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Information card for entry 7233592
Preview
| Coordinates | 7233592.cif |
|---|---|
| Original paper (by DOI) | HTML |
| External links | PubChem |
| Formula | C48 H48 N3 O3 P3 |
|---|---|
| Calculated formula | C48 H48 N3 O3 P3 |
| Title of publication | Catalyst-free hydrophosphination of alkenes in presence of 2-methyltetrahydrofuran: a green and easy access to a wide range of tertiary phosphines |
| Authors of publication | Bissessar, Damien; Egly, Julien; Achard, Thierry; Steffanut, Pascal; Bellemin-Laponnaz, Stéphane |
| Journal of publication | RSC Advances |
| Year of publication | 2019 |
| Journal volume | 9 |
| Journal issue | 47 |
| Pages of publication | 27250 |
| a | 15.8088 ± 0.0008 Å |
| b | 8.9035 ± 0.0005 Å |
| c | 33.389 ± 0.0016 Å |
| α | 90° |
| β | 116.64 ± 0.004° |
| γ | 90° |
| Cell volume | 4200.7 ± 0.4 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.1981 |
| Residual factor for significantly intense reflections | 0.1413 |
| Weighted residual factors for significantly intense reflections | 0.3985 |
| Weighted residual factors for all reflections included in the refinement | 0.4363 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.093 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301866 (current) | 2025-08-23 | Add cross-references to PubChem compounds in COD range 7/23/ Each referenced PubChem compound corresponds to the full crystal structure. |
7233592.cif |
| 217891 | 2019-08-31 | cif/ Adding structures of 7233592, 7233593 via cif-deposit CGI script. |
7233592.cif |
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Users of the data should acknowledge the original authors of the
structural data.