Crystallography Open Database

Information card for entry 7235265

Preview

Coordinates	7235265.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H22 N3 O P Pd S
Calculated formula	C26 H22 N3 O P Pd S
Title of publication	Controlled interaction of benzaldehyde thiosemicarbazones with palladium: formation of bis-complexes with cis-geometry and organopalladium complexes, and their catalytic application in C‒C and C‒N coupling
Authors of publication	Dutta, Jayita; Bhattacharya, Samaresh
Journal of publication	RSC Advances
Year of publication	2013
Journal volume	3
Journal issue	27
Pages of publication	10707
a	9.9825 ± 0.001 Å
b	10.0841 ± 0.001 Å
c	26.259 ± 0.003 Å
α	100.477 ± 0.005°
β	93.419 ± 0.006°
γ	96.826 ± 0.005°
Cell volume	2571.9 ± 0.5 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.2105
Residual factor for significantly intense reflections	0.2018
Weighted residual factors for significantly intense reflections	0.4921
Weighted residual factors for all reflections included in the refinement	0.4961
Goodness-of-fit parameter for all reflections included in the refinement	1.319
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
232640 (current)	2019-11-23	cif/ Adding structures of 7235260, 7235261, 7235262, 7235263, 7235264, 7235265 via cif-deposit CGI script.	7235265.cif