Crystallography Open Database

Information card for entry 7232223

Preview

Coordinates	7232223.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H26 N9 O6 Sm
Calculated formula	C46 H26 N9 O6 Sm
Title of publication	Synthesis, structures and properties of six lanthanide complexes based on a 2-(2-carboxyphenyl)imidazo(4,5-f)-(1,10)phenanthroline ligand
Authors of publication	Ren, Shanshan; Jiang, Wei; Wang, Qingwei; Li, Zhimin; Qiao, Yu; Che, Guangbo
Journal of publication	RSC Advances
Year of publication	2019
Journal volume	9
Journal issue	6
Pages of publication	3102
a	10.6094 ± 0.0006 Å
b	13.7009 ± 0.0007 Å
c	14.5285 ± 0.0007 Å
α	78.738 ± 0.001°
β	80.42 ± 0.001°
γ	68.369 ± 0.001°
Cell volume	1914.96 ± 0.17 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0511
Residual factor for significantly intense reflections	0.0391
Weighted residual factors for significantly intense reflections	0.0768
Weighted residual factors for all reflections included in the refinement	0.0824
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
213281 (current)	2019-01-24	cif/ Adding structures of 7232219, 7232220, 7232221, 7232222, 7232223, 7232224 via cif-deposit CGI script.	7232223.cif