Crystallography Open Database

Information card for entry 7232250

Preview

Coordinates	7232250.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C6 H24 N6 Ni Se7.5 Sn3
Calculated formula	C6 H16 N6 Ni Se7.5 Sn3
Title of publication	Alcohol-solvothermal syntheses, crystal structures and photocatalytic properties of tin selenides with polyselenide ligands
Authors of publication	Han, Jingyu; Zhang, Limei; Li, Shufen; Zheng, Wei; Jia, Dingxian; Yuan, Yaxian
Journal of publication	CrystEngComm
Year of publication	2019
Journal volume	21
Journal issue	10
Pages of publication	1642
a	14.869 ± 0.003 Å
b	11.888 ± 0.002 Å
c	13.86 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	2449.9 ± 0.8 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	6
Space group number	29
Hermann-Mauguin space group symbol	P c a 21
Hall space group symbol	P 2c -2ac
Residual factor for all reflections	0.0678
Residual factor for significantly intense reflections	0.0434
Weighted residual factors for significantly intense reflections	0.0842
Weighted residual factors for all reflections included in the refinement	0.1012
Goodness-of-fit parameter for all reflections included in the refinement	1.118
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
223487 (current)	2019-11-07	cif/ Updating files of 7232246, 7232247, 7232248, 7232249, 7232250, 7232251, 7232252, 7232253 Original log message: Adding full bibliography for 7232246--7232253.cif.	7232250.cif
213374	2019-01-30	cif/ Adding structures of 7232246, 7232247, 7232248, 7232249, 7232250, 7232251, 7232252, 7232253 via cif-deposit CGI script.	7232250.cif