title of publication	A series of metal‒organic frameworks constructed by a rigid-flexible 5-(bis(4-carboxybenzyl)amino)isophthalic acid: syntheses, crystal structures and physical properties
Authors of publication	Qiao, Yu; Ma, Yufeng; Jiang, Wei; Wang, Xiuyan; Guan, Weisheng; Che, Guangbo; Li, Weikang; Qin, Fang
Journal of publication	CrystEngComm
Year of publication	2018
Journal volume	20
Journal issue	48
Pages of publication	7782
a	11.117 ± 0.001 Å
b	11.2139 ± 0.001 Å
c	13.6948 ± 0.0012 Å
α	104.059 ± 0.001°
β	100.259 ± 0.001°
γ	93.09 ± 0.002°
Cell volume	1621.2 ± 0.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0742
Residual factor for significantly intense reflections	0.0562
Weighted residual factors for significantly intense reflections	0.1677
Weighted residual factors for all reflections included in the refinement	0.1823
Goodness-of-fit parameter for all reflections included in the refinement	1.079
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
229050 (current)	2019-11-17	cif/ Updating files of 7231749, 7231750, 7231751, 7231752 Original log message: Adding full bibliography for 7231749--7231752.cif.	7231750.cif
211732	2018-11-01	cif/ Adding structures of 7231749, 7231750, 7231751, 7231752 via cif-deposit CGI script.	7231750.cif