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Information card for entry 7235350
Preview
| Coordinates | 7235350.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C22 H19 Cl Fe O4 |
|---|---|
| Calculated formula | C22 H19 Cl Fe O4 |
| Title of publication | Rh2(OAc)4-catalyzed 2,3-migration of β-ferrocenecarboxyl α-diazocarbonyl compounds: an efficient synthesis of ferrocene-containing α,β-unsaturated esters |
| Authors of publication | Chen, Shufeng; Du, Yan; Zhao, Haiying; Li, Baoguo |
| Journal of publication | RSC Advances |
| Year of publication | 2014 |
| Journal volume | 4 |
| Journal issue | 24 |
| Pages of publication | 12482 |
| a | 5.8525 ± 0.0014 Å |
| b | 7.4196 ± 0.0018 Å |
| c | 45.092 ± 0.01 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 1958 ± 0.8 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0468 |
| Residual factor for significantly intense reflections | 0.0422 |
| Weighted residual factors for significantly intense reflections | 0.0806 |
| Weighted residual factors for all reflections included in the refinement | 0.0813 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.935 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 232713 (current) | 2019-11-23 | cif/ Adding structures of 7235350 via cif-deposit CGI script. |
7235350.cif |
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Users of the data should acknowledge the original authors of the
structural data.