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Information card for entry 7231763
Preview
| Coordinates | 7231763.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C17 H20 N4 O5 |
|---|---|
| Calculated formula | C17 H20 N4 O5 |
| Title of publication | An efficient nickel/silver co-catalyzed remote C‒H amination of 8-aminoquinolines with azodicarboxylates at room temperature |
| Authors of publication | Zhao, Ruinan; Yang, Yaocheng; Wang, Xia; Ren, Peng; Zhang, Qian; Li, Dong |
| Journal of publication | RSC Advances |
| Year of publication | 2018 |
| Journal volume | 8 |
| Journal issue | 65 |
| Pages of publication | 37064 |
| a | 9.3537 ± 0.0005 Å |
| b | 22.3285 ± 0.0017 Å |
| c | 8.8584 ± 0.0006 Å |
| α | 90° |
| β | 105.591 ± 0.006° |
| γ | 90° |
| Cell volume | 1782 ± 0.2 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.056 |
| Residual factor for significantly intense reflections | 0.0436 |
| Weighted residual factors for significantly intense reflections | 0.1129 |
| Weighted residual factors for all reflections included in the refinement | 0.1236 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.05 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 211807 (current) | 2018-11-06 | cif/ Adding structures of 7231763 via cif-deposit CGI script. |
7231763.cif |
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Users of the data should acknowledge the original authors of the
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