Crystallography Open Database

Information card for entry 7235283

Preview

Coordinates	7235283.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C135.75 H108.4 Cl2 N27 Ni8 O29.95
Calculated formula	C135.75 H108 Cl2 N27 Ni8 O29.95
Title of publication	An indeno-quinoxaline based oxime ligand for the synthesis of polynuclear Ni(ii) clusters
Authors of publication	Canaj, Angelos B.; Nodaraki, Lydia E.; Philippidis, Aggelos; Tzimopoulos, Demetrios I.; Fotopoulou, Eirini; Siczek, Milosz; Lis, Tadeusz; Milios, Constantinos J.
Journal of publication	RSC Advances
Year of publication	2013
Journal volume	3
Journal issue	32
Pages of publication	13214
a	17.608 ± 0.005 Å
b	18.43 ± 0.005 Å
c	21.084 ± 0.006 Å
α	81.07 ± 0.03°
β	82.32 ± 0.03°
γ	83.47 ± 0.03°
Cell volume	6668 ± 3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.174
Residual factor for significantly intense reflections	0.0613
Weighted residual factors for significantly intense reflections	0.0903
Weighted residual factors for all reflections included in the refinement	0.1021
Goodness-of-fit parameter for all reflections included in the refinement	1.019
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
232648 (current)	2019-11-23	cif/ Adding structures of 7235279, 7235280, 7235281, 7235282, 7235283 via cif-deposit CGI script.	7235283.cif