Crystallography Open Database

Information card for entry 7235279

Preview

Coordinates	7235279.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C83.9 H58 N17.6 Ni3 O8.9
Calculated formula	C83.9 H57.6 N17.6 Ni3 O8.9
Title of publication	An indeno-quinoxaline based oxime ligand for the synthesis of polynuclear Ni(ii) clusters
Authors of publication	Canaj, Angelos B.; Nodaraki, Lydia E.; Philippidis, Aggelos; Tzimopoulos, Demetrios I.; Fotopoulou, Eirini; Siczek, Milosz; Lis, Tadeusz; Milios, Constantinos J.
Journal of publication	RSC Advances
Year of publication	2013
Journal volume	3
Journal issue	32
Pages of publication	13214
a	14.565 ± 0.007 Å
b	15.905 ± 0.007 Å
c	16.366 ± 0.008 Å
α	85.02 ± 0.05°
β	88.64 ± 0.05°
γ	73.41 ± 0.05°
Cell volume	3620 ± 3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.4374
Residual factor for significantly intense reflections	0.1214
Weighted residual factors for significantly intense reflections	0.1253
Weighted residual factors for all reflections included in the refinement	0.2189
Goodness-of-fit parameter for all reflections included in the refinement	0.932
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
232648 (current)	2019-11-23	cif/ Adding structures of 7235279, 7235280, 7235281, 7235282, 7235283 via cif-deposit CGI script.	7235279.cif