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Information card for entry 7234985
Preview
| Coordinates | 7234985.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C23 H21 N S |
|---|---|
| Calculated formula | C23 H21 N S |
| Title of publication | Ultra-small palladium nano-particles synthesized using bulky S/Se and N donor ligands as a stabilizer: application as catalysts for Suzuki‒Miyaura coupling |
| Authors of publication | Oswal, Preeti; Arora, Aayushi; Kaushal, Jolly; Rao, Gyandshwar Kumar; Kumar, Sushil; Singh, Ajai K.; Kumar, Arun |
| Journal of publication | RSC Advances |
| Year of publication | 2019 |
| Journal volume | 9 |
| Journal issue | 39 |
| Pages of publication | 22313 |
| a | 5.3825 ± 0.0007 Å |
| b | 15.3166 ± 0.0013 Å |
| c | 21.472 ± 0.003 Å |
| α | 89.91 ± 0.008° |
| β | 84.752 ± 0.01° |
| γ | 89.905 ± 0.009° |
| Cell volume | 1762.8 ± 0.4 Å3 |
| Cell temperature | 150.01 ± 0.1 K |
| Ambient diffraction temperature | 150.01 ± 0.1 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1042 |
| Residual factor for significantly intense reflections | 0.0821 |
| Weighted residual factors for significantly intense reflections | 0.2427 |
| Weighted residual factors for all reflections included in the refinement | 0.2912 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.131 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 223456 (current) | 2019-11-07 | cif/ Adding structures of 7234985 via cif-deposit CGI script. |
7234985.cif |
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Users of the data should acknowledge the original authors of the
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